JPS62226815A - ジルコニア系コロイドゾルの製造方法 - Google Patents
ジルコニア系コロイドゾルの製造方法Info
- Publication number
- JPS62226815A JPS62226815A JP6729386A JP6729386A JPS62226815A JP S62226815 A JPS62226815 A JP S62226815A JP 6729386 A JP6729386 A JP 6729386A JP 6729386 A JP6729386 A JP 6729386A JP S62226815 A JPS62226815 A JP S62226815A
- Authority
- JP
- Japan
- Prior art keywords
- colloidal
- soln
- salt
- solution
- washing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 title claims abstract description 32
- 238000004519 manufacturing process Methods 0.000 title claims description 5
- 238000005406 washing Methods 0.000 claims abstract description 15
- 239000012528 membrane Substances 0.000 claims abstract description 14
- 150000003839 salts Chemical class 0.000 claims abstract description 10
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 5
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 5
- 229910052727 yttrium Inorganic materials 0.000 claims abstract description 5
- 230000003301 hydrolyzing effect Effects 0.000 claims abstract description 4
- 229910052751 metal Inorganic materials 0.000 claims abstract description 3
- 239000000243 solution Substances 0.000 claims description 42
- 239000007864 aqueous solution Substances 0.000 claims description 22
- 239000000084 colloidal system Substances 0.000 claims description 20
- 238000001914 filtration Methods 0.000 claims description 17
- 239000011148 porous material Substances 0.000 claims description 8
- 150000003754 zirconium Chemical class 0.000 claims description 7
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 3
- 239000011575 calcium Substances 0.000 claims description 3
- 239000011777 magnesium Substances 0.000 claims description 3
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 2
- 239000002245 particle Substances 0.000 abstract description 26
- 239000000843 powder Substances 0.000 abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 16
- 238000000034 method Methods 0.000 abstract description 9
- 239000003960 organic solvent Substances 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 5
- 239000002904 solvent Substances 0.000 abstract description 4
- 238000001354 calcination Methods 0.000 abstract description 2
- 230000002349 favourable effect Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 description 8
- 230000007062 hydrolysis Effects 0.000 description 7
- 238000006460 hydrolysis reaction Methods 0.000 description 7
- 150000001450 anions Chemical class 0.000 description 6
- 229910021645 metal ion Inorganic materials 0.000 description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 239000007788 liquid Substances 0.000 description 4
- 239000000758 substrate Substances 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 238000010304 firing Methods 0.000 description 3
- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 description 3
- -1 oxygen ion Chemical class 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 239000011164 primary particle Substances 0.000 description 2
- 238000000108 ultra-filtration Methods 0.000 description 2
- OERNJTNJEZOPIA-UHFFFAOYSA-N zirconium nitrate Chemical compound [Zr+4].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O OERNJTNJEZOPIA-UHFFFAOYSA-N 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- OBOSXEWFRARQPU-UHFFFAOYSA-N 2-n,2-n-dimethylpyridine-2,5-diamine Chemical compound CN(C)C1=CC=C(N)C=N1 OBOSXEWFRARQPU-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000012620 biological material Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000011437 continuous method Methods 0.000 description 1
- RKTYLMNFRDHKIL-UHFFFAOYSA-N copper;5,10,15,20-tetraphenylporphyrin-22,24-diide Chemical compound [Cu+2].C1=CC(C(=C2C=CC([N-]2)=C(C=2C=CC=CC=2)C=2C=CC(N=2)=C(C=2C=CC=CC=2)C2=CC=C3[N-]2)C=2C=CC=CC=2)=NC1=C3C1=CC=CC=C1 RKTYLMNFRDHKIL-UHFFFAOYSA-N 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000000502 dialysis Methods 0.000 description 1
- RCJVRSBWZCNNQT-UHFFFAOYSA-N dichloridooxygen Chemical compound ClOCl RCJVRSBWZCNNQT-UHFFFAOYSA-N 0.000 description 1
- 238000007604 dielectric heating drying Methods 0.000 description 1
- 238000004455 differential thermal analysis Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000002296 dynamic light scattering Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000020169 heat generation Effects 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000011226 reinforced ceramic Substances 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000011163 secondary particle Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- ZXAUZSQITFJWPS-UHFFFAOYSA-J zirconium(4+);disulfate Chemical compound [Zr+4].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O ZXAUZSQITFJWPS-UHFFFAOYSA-J 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6729386A JPS62226815A (ja) | 1986-03-27 | 1986-03-27 | ジルコニア系コロイドゾルの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6729386A JPS62226815A (ja) | 1986-03-27 | 1986-03-27 | ジルコニア系コロイドゾルの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62226815A true JPS62226815A (ja) | 1987-10-05 |
