JPS6121928B2 - - Google Patents
Info
- Publication number
- JPS6121928B2 JPS6121928B2 JP12730684A JP12730684A JPS6121928B2 JP S6121928 B2 JPS6121928 B2 JP S6121928B2 JP 12730684 A JP12730684 A JP 12730684A JP 12730684 A JP12730684 A JP 12730684A JP S6121928 B2 JPS6121928 B2 JP S6121928B2
- Authority
- JP
- Japan
- Prior art keywords
- diethylbenzene
- metacyclophane
- pdeb
- crystals
- mdeb
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- DSNHSQKRULAAEI-UHFFFAOYSA-N 1,4-Diethylbenzene Chemical compound CCC1=CC=C(CC)C=C1 DSNHSQKRULAAEI-UHFFFAOYSA-N 0.000 claims description 112
- 239000000203 mixture Substances 0.000 claims description 24
- 150000001875 compounds Chemical class 0.000 claims description 22
- 238000000034 method Methods 0.000 claims description 19
- KVNYFPKFSJIPBJ-UHFFFAOYSA-N 1,2-diethylbenzene Chemical compound CCC1=CC=CC=C1CC KVNYFPKFSJIPBJ-UHFFFAOYSA-N 0.000 description 32
- 239000013078 crystal Substances 0.000 description 25
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 15
- 239000000243 solution Substances 0.000 description 8
- AFZZYIJIWUTJFO-UHFFFAOYSA-N 1,3-diethylbenzene Chemical compound CCC1=CC=CC(CC)=C1 AFZZYIJIWUTJFO-UHFFFAOYSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 6
- 238000004817 gas chromatography Methods 0.000 description 6
- 230000009102 absorption Effects 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 4
- 150000005195 diethylbenzenes Chemical class 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 230000004580 weight loss Effects 0.000 description 3
- YNQLUTRBYVCPMQ-UHFFFAOYSA-N Ethylbenzene Chemical compound CCC1=CC=CC=C1 YNQLUTRBYVCPMQ-UHFFFAOYSA-N 0.000 description 2
- 238000004455 differential thermal analysis Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 230000029936 alkylation Effects 0.000 description 1
- 238000005804 alkylation reaction Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 150000001923 cyclic compounds Chemical class 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12730684A JPS6016941A (ja) | 1984-06-22 | 1984-06-22 | ｐ−ジエチルベンゼン含有混合物からのｐ−ジエチルベンゼンの分離法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP12730684A JPS6016941A (ja) | 1984-06-22 | 1984-06-22 | ｐ−ジエチルベンゼン含有混合物からのｐ−ジエチルベンゼンの分離法 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP5993076A Division JPS601285B2 (ja) | 1975-10-22 | 1976-05-26 | 包接化合物並びにその製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6016941A JPS6016941A (ja) | 1985-01-28 |
| JPS6121928B2 true JPS6121928B2 (enrdf_load_stackoverflow) | 1986-05-29 |
Family
ID=14956683
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP12730684A Granted JPS6016941A (ja) | 1984-06-22 | 1984-06-22 | ｐ−ジエチルベンゼン含有混合物からのｐ−ジエチルベンゼンの分離法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6016941A (enrdf_load_stackoverflow) |
-
1984
- 1984-06-22 JP JP12730684A patent/JPS6016941A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6016941A (ja) | 1985-01-28 |
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