JPS59179100A - オリゴ糖の分離法 - Google Patents
オリゴ糖の分離法Info
- Publication number
- JPS59179100A JPS59179100A JP5156383A JP5156383A JPS59179100A JP S59179100 A JPS59179100 A JP S59179100A JP 5156383 A JP5156383 A JP 5156383A JP 5156383 A JP5156383 A JP 5156383A JP S59179100 A JPS59179100 A JP S59179100A
- Authority
- JP
- Japan
- Prior art keywords
- solution
- trisaccharide
- oligosaccharides
- oligosaccharide
- trisaccharides
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920001542 oligosaccharide Polymers 0.000 title claims description 99
- 150000002482 oligosaccharides Chemical class 0.000 title claims description 99
- 238000000926 separation method Methods 0.000 title claims description 19
- 150000004043 trisaccharides Chemical class 0.000 claims description 94
- 239000007788 liquid Substances 0.000 claims description 86
- 239000000243 solution Substances 0.000 claims description 78
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 35
- 239000011550 stock solution Substances 0.000 claims description 34
- 238000000034 method Methods 0.000 claims description 25
- 235000000346 sugar Nutrition 0.000 claims description 20
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 13
- 230000002378 acidificating effect Effects 0.000 claims description 12
- 239000003729 cation exchange resin Substances 0.000 claims description 12
- 238000001179 sorption measurement Methods 0.000 claims description 11
- 150000001342 alkaline earth metals Chemical class 0.000 claims description 10
- 150000001340 alkali metals Chemical class 0.000 claims description 8
- 229910052784 alkaline earth metal Inorganic materials 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 150000001720 carbohydrates Chemical class 0.000 claims description 7
- 229910052783 alkali metal Inorganic materials 0.000 claims description 6
- 150000002016 disaccharides Chemical class 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 5
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 4
- 150000008163 sugars Chemical class 0.000 claims description 4
- 150000001447 alkali salts Chemical class 0.000 claims description 3
- 239000012530 fluid Substances 0.000 claims description 3
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 230000007935 neutral effect Effects 0.000 claims description 2
- 230000004888 barrier function Effects 0.000 claims 1
- 239000000706 filtrate Substances 0.000 claims 1
- 150000002772 monosaccharides Chemical class 0.000 description 84
- 239000011347 resin Substances 0.000 description 30
- 229920005989 resin Polymers 0.000 description 30
- 229930006000 Sucrose Natural products 0.000 description 7
- 239000005720 sucrose Substances 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 5
- 238000002347 injection Methods 0.000 description 5
- 239000007924 injection Substances 0.000 description 5
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 4
- 238000013375 chromatographic separation Methods 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 239000001632 sodium acetate Substances 0.000 description 4
- 235000017281 sodium acetate Nutrition 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 3
- ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical group [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 description 2
- 229930091371 Fructose Natural products 0.000 description 2
- 239000005715 Fructose Substances 0.000 description 2
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 2
- 239000008101 lactose Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 239000004071 soot Substances 0.000 description 2
- 125000000185 sucrose group Chemical group 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- 229920002307 Dextran Polymers 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 108010042889 Inulosucrase Proteins 0.000 description 1
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 1
- 101710184309 Probable sucrose-6-phosphate hydrolase Proteins 0.000 description 1
- 241000194017 Streptococcus Species 0.000 description 1
- 102400000472 Sucrase Human genes 0.000 description 1
- 101710112652 Sucrose-6-phosphate hydrolase Proteins 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 108010042194 dextransucrase Proteins 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- -1 hydroxide Chemical class 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 235000011073 invertase Nutrition 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000006276 transfer reaction Methods 0.000 description 1
Landscapes
- Saccharide Compounds (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5156383A JPS59179100A (ja) | 1983-03-29 | 1983-03-29 | オリゴ糖の分離法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP5156383A JPS59179100A (ja) | 1983-03-29 | 1983-03-29 | オリゴ糖の分離法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS59179100A true JPS59179100A (ja) | 1984-10-11 |
| JPS6351000B2 JPS6351000B2 (enrdf_load_stackoverflow) | 1988-10-12 |
Family
ID=12890438
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5156383A Granted JPS59179100A (ja) | 1983-03-29 | 1983-03-29 | オリゴ糖の分離法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS59179100A (enrdf_load_stackoverflow) |
-
1983
- 1983-03-29 JP JP5156383A patent/JPS59179100A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6351000B2 (enrdf_load_stackoverflow) | 1988-10-12 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0663224B1 (en) | Method of separation using a simulated moving bed | |
| CN111450903A (zh) | 一种用于木糖生产的连续离子交换系统及其使用方法 | |
| US5618502A (en) | Zirconium and hafnium separation in sulfate solutions using continuous ion exchange chromatography | |
| US4443267A (en) | Method and apparatus for the continuous separation of fructose from glucose starting from invert sugar or from isomerized glucose syrups | |
| JPS59179100A (ja) | オリゴ糖の分離法 | |
| CN212732180U (zh) | 一种用于木糖生产的连续离子交换系统 | |
| CN1081191C (zh) | 从发酵液中分离d－核糖的方法 | |
| US3403097A (en) | Process for regeneration of cation exchange resin | |
| CN100463914C (zh) | 一种单糖苷酸纯化方法 | |
| JP3694908B2 (ja) | 擬似移動床を用いた３成分分離方法 | |
| JPS6364200B2 (enrdf_load_stackoverflow) | ||
| CN1090217A (zh) | 用二磷酸氢钛分离锂元素同位素的方法 | |
| JPS5845341A (ja) | 希土類金属の分離方法 | |
| JP7142753B1 (ja) | ロジウム含有めっき溶液からのロジウムの回収方法 | |
| JPH059080B2 (enrdf_load_stackoverflow) | ||
| KR820000714B1 (ko) | 탑외 재생형 혼상식 이온 교환장치의 음이온 교환수지의 재생방법 | |
| JPS6019041A (ja) | 混合樹脂の逆洗分離方法 | |
| JPH1146788A (ja) | ガラクトシルスクロースの製造方法 | |
| CN210826007U (zh) | 一种磷酸三丁酯再生装置 | |
| CN1025562C (zh) | 一种用于电镀液的羟基烷磺酸的制备工艺 | |
| JPH10230170A (ja) | イオン交換樹脂の再生方法 | |
| JPS6133624B2 (enrdf_load_stackoverflow) | ||
| JPS6140462B2 (enrdf_load_stackoverflow) | ||
| CN108636462A (zh) | 扁平床及其作为离子交换设备的物料分离方法 | |
| JPH052320B2 (enrdf_load_stackoverflow) |