JPS61247607A - ペロブスカイト構造を持つ化合物の原料粉末の調製方法 - Google Patents
ペロブスカイト構造を持つ化合物の原料粉末の調製方法Info
- Publication number
- JPS61247607A JPS61247607A JP60086142A JP8614285A JPS61247607A JP S61247607 A JPS61247607 A JP S61247607A JP 60086142 A JP60086142 A JP 60086142A JP 8614285 A JP8614285 A JP 8614285A JP S61247607 A JPS61247607 A JP S61247607A
- Authority
- JP
- Japan
- Prior art keywords
- precipitate
- raw material
- material powder
- component
- compound
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 46
- 239000002994 raw material Substances 0.000 title claims abstract description 27
- 238000000034 method Methods 0.000 title claims description 37
- 150000001875 compounds Chemical class 0.000 title claims description 29
- 239000002244 precipitate Substances 0.000 claims abstract description 35
- 229910052751 metal Inorganic materials 0.000 claims abstract description 32
- 239000002184 metal Substances 0.000 claims abstract description 27
- 239000000470 constituent Substances 0.000 claims abstract description 16
- 238000001354 calcination Methods 0.000 claims abstract description 12
- 239000006185 dispersion Substances 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 230000001476 alcoholic effect Effects 0.000 claims abstract description 7
- 238000002156 mixing Methods 0.000 claims abstract description 3
- 150000004703 alkoxides Chemical class 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 150000002739 metals Chemical class 0.000 claims description 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 7
- 239000001301 oxygen Substances 0.000 claims description 7
- 229910052760 oxygen Inorganic materials 0.000 claims description 7
- 238000001035 drying Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 abstract description 2
- 125000004430 oxygen atom Chemical group O* 0.000 abstract 2
- 239000000243 solution Substances 0.000 description 21
- 239000010936 titanium Substances 0.000 description 12
- 229910052719 titanium Inorganic materials 0.000 description 10
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 9
- 239000007864 aqueous solution Substances 0.000 description 9
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
- 238000000975 co-precipitation Methods 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 6
- OERNJTNJEZOPIA-UHFFFAOYSA-N zirconium nitrate Chemical compound [Zr+4].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O OERNJTNJEZOPIA-UHFFFAOYSA-N 0.000 description 6
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 5
- HTUMBQDCCIXGCV-UHFFFAOYSA-N lead oxide Chemical compound [O-2].[Pb+2] HTUMBQDCCIXGCV-UHFFFAOYSA-N 0.000 description 5
- YEXPOXQUZXUXJW-UHFFFAOYSA-N lead(II) oxide Inorganic materials [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 5
- 229910017604 nitric acid Inorganic materials 0.000 description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 3
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- 230000007547 defect Effects 0.000 description 3
- 229910052746 lanthanum Inorganic materials 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 229910052726 zirconium Inorganic materials 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 150000004679 hydroxides Chemical class 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- 239000006082 mold release agent Substances 0.000 description 2
- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 description 2
- DCKVFVYPWDKYDN-UHFFFAOYSA-L oxygen(2-);titanium(4+);sulfate Chemical compound [O-2].[Ti+4].[O-]S([O-])(=O)=O DCKVFVYPWDKYDN-UHFFFAOYSA-L 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000011163 secondary particle Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000006104 solid solution Substances 0.000 description 2
- 229910000348 titanium sulfate Inorganic materials 0.000 description 2
- IVORCBKUUYGUOL-UHFFFAOYSA-N 1-ethynyl-2,4-dimethoxybenzene Chemical compound COC1=CC=C(C#C)C(OC)=C1 IVORCBKUUYGUOL-UHFFFAOYSA-N 0.000 description 1
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
- 150000001242 acetic acid derivatives Chemical class 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 235000012501 ammonium carbonate Nutrition 0.000 description 1
