JPS6351000B2 - - Google Patents
Info
- Publication number
- JPS6351000B2 JPS6351000B2 JP5156383A JP5156383A JPS6351000B2 JP S6351000 B2 JPS6351000 B2 JP S6351000B2 JP 5156383 A JP5156383 A JP 5156383A JP 5156383 A JP5156383 A JP 5156383A JP S6351000 B2 JPS6351000 B2 JP S6351000B2
- Authority
- JP
- Japan
- Prior art keywords
- liquid
- oligosaccharide
- disaccharides
- solution
- disaccharide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000002482 oligosaccharides Chemical class 0.000 claims description 124
- 229920001542 oligosaccharide Polymers 0.000 claims description 123
- 239000007788 liquid Substances 0.000 claims description 112
- 150000002016 disaccharides Chemical class 0.000 claims description 99
- 239000000243 solution Substances 0.000 claims description 64
- 239000011550 stock solution Substances 0.000 claims description 43
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 37
- 238000000034 method Methods 0.000 claims description 25
- 235000000346 sugar Nutrition 0.000 claims description 23
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 14
- 230000002378 acidificating effect Effects 0.000 claims description 13
- 239000003729 cation exchange resin Substances 0.000 claims description 13
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 11
- 150000001340 alkali metals Chemical class 0.000 claims description 10
- 150000004043 trisaccharides Chemical class 0.000 claims description 10
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 9
- 229910052783 alkali metal Inorganic materials 0.000 claims description 8
- 239000012530 fluid Substances 0.000 claims description 7
- 238000013375 chromatographic separation Methods 0.000 claims description 6
- 150000001720 carbohydrates Chemical class 0.000 claims description 5
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 4
- 150000008163 sugars Chemical class 0.000 claims description 4
- 150000001447 alkali salts Chemical class 0.000 claims description 3
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 claims description 3
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 230000007935 neutral effect Effects 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 150000002772 monosaccharides Chemical class 0.000 description 88
- 239000011347 resin Substances 0.000 description 30
- 229920005989 resin Polymers 0.000 description 30
- 238000000926 separation method Methods 0.000 description 21
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 12
- 229930006000 Sucrose Natural products 0.000 description 7
- 239000005720 sucrose Substances 0.000 description 7
- 238000001179 sorption measurement Methods 0.000 description 6
- 229930091371 Fructose Natural products 0.000 description 5
- 239000005715 Fructose Substances 0.000 description 5
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 5
- 238000002347 injection Methods 0.000 description 5
- 239000007924 injection Substances 0.000 description 5
- 229920002307 Dextran Polymers 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 239000001632 sodium acetate Substances 0.000 description 4
- 235000017281 sodium acetate Nutrition 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 3
- 125000000185 sucrose group Chemical group 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 229910052700 potassium Inorganic materials 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical group [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 108010042889 Inulosucrase Proteins 0.000 description 1
- 241000194019 Streptococcus mutans Species 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001595 flow curve Methods 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 238000006276 transfer reaction Methods 0.000 description 1
Landscapes
- Saccharide Compounds (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5156383A JPS59179100A (ja) | 1983-03-29 | 1983-03-29 | オリゴ糖の分離法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5156383A JPS59179100A (ja) | 1983-03-29 | 1983-03-29 | オリゴ糖の分離法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59179100A JPS59179100A (ja) | 1984-10-11 |
| JPS6351000B2 true JPS6351000B2 (enrdf_load_stackoverflow) | 1988-10-12 |
Family
ID=12890438
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5156383A Granted JPS59179100A (ja) | 1983-03-29 | 1983-03-29 | オリゴ糖の分離法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59179100A (enrdf_load_stackoverflow) |
-
1983
- 1983-03-29 JP JP5156383A patent/JPS59179100A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS59179100A (ja) | 1984-10-11 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US5556546A (en) | Method of separation into three components using a simulated moving bed | |
| EP0103406B1 (en) | Extraction of sucrose | |
| JP3604935B2 (ja) | 糖類の精製方法 | |
| JPS6335636B2 (enrdf_load_stackoverflow) | ||
| US6482323B2 (en) | Chromatographic separation process | |
| US8865948B2 (en) | Method for manufacturing high-purity sorbitol syrups from sucrose and uses thereof | |
| CN113150042B (zh) | 一种乳果糖的制备方法 | |
| JPH02275835A (ja) | クエン酸含有液からのクエン酸の回収方法 | |
| JPS6351000B2 (enrdf_load_stackoverflow) | ||
| JPS6364200B2 (enrdf_load_stackoverflow) | ||
| US3403097A (en) | Process for regeneration of cation exchange resin | |
| US4226639A (en) | Silica guard bed for adsorbent used in an aqueous system | |
| FI65086C (fi) | Foerfarande foer packning av adsorbent i en separationskolonn och kromatografisk separering av en fruktor/dextrosloesning | |
| JP3694908B2 (ja) | 擬似移動床を用いた３成分分離方法 | |
| JPS5925600B2 (ja) | 果糖の製造方法 | |
| JPS6141558B2 (enrdf_load_stackoverflow) | ||
| JPH059080B2 (enrdf_load_stackoverflow) | ||
| JP4193432B2 (ja) | 糖液の精製方法 | |
| JP2834807B2 (ja) | 精製ラクチュロースの製造法 | |
| JPH1146788A (ja) | ガラクトシルスクロースの製造方法 | |
| JPH059079B2 (enrdf_load_stackoverflow) | ||
| JPS6119240B2 (enrdf_load_stackoverflow) | ||
| JP2012007907A (ja) | １，５−ｄ−アンヒドログルシトールの分離方法 | |
| KR102302447B1 (ko) | 아크릴계 이온 교환수지 및 스티렌계 이온 교환수지를 이용한 당 함유 용액의 정제 방법 | |
| CN102743897A (zh) | 一种淀粉糖液的精制方法 |