JPS6237039B2 - - Google Patents
Info
- Publication number
- JPS6237039B2 JPS6237039B2 JP9235081A JP9235081A JPS6237039B2 JP S6237039 B2 JPS6237039 B2 JP S6237039B2 JP 9235081 A JP9235081 A JP 9235081A JP 9235081 A JP9235081 A JP 9235081A JP S6237039 B2 JPS6237039 B2 JP S6237039B2
- Authority
- JP
- Japan
- Prior art keywords
- sorbitan
- reaction
- formula
- hydrocarbon group
- modified silicone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical class OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 claims description 44
- 229920001296 polysiloxane Polymers 0.000 claims description 34
- 150000001875 compounds Chemical class 0.000 claims description 17
- 238000007259 addition reaction Methods 0.000 claims description 13
- -1 polysiloxane Polymers 0.000 claims description 13
- 125000001183 hydrocarbyl group Chemical group 0.000 claims description 8
- 125000001931 aliphatic group Chemical group 0.000 claims description 7
- 239000007809 chemical reaction catalyst Substances 0.000 claims description 5
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 125000004430 oxygen atom Chemical group O* 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims description 2
- 125000004429 atom Chemical group 0.000 claims 1
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 36
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 23
- 238000006243 chemical reaction Methods 0.000 description 17
- SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical compound [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 description 16
- 239000000047 product Substances 0.000 description 12
- 238000000034 method Methods 0.000 description 11
- 239000000243 solution Substances 0.000 description 10
- 235000011056 potassium acetate Nutrition 0.000 description 8
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Substances [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 230000001476 alcoholic effect Effects 0.000 description 5
- 239000003513 alkali Substances 0.000 description 5
- 239000007810 chemical reaction solvent Substances 0.000 description 5
- 238000006356 dehydrogenation reaction Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 150000005846 sugar alcohols Polymers 0.000 description 5
- 239000004094 surface-active agent Substances 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 4
- 239000002253 acid Substances 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 4
- 238000002329 infrared spectrum Methods 0.000 description 4
- STMDPCBYJCIZOD-UHFFFAOYSA-N 2-(2,4-dinitroanilino)-4-methylpentanoic acid Chemical compound CC(C)CC(C(O)=O)NC1=CC=C([N+]([O-])=O)C=C1[N+]([O-])=O STMDPCBYJCIZOD-UHFFFAOYSA-N 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 3
- BHELZAPQIKSEDF-UHFFFAOYSA-N allyl bromide Chemical compound BrCC=C BHELZAPQIKSEDF-UHFFFAOYSA-N 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical group [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 238000005481 NMR spectroscopy Methods 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 239000005456 alcohol based solvent Substances 0.000 description 2
- 239000002537 cosmetic Substances 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 239000004205 dimethyl polysiloxane Substances 0.000 description 2
- 235000013870 dimethyl polysiloxane Nutrition 0.000 description 2
- 238000001879 gelation Methods 0.000 description 2
- 238000000655 nuclear magnetic resonance spectrum Methods 0.000 description 2
- 125000000962 organic group Chemical group 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 230000002250 progressing effect Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000002216 antistatic agent Substances 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000004872 foam stabilizing agent Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 125000001165 hydrophobic group Chemical group 0.000 description 1
- MOYKHGMNXAOIAT-JGWLITMVSA-N isosorbide dinitrate Chemical compound [O-][N+](=O)O[C@H]1CO[C@@H]2[C@H](O[N+](=O)[O-])CO[C@@H]21 MOYKHGMNXAOIAT-JGWLITMVSA-N 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 125000006353 oxyethylene group Chemical group 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000004597 plastic additive Substances 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical group 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate group Chemical group S(=O)(=O)([O-])[O-] QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Landscapes
- Silicon Polymers (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP9235081A JPS57209295A (en) | 1981-06-17 | 1981-06-17 | Preparation of sorbitan-modified silicone compound |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP9235081A JPS57209295A (en) | 1981-06-17 | 1981-06-17 | Preparation of sorbitan-modified silicone compound |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS57209295A JPS57209295A (en) | 1982-12-22 |
JPS6237039B2 true JPS6237039B2 (enrdf_load_stackoverflow) | 1987-08-10 |
Family
ID=14051950
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP9235081A Granted JPS57209295A (en) | 1981-06-17 | 1981-06-17 | Preparation of sorbitan-modified silicone compound |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS57209295A (enrdf_load_stackoverflow) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4318537A1 (de) * | 1993-06-04 | 1994-12-08 | Bayer Ag | Kationische siloxanylmodifizierte polyhydroxylierte Kohlenwasserstoffe |
DE4318536A1 (de) * | 1993-06-04 | 1994-12-08 | Bayer Ag | Siloxanylmodifizierte polyhydroxylierte Kohlenwasserstoffe |
DE4318539A1 (de) * | 1993-06-04 | 1994-12-08 | Bayer Ag | Anionische siloxanylmodifizierte polyhydroxylierte Kohlenwasserstoffe |
US8288498B2 (en) | 2007-03-30 | 2012-10-16 | Nof Corporation | Sugar-alcohol-modified organopolysiloxane compound and processes for producing the same |
GB0714817D0 (en) * | 2007-07-31 | 2007-09-12 | Croda Int Plc | Polyglycerol derivatives |
US8124061B2 (en) | 2007-11-02 | 2012-02-28 | Kimberly-Clark Worldwide, Inc. | Cleansing compositions including modified sorbitan siloxanes and use thereof |
EP2211995B1 (en) * | 2007-11-02 | 2012-01-18 | Kimberly-Clark Worldwide, Inc. | Cleansing compositions including modified sorbitan siloxanes and use thereof |
US7820149B2 (en) | 2007-11-02 | 2010-10-26 | Kimberly-Clark Worldwide, Inc. | Modified sorbitan siloxane compositions and use thereof |
KR101313974B1 (ko) * | 2009-09-02 | 2013-10-01 | 캐논 가부시끼가이샤 | 액체 토출 헤드 |
JP6292438B2 (ja) * | 2013-12-05 | 2018-03-14 | ナガセケムテックス株式会社 | 二糖類化合物、変性オルガノポリシロキサン化合物及び界面活性剤 |
EP3147308A4 (en) | 2014-04-21 | 2018-02-28 | Dow Corning Toray Co., Ltd. | Method for producing liquid high-purity sugar derivative-modified silicone or composition thereof |
FR3022246B1 (fr) * | 2014-06-13 | 2018-03-02 | Centre National De La Recherche Scientifique | Compositions d'ethers mono-alkyliques de monoanhydro-hexitols, procedes de preparation et leur utilisation |
JP2024111903A (ja) * | 2023-02-07 | 2024-08-20 | 信越化学工業株式会社 | 有機ケイ素化合物、その加水分解縮合物、コーティング組成物および被覆物品 |
-
1981
- 1981-06-17 JP JP9235081A patent/JPS57209295A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS57209295A (en) | 1982-12-22 |
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