JPS6325595B2 - - Google Patents
Info
- Publication number
- JPS6325595B2 JPS6325595B2 JP568081A JP568081A JPS6325595B2 JP S6325595 B2 JPS6325595 B2 JP S6325595B2 JP 568081 A JP568081 A JP 568081A JP 568081 A JP568081 A JP 568081A JP S6325595 B2 JPS6325595 B2 JP S6325595B2
- Authority
- JP
- Japan
- Prior art keywords
- trialkoxysilane
- alcohol
- alkyl alcohol
- trimethoxysilane
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 125000005233 alkylalcohol group Chemical group 0.000 claims description 17
- 239000000203 mixture Substances 0.000 claims description 16
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 15
- YUYCVXFAYWRXLS-UHFFFAOYSA-N trimethoxysilane Chemical group CO[SiH](OC)OC YUYCVXFAYWRXLS-UHFFFAOYSA-N 0.000 claims description 11
- 150000001412 amines Chemical class 0.000 claims description 9
- VKYKSIONXSXAKP-UHFFFAOYSA-N hexamethylenetetramine Chemical compound C1N(C2)CN3CN1CN2C3 VKYKSIONXSXAKP-UHFFFAOYSA-N 0.000 claims description 8
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical group C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims description 6
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 4
- 235000010299 hexamethylene tetramine Nutrition 0.000 claims description 4
- 239000004312 hexamethylene tetramine Substances 0.000 claims description 4
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims description 3
- KWYHDKDOAIKMQN-UHFFFAOYSA-N N,N,N',N'-tetramethylethylenediamine Chemical compound CN(C)CCN(C)C KWYHDKDOAIKMQN-UHFFFAOYSA-N 0.000 claims description 2
- OMAUSUKGZFZKBA-UHFFFAOYSA-N 5,5,6-trimethylheptane-1,6-diamine Chemical compound CC(C)(N)C(C)(C)CCCCN OMAUSUKGZFZKBA-UHFFFAOYSA-N 0.000 claims 1
- 238000000034 method Methods 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 4
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 235000019441 ethanol Nutrition 0.000 description 3
- 238000004817 gas chromatography Methods 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 239000010703 silicon Substances 0.000 description 3
- -1 triamyloxysilane Chemical compound 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 description 2
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
- NQRYJNQNLNOLGT-UHFFFAOYSA-N Piperidine Chemical compound C1CCNCC1 NQRYJNQNLNOLGT-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000007810 chemical reaction solvent Substances 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 238000001139 pH measurement Methods 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- RIOQSEWOXXDEQQ-UHFFFAOYSA-N triphenylphosphine Chemical compound C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 RIOQSEWOXXDEQQ-UHFFFAOYSA-N 0.000 description 2
- OTJFQRMIRKXXRS-UHFFFAOYSA-N (hydroxymethylamino)methanol Chemical compound OCNCO OTJFQRMIRKXXRS-UHFFFAOYSA-N 0.000 description 1
- DHCFZIKTQVIFQX-UHFFFAOYSA-N 2,2-dimethoxyethoxysilane Chemical compound O(C)C(CO[SiH3])OC DHCFZIKTQVIFQX-UHFFFAOYSA-N 0.000 description 1
- QHJZPBIYMJZXEO-UHFFFAOYSA-N 3,3-diethoxypropoxysilane Chemical compound C(C)OC(CCO[SiH3])OCC QHJZPBIYMJZXEO-UHFFFAOYSA-N 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 239000004471 Glycine Substances 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- PASDCCFISLVPSO-UHFFFAOYSA-N benzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1 PASDCCFISLVPSO-UHFFFAOYSA-N 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 150000004985 diamines Chemical class 0.000 description 1
- AWQTZFCYSLRFJO-UHFFFAOYSA-N diethoxy(methoxy)silane Chemical compound CCO[SiH](OC)OCC AWQTZFCYSLRFJO-UHFFFAOYSA-N 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- SYECJBOWSGTPLU-UHFFFAOYSA-N hexane-1,1-diamine Chemical compound CCCCCC(N)N SYECJBOWSGTPLU-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- TXXWBTOATXBWDR-UHFFFAOYSA-N n,n,n',n'-tetramethylhexane-1,6-diamine Chemical compound CN(C)CCCCCCN(C)C TXXWBTOATXBWDR-UHFFFAOYSA-N 0.000 description 1