| JPH0355413B2 JPH0355413B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1991-08-23 |
Family
ID=13340790
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP6729386A Granted JPS62226815A (ja) | 1986-03-27 | 1986-03-27 | ジルコニア系コロイドゾルの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62226815A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6483521A (en) * | 1987-09-25 | 1989-03-29 | Nissan Chemical Ind Ltd | Production of zirconium oxide fine powder |
| JPH05170442A (ja) * | 1991-12-24 | 1993-07-09 | Nissan Chem Ind Ltd | ジルコニア系ゾルの製造方法 |
| JP2547477B2 (ja) * | 1989-02-10 | 1996-10-23 | 株式会社日本触媒 | ジルコニアゾルおよびその製造方法 |
| US6899948B2 (en) | 1999-10-28 | 2005-05-31 | 3M Innovative Properties Company | Dental materials with nano-sized silica particles |
| JP2008024555A (ja) * | 2006-07-21 | 2008-02-07 | Tosoh Corp | ジルコニア微粉末及びその製造方法並びにその用途 |
| JPWO2006006277A1 (ja) * | 2004-07-09 | 2008-04-24 | 旭化成ケミカルズ株式会社 | シクロオレフィン製造用触媒及び製造方法 |
| US7393882B2 (en) | 2002-01-31 | 2008-07-01 | 3M Innovative Properties Company | Dental pastes, dental articles, and methods |
| CN108550904A (zh) * | 2018-04-19 | 2018-09-18 | 北京理工大学 | 一种纳米多孔阵列状固态化电解质、制备方法及锂电池 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61141619A (ja) * | 1984-12-13 | 1986-06-28 | Dowa Mining Co Ltd | ジルコニア微粉体の製造法 |
-
1986
- 1986-03-27 JP JP6729386A patent/JPS62226815A/ja active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61141619A (ja) * | 1984-12-13 | 1986-06-28 | Dowa Mining Co Ltd | ジルコニア微粉体の製造法 |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6483521A (en) * | 1987-09-25 | 1989-03-29 | Nissan Chemical Ind Ltd | Production of zirconium oxide fine powder |
| JP2547477B2 (ja) * | 1989-02-10 | 1996-10-23 | 株式会社日本触媒 | ジルコニアゾルおよびその製造方法 |
| JPH05170442A (ja) * | 1991-12-24 | 1993-07-09 | Nissan Chem Ind Ltd | ジルコニア系ゾルの製造方法 |
| US6899948B2 (en) | 1999-10-28 | 2005-05-31 | 3M Innovative Properties Company | Dental materials with nano-sized silica particles |
| US7393882B2 (en) | 2002-01-31 | 2008-07-01 | 3M Innovative Properties Company | Dental pastes, dental articles, and methods |
| JPWO2006006277A1 (ja) * | 2004-07-09 | 2008-04-24 | 旭化成ケミカルズ株式会社 | シクロオレフィン製造用触媒及び製造方法 |
| JP2008024555A (ja) * | 2006-07-21 | 2008-02-07 | Tosoh Corp | ジルコニア微粉末及びその製造方法並びにその用途 |
| CN108550904A (zh) * | 2018-04-19 | 2018-09-18 | 北京理工大学 | 一种纳米多孔阵列状固态化电解质、制备方法及锂电池 |
| CN108550904B (zh) * | 2018-04-19 | 2021-01-29 | 北京理工大学 | 一种纳米多孔阵列状固态化电解质、制备方法及锂电池 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0355413B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1991-08-23 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Fu et al. | A novel γ-Al2O3 nanofiltration membrane via introducing hollow microspheres into interlayers for improving water permeability | |
| CN106044951A (zh) | 一种工业酸性废水的回收利用方法及装置 | |
| JPS62226815A (ja) | ジルコニア系コロイドゾルの製造方法 | |
| JPS62265104A (ja) | セラミツク粉末の製造方法 | |
| US3442817A (en) | Preparation of zirconia and hafnia sols | |
| JP3446057B2 (ja) | シリカゾルの製造及び濃縮法 | |
| CN107349787A (zh) | 一种添加氨基化石墨烯量子点的正渗透膜制备方法、所制备的正渗透膜以及该膜的应用 | |
| JPH0524844A (ja) | 水和ジルコニアゾルおよびジルコニア粉末の製造方法 | |
| CN111620458A (zh) | 一种卤水浓缩和软化处理的方法及装置 | |
| US4722833A (en) | Fine coagulated particles of ultrafine monoclinic zirconia crystals oriented in a fiber bundle-like form and method of manufacturing them | |
| EP3328523B1 (en) | Process for the recovery of sodium sulfate | |
| Da et al. | Influence of compatibility between sol and intermediate layer on the performance of yttria-stabilized zirconia nanofiltration membrane | |
| JPS632809A (ja) | 高純度ジルコニアゾルの製造方法 | |
| JPS6143286B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
| JPS62235215A (ja) | ルチル型酸化チタンゾルの製造方法 | |
| CN211921101U (zh) | 一种钛白酸性废水中水回用装置 | |
| CN1509805A (zh) | 一种水处理用纳米多微孔陶瓷复合膜的制备方法 | |
| Wang et al. | Formation of dextran-Zr dynamic membrane and study on concentration of protein hemoglobin solution | |
| JPH0617233B2 (ja) | 五酸化アンチモンゾルの製造法 | |
| CN114804546B (zh) | 一种基于膜技术的pta母液回收处理方法 | |
| CN108097046A (zh) | 一种用无机陶瓷膜技术制备纳米粉体材料的方法 | |
| Missaoui et al. | Removing organic dye by cellulose acetate nanocomposite membrane ultrafiltration: Effect of bio-nanoparticle size | |
| CN85107743A (zh) | 联产硫酸钡和氧化镁的盐酸循环法 | |
| JPS62212225A (ja) | ジルコニア含有微粉末の製造方法 | |
| CN211920886U (zh) | 一种利用膜分离技术制备电池级碳酸锂的装置 |