JPS624807A - 希土類磁石用合金粉末の製造方法 - Google Patents
希土類磁石用合金粉末の製造方法Info
- Publication number
- JPS624807A JPS624807A JP14318385A JP14318385A JPS624807A JP S624807 A JPS624807 A JP S624807A JP 14318385 A JP14318385 A JP 14318385A JP 14318385 A JP14318385 A JP 14318385A JP S624807 A JPS624807 A JP S624807A
- Authority
- JP
- Japan
- Prior art keywords
- powder
- rare earth
- less
- alloy powder
- atomic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 150
- 229910045601 alloy Inorganic materials 0.000 title claims abstract description 67
- 239000000956 alloy Substances 0.000 title claims abstract description 67
- 229910052761 rare earth metal Inorganic materials 0.000 title claims abstract description 32
- 150000002910 rare earth metals Chemical class 0.000 title claims abstract description 24
- 238000004519 manufacturing process Methods 0.000 title claims description 22
- 229910001404 rare earth metal oxide Inorganic materials 0.000 claims abstract description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 25
- 239000001301 oxygen Substances 0.000 claims abstract description 25
- 239000002994 raw material Substances 0.000 claims abstract description 25
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 22
- 238000009792 diffusion process Methods 0.000 claims abstract description 19
- 239000000203 mixture Substances 0.000 claims abstract description 18
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 11
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052692 Dysprosium Inorganic materials 0.000 claims abstract description 8
- 229910052742 iron Inorganic materials 0.000 claims abstract description 8
- 229910052777 Praseodymium Inorganic materials 0.000 claims abstract description 7
- 229910052810 boron oxide Inorganic materials 0.000 claims abstract description 7
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052779 Neodymium Inorganic materials 0.000 claims abstract description 4
- 239000002245 particle Substances 0.000 claims description 29
- 239000007795 chemical reaction product Substances 0.000 claims description 15
- 239000002002 slurry Substances 0.000 claims description 14
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 10
- 229910052746 lanthanum Inorganic materials 0.000 claims description 10
- 239000011812 mixed powder Substances 0.000 claims description 10
- 239000000470 constituent Substances 0.000 claims description 8
- 230000002829 reductive effect Effects 0.000 claims description 7
- 229910052691 Erbium Inorganic materials 0.000 claims description 6
- 239000011261 inert gas Substances 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 239000002184 metal Substances 0.000 claims description 6
- 229910052693 Europium Inorganic materials 0.000 claims description 5
- 229910052772 Samarium Inorganic materials 0.000 claims description 5
- 229910052727 yttrium Inorganic materials 0.000 claims description 5
- 229910052684 Cerium Inorganic materials 0.000 claims description 4
- 229910052769 Ytterbium Inorganic materials 0.000 claims description 4
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 claims description 4
- 229910052688 Gadolinium Inorganic materials 0.000 claims description 3
- 229910052775 Thulium Inorganic materials 0.000 claims description 3
- 238000011282 treatment Methods 0.000 abstract description 8
- 238000005342 ion exchange Methods 0.000 abstract description 7
- 229910052791 calcium Inorganic materials 0.000 abstract description 6
- 239000013078 crystal Substances 0.000 abstract description 6
- 229910052796 boron Inorganic materials 0.000 abstract description 5
- 238000002156 mixing Methods 0.000 abstract description 4
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 abstract description 2
- 239000001110 calcium chloride Substances 0.000 abstract description 2
- 229910001628 calcium chloride Inorganic materials 0.000 abstract description 2
- 235000011148 calcium chloride Nutrition 0.000 abstract description 2
- 238000006722 reduction reaction Methods 0.000 description 40
- 239000011575 calcium Substances 0.000 description 39
- 238000006243 chemical reaction Methods 0.000 description 11
- 238000000034 method Methods 0.000 description 9
- 230000004907 flux Effects 0.000 description 8
- 239000003638 chemical reducing agent Substances 0.000 description 6
- 239000004575 stone Substances 0.000 description 6
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- -1 CtJ Inorganic materials 0.000 description 4
- 229910000640 Fe alloy Inorganic materials 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 230000032683 aging Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- 102100036439 Amyloid beta precursor protein binding family B member 1 Human genes 0.000 description 2
- 101100444028 Drosophila melanogaster Dso2 gene Proteins 0.000 description 2
- 229910000592 Ferroniobium Inorganic materials 0.000 description 2