- 150000002903 organophosphorus compounds Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000011863 silicon-based powder Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- LFQCEHFDDXELDD-UHFFFAOYSA-N tetramethyl orthosilicate Chemical compound CO[Si](OC)(OC)OC LFQCEHFDDXELDD-UHFFFAOYSA-N 0.000 description 1
- UCSBCWBHZLSFGC-UHFFFAOYSA-N tributoxysilane Chemical compound CCCCO[SiH](OCCCC)OCCCC UCSBCWBHZLSFGC-UHFFFAOYSA-N 0.000 description 1
- QQQSFSZALRVCSZ-UHFFFAOYSA-N triethoxysilane Chemical compound CCO[SiH](OCC)OCC QQQSFSZALRVCSZ-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP568081A JPS57118592A (en) | 1981-01-16 | 1981-01-16 | Stable trialkoxysilane composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP568081A JPS57118592A (en) | 1981-01-16 | 1981-01-16 | Stable trialkoxysilane composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS57118592A JPS57118592A (en) | 1982-07-23 |
| JPS6325595B2 true JPS6325595B2 (enrdf_load_html_response) | 1988-05-26 |
Family
ID=11617803
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP568081A Granted JPS57118592A (en) | 1981-01-16 | 1981-01-16 | Stable trialkoxysilane composition |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS57118592A (enrdf_load_html_response) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1323037C (en) * | 1987-02-23 | 1993-10-12 | Yoshiro Ohta | Process for the production of trialkoxysilanes |
| US5116637A (en) * | 1990-06-04 | 1992-05-26 | Dow Corning Corporation | Amine catalysts for the low temperature conversion of silica precursors to silica |
| US20050215713A1 (en) * | 2004-03-26 | 2005-09-29 | Hessell Edward T | Method of producing a crosslinked coating in the manufacture of integrated circuits |
| WO2024111422A1 (ja) | 2022-11-21 | 2024-05-30 | 信越化学工業株式会社 | ハイドロジェンシラン組成物およびヒドロシリル化反応物の製造方法 |
-
1981
- 1981-01-16 JP JP568081A patent/JPS57118592A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS57118592A (en) | 1982-07-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0135813A2 (en) | Preparation of aminopropyltrialkoxysilanes and/or aminoalkylaloxysilanes | |
| JP7457762B2 (ja) | コロイダルシリカ及びその製造方法 | |
| JPS6325595B2 (enrdf_load_html_response) | ||
| JPS61263986A (ja) | 有機けい素化合物 | |
| BR112015024975B1 (pt) | Processo para preparação de tiocarboxilato silano e processo para preparação de uma solução aquosa de um sal de um ácido tiocarboxílico | |
| JP6479996B2 (ja) | シラノールの金属塩からのシロキサノールの製造方法 | |
| JP2009263316A (ja) | 不完全縮合オリゴシルセスキオキサンの製造方法 | |
| SU414794A3 (enrdf_load_html_response) | ||
| US20100113812A1 (en) | Process for preparing organic silane compounds having beta-cyano ester group | |
| WO2001042250A2 (en) | Process for production of diphenyl-dialkoxysilane, phenylalkyl-dialkoxysilane, octaphenylcyclotetrasiloxane and sym-tetraalkyltetraphenyl-cyclotetrasiloxane | |
| US3954651A (en) | Silyation agent for gas chromatography | |
| JPS5970691A (ja) | 水素含有シリルカ−バメ−ト | |
| US4395564A (en) | Process for the preparation of alkoxyhydridosilanes | |
| SU482046A3 (ru) | Способ получени органогидросиланов | |
| JPH0219385A (ja) | アミノアルキル基含有ケイ素化合物の製造方法 | |
| JP3288747B2 (ja) | トリメチルシリルシアニドの製造法 | |
| JPH05239072A (ja) | 含フッ素有機ケイ素化合物及びその製造方法 | |
| EP0322819B1 (en) | Method for the preparation of beta-substituted allylsilane | |
| JPS6323196B2 (enrdf_load_html_response) | ||
| Anderson | Phenyl silicon isothiocyanates | |
| JPH026488A (ja) | ω−アルケニルシラン化合物 | |
| JPH0357110B2 (enrdf_load_html_response) | ||
| JPS5939849A (ja) | 含フツ素脂肪族基置換アルキル化又はアルケニル化マロン酸エステル又はその誘導体 | |
| JPH085900B2 (ja) | ビニル基含有シロキサン化合物及びその製造方法 | |
| JP2584775B2 (ja) | トリアルコキシシランの分離精製法 |