JPS61191505A - 窒化ほう素の製造法 - Google Patents
窒化ほう素の製造法Info
- Publication number
- JPS61191505A JPS61191505A JP22248584A JP22248584A JPS61191505A JP S61191505 A JPS61191505 A JP S61191505A JP 22248584 A JP22248584 A JP 22248584A JP 22248584 A JP22248584 A JP 22248584A JP S61191505 A JPS61191505 A JP S61191505A
- Authority
- JP
- Japan
- Prior art keywords
- melamine
- boron nitride
- water
- boric acid
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052582 BN Inorganic materials 0.000 title claims description 14
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 title claims description 14
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 229920000877 Melamine resin Polymers 0.000 claims description 21
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 13
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 claims description 11
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 10
- 239000004327 boric acid Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 10
- 229910052810 boron oxide Inorganic materials 0.000 claims description 9
- 239000000203 mixture Substances 0.000 claims description 8
- 238000001354 calcination Methods 0.000 claims description 3
- 230000001590 oxidative effect Effects 0.000 claims description 3
- 239000000843 powder Substances 0.000 description 10
- 238000002441 X-ray diffraction Methods 0.000 description 9
- 239000002994 raw material Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 238000007796 conventional method Methods 0.000 description 3
- 230000018044 dehydration Effects 0.000 description 3
- 238000006297 dehydration reaction Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 238000002844 melting Methods 0.000 description 3
- 230000008018 melting Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 229910001873 dinitrogen Inorganic materials 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000004580 weight loss Effects 0.000 description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910021538 borax Inorganic materials 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000007872 degassing Methods 0.000 description 1
- QGBSISYHAICWAH-UHFFFAOYSA-N dicyandiamide Chemical compound NC(N)=NC#N QGBSISYHAICWAH-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000011812 mixed powder Substances 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000000859 sublimation Methods 0.000 description 1
- 230000008022 sublimation Effects 0.000 description 1
Landscapes
- Ceramic Products (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP22248584A JPS61191505A (ja) | 1984-10-23 | 1984-10-23 | 窒化ほう素の製造法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP22248584A JPS61191505A (ja) | 1984-10-23 | 1984-10-23 | 窒化ほう素の製造法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS61191505A true JPS61191505A (ja) | 1986-08-26 |
JPH0214282B2 JPH0214282B2 (enrdf_load_stackoverflow) | 1990-04-06 |
Family
ID=16783166
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP22248584A Granted JPS61191505A (ja) | 1984-10-23 | 1984-10-23 | 窒化ほう素の製造法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS61191505A (enrdf_load_stackoverflow) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61286207A (ja) * | 1985-06-08 | 1986-12-16 | Showa Denko Kk | 窒化ホウ素の製造法 |
JPH01278404A (ja) * | 1988-04-27 | 1989-11-08 | Union Carbide Corp | 窒化ホウ素の製造方法 |
JPH11322310A (ja) * | 1998-05-11 | 1999-11-24 | Sumitomo Electric Ind Ltd | 立方晶窒化ホウ素多結晶砥粒およびその製造方法 |
CN100368284C (zh) * | 2005-12-02 | 2008-02-13 | 中国科学院物理研究所 | 利用金属氧化物合成氮化物的方法 |
JP2010100448A (ja) * | 2008-10-21 | 2010-05-06 | Denki Kagaku Kogyo Kk | 六方晶窒化ホウ素の製造方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB874165A (en) * | 1957-12-11 | 1961-08-02 | Union Carbide Corp | Improvements in the preparation of boron nitride |
US3241918A (en) * | 1962-05-09 | 1966-03-22 | Union Carbide Corp | Method for preparing boron nitride |
JPS60151202A (ja) * | 1983-08-25 | 1985-08-09 | Yuka Meramin Kk | 窒化ホウ素の製造方法 |
-
1984
- 1984-10-23 JP JP22248584A patent/JPS61191505A/ja active Granted
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB874165A (en) * | 1957-12-11 | 1961-08-02 | Union Carbide Corp | Improvements in the preparation of boron nitride |
US3241918A (en) * | 1962-05-09 | 1966-03-22 | Union Carbide Corp | Method for preparing boron nitride |
JPS60151202A (ja) * | 1983-08-25 | 1985-08-09 | Yuka Meramin Kk | 窒化ホウ素の製造方法 |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61286207A (ja) * | 1985-06-08 | 1986-12-16 | Showa Denko Kk | 窒化ホウ素の製造法 |
JPH01278404A (ja) * | 1988-04-27 | 1989-11-08 | Union Carbide Corp | 窒化ホウ素の製造方法 |
JPH11322310A (ja) * | 1998-05-11 | 1999-11-24 | Sumitomo Electric Ind Ltd | 立方晶窒化ホウ素多結晶砥粒およびその製造方法 |
CN100368284C (zh) * | 2005-12-02 | 2008-02-13 | 中国科学院物理研究所 | 利用金属氧化物合成氮化物的方法 |
JP2010100448A (ja) * | 2008-10-21 | 2010-05-06 | Denki Kagaku Kogyo Kk | 六方晶窒化ホウ素の製造方法 |
Also Published As
Publication number | Publication date |
---|---|
JPH0214282B2 (enrdf_load_stackoverflow) | 1990-04-06 |
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