- 229910001047 Hard ferrite Inorganic materials 0.000 description 2
- 101000928670 Homo sapiens Amyloid beta precursor protein binding family B member 1 Proteins 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 229910017052 cobalt Inorganic materials 0.000 description 2
- 239000010941 cobalt Substances 0.000 description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000005347 demagnetization Effects 0.000 description 2
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000009776 industrial production Methods 0.000 description 2
- ZFGFKQDDQUAJQP-UHFFFAOYSA-N iron niobium Chemical compound [Fe].[Fe].[Nb] ZFGFKQDDQUAJQP-UHFFFAOYSA-N 0.000 description 2
- 230000005415 magnetization Effects 0.000 description 2
- 229910052758 niobium Inorganic materials 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 229910052715 tantalum Inorganic materials 0.000 description 2
- 229910052720 vanadium Inorganic materials 0.000 description 2
- 229910000967 As alloy Inorganic materials 0.000 description 1
- 229910000758 Br alloy Inorganic materials 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 229910052689 Holmium Inorganic materials 0.000 description 1
- 101100448410 Mus musculus Gkn1 gene Proteins 0.000 description 1
- BGPVFRJUHWVFKM-UHFFFAOYSA-N N1=C2C=CC=CC2=[N+]([O-])C1(CC1)CCC21N=C1C=CC=CC1=[N+]2[O-] Chemical compound N1=C2C=CC=CC2=[N+]([O-])C1(CC1)CCC21N=C1C=CC=CC1=[N+]2[O-] BGPVFRJUHWVFKM-UHFFFAOYSA-N 0.000 description 1
- 229910052771 Terbium Inorganic materials 0.000 description 1
- 229910000828 alnico Inorganic materials 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 1
- MOWNZPNSYMGTMD-UHFFFAOYSA-N oxidoboron Chemical class O=[B] MOWNZPNSYMGTMD-UHFFFAOYSA-N 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 229910000679 solder Inorganic materials 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
Landscapes
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14318385A JPS624807A (ja) | 1985-06-28 | 1985-06-28 | 希土類磁石用合金粉末の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14318385A JPS624807A (ja) | 1985-06-28 | 1985-06-28 | 希土類磁石用合金粉末の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS624807A true JPS624807A (ja) | 1987-01-10 |
| JPH0586441B2 JPH0586441B2 (enrdf_load_stackoverflow) | 1993-12-13 |
Family
ID=15332812
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP14318385A Granted JPS624807A (ja) | 1985-06-28 | 1985-06-28 | 希土類磁石用合金粉末の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS624807A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5064465A (en) * | 1990-11-29 | 1991-11-12 | Industrial Technology Research Institute | Process for preparing rare earth-iron-boron alloy powders |
| JP2009113375A (ja) * | 2007-11-07 | 2009-05-28 | Toshiba Corp | バイオプラスチック及びバイオプラスチック成形品 |
-
1985
- 1985-06-28 JP JP14318385A patent/JPS624807A/ja active Granted
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5064465A (en) * | 1990-11-29 | 1991-11-12 | Industrial Technology Research Institute | Process for preparing rare earth-iron-boron alloy powders |
| JP2009113375A (ja) * | 2007-11-07 | 2009-05-28 | Toshiba Corp | バイオプラスチック及びバイオプラスチック成形品 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0586441B2 (enrdf_load_stackoverflow) | 1993-12-13 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR960008185B1 (ko) | 희토류-철계 영구자석 및 이의 제조방법 | |
| US4762574A (en) | Rare earth-iron-boron premanent magnets | |
| US4747874A (en) | Rare earth-iron-boron permanent magnets with enhanced coercivity | |
| JPS61270313A (ja) | 希土類合金紛末の製造方法 | |
| US4954186A (en) | Rear earth-iron-boron permanent magnets containing aluminum | |
| US4952252A (en) | Rare earth-iron-boron-permanent magnets | |
| JPS624807A (ja) | 希土類磁石用合金粉末の製造方法 | |
| JPH0685369B2 (ja) | 永久磁石の製造方法 | |
| JPS624806A (ja) | 希土類磁石用合金粉末の製造方法 | |
| JPS6223960A (ja) | 高性能永久磁石材料 | |
| US4878958A (en) | Method for preparing rare earth-iron-boron permanent magnets | |
| JPS627831A (ja) | 永久磁石材料の製造方法 | |
| KR20200018267A (ko) | 자석 분말 및 자석 분말의 제조 방법 | |
| JP3151087B2 (ja) | Ｒ−Ｆｅ−Ｂ系永久磁石用原料粉末の製造方法及び原料粉末調整用合金粉末 | |
| JPS62132302A (ja) | 希土類−鉄−ホウ素系合金粉末及びその製法 | |
| JP3178848B2 (ja) | 永久磁石の製造方法 | |
| US4933009A (en) | Composition for preparing rare earth-iron-boron-permanent magnets | |
| JPS6247455A (ja) | 高性能永久磁石材料 | |
| JPS627830A (ja) | 永久磁石材料の製造方法 | |
| JP3299000B2 (ja) | Ｒ−Ｆｅ−Ｂ系永久磁石用原料粉末の製造方法及び原料粉末調整用合金粉末 | |
| JP3151088B2 (ja) | Ｒ−Ｆｅ−Ｂ系永久磁石用原料粉末の製造方法及び原料粉末調整用合金粉末 | |
| JPH0320044B2 (enrdf_load_stackoverflow) | ||
| JPS6271201A (ja) | ボンド磁石 | |
| JPH0422104A (ja) | 永久磁石の製造方法 | |
| JPH05179313A (ja) | 希土類磁石材料の製造法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| S533 | Written request for registration of change of name |
Free format text: JAPANESE INTERMEDIATE CODE: R313533 |
|
| R350 | Written notification of registration of transfer |
Free format text: JAPANESE INTERMEDIATE CODE: R350 |
|
| EXPY | Cancellation because of completion of term |