- 239000001099 ammonium carbonate Substances 0.000 description 1
- VBIXEXWLHSRNKB-UHFFFAOYSA-N ammonium oxalate Chemical compound [NH4+].[NH4+].[O-]C(=O)C([O-])=O VBIXEXWLHSRNKB-UHFFFAOYSA-N 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- -1 chlorine ions Chemical class 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 150000004675 formic acid derivatives Chemical class 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- MRELNEQAGSRDBK-UHFFFAOYSA-N lanthanum oxide Inorganic materials [O-2].[O-2].[O-2].[La+3].[La+3] MRELNEQAGSRDBK-UHFFFAOYSA-N 0.000 description 1
- 229910000464 lead oxide Inorganic materials 0.000 description 1
- 239000008204 material by function Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- 230000005693 optoelectronics Effects 0.000 description 1
- 150000003891 oxalate salts Chemical class 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- KTUFCUMIWABKDW-UHFFFAOYSA-N oxo(oxolanthaniooxy)lanthanum Chemical compound O=[La]O[La]=O KTUFCUMIWABKDW-UHFFFAOYSA-N 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- MCJGNVYPOGVAJF-UHFFFAOYSA-N quinolin-8-ol Chemical compound C1=CN=C2C(O)=CC=CC2=C1 MCJGNVYPOGVAJF-UHFFFAOYSA-N 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 238000002834 transmittance Methods 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
- Oxygen, Ozone, And Oxides In General (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60086142A JPS61247607A (ja) | 1985-04-22 | 1985-04-22 | ペロブスカイト構造を持つ化合物の原料粉末の調製方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP60086142A JPS61247607A (ja) | 1985-04-22 | 1985-04-22 | ペロブスカイト構造を持つ化合物の原料粉末の調製方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS61247607A true JPS61247607A (ja) | 1986-11-04 |
| JPH0159967B2 JPH0159967B2 (enrdf_load_stackoverflow) | 1989-12-20 |
Family
ID=13878474
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP60086142A Granted JPS61247607A (ja) | 1985-04-22 | 1985-04-22 | ペロブスカイト構造を持つ化合物の原料粉末の調製方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS61247607A (enrdf_load_stackoverflow) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63288963A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | （Ｐｂ，Ｂａ）（Ｚｒ，Ｔｉ）０↓３の製造方法 |
| JPS63288961A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | （Ｐｂ，Ｌａ）（Ｈｆ，Ｔｉ）０↓３の製造方法 |
| JPS63288962A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | （Ｐｂ，Ｓｒ）（Ｚｒ，Ｔｉ）０↓３の製造方法 |
| JPS63288958A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | Ｓｒ（Ｃｅ，Ｚｒ）０↓３系セラミックスの製造方法 |
| JPS63288960A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | （Ｐｂ，Ｂｉ）（Ｚｒ，Ｔｉ）０↓３の製造方法 |
| JPH01111725A (ja) * | 1987-10-26 | 1989-04-28 | Natl Inst For Res In Inorg Mater | 凝３成分系鉛ペロブスカイト固溶体粉末および凝３成分系鉛ペロブスカイトセラミックスの製造方法 |
| US5340607A (en) * | 1992-03-19 | 1994-08-23 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Vapor-deposition material for the production of high-refraction optical coatings |
| JP2006298746A (ja) * | 2005-03-22 | 2006-11-02 | Tdk Corp | 粉末の製造方法、その粉末及びその粉末を用いた積層セラミックコンデンサ |
-
1985
- 1985-04-22 JP JP60086142A patent/JPS61247607A/ja active Granted
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63288963A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | （Ｐｂ，Ｂａ）（Ｚｒ，Ｔｉ）０↓３の製造方法 |
| JPS63288961A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | （Ｐｂ，Ｌａ）（Ｈｆ，Ｔｉ）０↓３の製造方法 |
| JPS63288962A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | （Ｐｂ，Ｓｒ）（Ｚｒ，Ｔｉ）０↓３の製造方法 |
| JPS63288958A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | Ｓｒ（Ｃｅ，Ｚｒ）０↓３系セラミックスの製造方法 |
| JPS63288960A (ja) * | 1987-05-21 | 1988-11-25 | Nippon Denso Co Ltd | （Ｐｂ，Ｂｉ）（Ｚｒ，Ｔｉ）０↓３の製造方法 |
| JPH01111725A (ja) * | 1987-10-26 | 1989-04-28 | Natl Inst For Res In Inorg Mater | 凝３成分系鉛ペロブスカイト固溶体粉末および凝３成分系鉛ペロブスカイトセラミックスの製造方法 |
| US5340607A (en) * | 1992-03-19 | 1994-08-23 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Vapor-deposition material for the production of high-refraction optical coatings |
| JP2006298746A (ja) * | 2005-03-22 | 2006-11-02 | Tdk Corp | 粉末の製造方法、その粉末及びその粉末を用いた積層セラミックコンデンサ |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0159967B2 (enrdf_load_stackoverflow) | 1989-12-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |