JPS6318933B2 - - Google Patents
Info
- Publication number
- JPS6318933B2 JPS6318933B2 JP11875882A JP11875882A JPS6318933B2 JP S6318933 B2 JPS6318933 B2 JP S6318933B2 JP 11875882 A JP11875882 A JP 11875882A JP 11875882 A JP11875882 A JP 11875882A JP S6318933 B2 JPS6318933 B2 JP S6318933B2
- Authority
- JP
- Japan
- Prior art keywords
- reaction
- ammonia
- reactor
- mixture
- alkylene oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 98
- 239000000203 mixture Substances 0.000 claims description 65
- 238000006243 chemical reaction Methods 0.000 claims description 51
- 229910021529 ammonia Inorganic materials 0.000 claims description 45
- 125000002947 alkylene group Chemical group 0.000 claims description 28
- 238000000034 method Methods 0.000 claims description 26
- 239000012530 fluid Substances 0.000 claims description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 230000003197 catalytic effect Effects 0.000 claims description 4
- 239000008240 homogeneous mixture Substances 0.000 claims description 2
- 239000000047 product Substances 0.000 description 45
- 239000011541 reaction mixture Substances 0.000 description 35
- 239000012071 phase Substances 0.000 description 16
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 14
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 9
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- 239000007788 liquid Substances 0.000 description 6
- 239000007791 liquid phase Substances 0.000 description 6
- 239000000376 reactant Substances 0.000 description 6
- 230000001105 regulatory effect Effects 0.000 description 6
- 150000001412 amines Chemical class 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical group C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 4
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 125000002091 cationic group Chemical group 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 238000010924 continuous production Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- RBACIKXCRWGCBB-UHFFFAOYSA-N 1,2-Epoxybutane Chemical compound CCC1CO1 RBACIKXCRWGCBB-UHFFFAOYSA-N 0.000 description 1
- GELKGHVAFRCJNA-UHFFFAOYSA-N 2,2-Dimethyloxirane Chemical compound CC1(C)CO1 GELKGHVAFRCJNA-UHFFFAOYSA-N 0.000 description 1
- PQXKWPLDPFFDJP-UHFFFAOYSA-N 2,3-dimethyloxirane Chemical compound CC1OC1C PQXKWPLDPFFDJP-UHFFFAOYSA-N 0.000 description 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 238000013517 stratification Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11875882A JPS5913751A (ja) | 1982-07-09 | 1982-07-09 | アルカノ−ルアミンの連続的製法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11875882A JPS5913751A (ja) | 1982-07-09 | 1982-07-09 | アルカノ−ルアミンの連続的製法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5913751A JPS5913751A (ja) | 1984-01-24 |
| JPS6318933B2 true JPS6318933B2 (enrdf_load_stackoverflow) | 1988-04-20 |
Family
ID=14744324
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11875882A Granted JPS5913751A (ja) | 1982-07-09 | 1982-07-09 | アルカノ−ルアミンの連続的製法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5913751A (enrdf_load_stackoverflow) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5633408A (en) | 1994-06-28 | 1997-05-27 | Mitsui Toatsu Chemicals, Inc. | Process for preparing alkanolamines |
| JP5107260B2 (ja) | 2006-12-07 | 2012-12-26 | 三菱重工業株式会社 | モノ低級アルキルモノアルカノールアミンの製造方法及び装置 |
| JP5330735B2 (ja) | 2008-05-26 | 2013-10-30 | 三菱重工業株式会社 | モノ低級アルキルモノアルカノールアミンの製造方法及び装置 |
| JP5701442B1 (ja) * | 2014-09-05 | 2015-04-15 | 関西ペイント株式会社 | カチオン電着塗料組成物 |
| US11753364B2 (en) * | 2018-02-06 | 2023-09-12 | Basf Se | Method for producing C2-C4 mono alkanol amines using an acid cation exchanger as a catalyst |
-
1982
- 1982-07-09 JP JP11875882A patent/JPS5913751A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5913751A (ja) | 1984-01-24 |
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