JPS6114134A - 四塩化チタンの精製法 - Google Patents
四塩化チタンの精製法Info
- Publication number
- JPS6114134A JPS6114134A JP59136036A JP13603684A JPS6114134A JP S6114134 A JPS6114134 A JP S6114134A JP 59136036 A JP59136036 A JP 59136036A JP 13603684 A JP13603684 A JP 13603684A JP S6114134 A JPS6114134 A JP S6114134A
- Authority
- JP
- Japan
- Prior art keywords
- titanium tetrachloride
- ticl4
- oxychlorides
- vapor
- oxygen content
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 title claims description 13
- 239000012535 impurity Substances 0.000 claims abstract description 12
- 229910052751 metal Inorganic materials 0.000 claims abstract description 12
- 239000002184 metal Substances 0.000 claims abstract description 12
- 239000003054 catalyst Substances 0.000 claims abstract description 11
- 238000000354 decomposition reaction Methods 0.000 claims abstract description 7
- RCJVRSBWZCNNQT-UHFFFAOYSA-N dichloridooxygen Chemical compound ClOCl RCJVRSBWZCNNQT-UHFFFAOYSA-N 0.000 claims description 5
- 239000000126 substance Substances 0.000 claims description 3
- 229910052760 oxygen Inorganic materials 0.000 abstract description 14
- 239000001301 oxygen Substances 0.000 abstract description 14
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract description 13
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract description 6
- 238000001816 cooling Methods 0.000 abstract description 3
- 239000011889 copper foil Substances 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
- 229910003074 TiCl4 Inorganic materials 0.000 abstract 4
- 229910010270 TiOCl2 Inorganic materials 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 9
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 8
- 239000007789 gas Substances 0.000 description 7
- 239000010936 titanium Substances 0.000 description 7
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 229910052719 titanium Inorganic materials 0.000 description 5
- 229910052742 iron Inorganic materials 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000006722 reduction reaction Methods 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- 241000272201 Columbiformes Species 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 101100497923 Viola odorata Voc1 gene Proteins 0.000 description 2
- 229910052786 argon Inorganic materials 0.000 description 2
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 229910052802 copper Inorganic materials 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 229910000975 Carbon steel Inorganic materials 0.000 description 1
- 101100481404 Danio rerio tie1 gene Proteins 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 101100481406 Mus musculus Tie1 gene Proteins 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000010962 carbon steel Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- YDZQQRWRVYGNER-UHFFFAOYSA-N iron;titanium;trihydrate Chemical compound O.O.O.[Ti].[Fe] YDZQQRWRVYGNER-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 150000002680 magnesium Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 238000011946 reduction process Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000001577 simple distillation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/022—Titanium tetrachloride
- C01G23/024—Purification of tetrachloride
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59136036A JPS6114134A (ja) | 1984-06-30 | 1984-06-30 | 四塩化チタンの精製法 |
| AU43620/85A AU580067B2 (en) | 1984-06-30 | 1985-06-12 | Method of purificating titanium tetrachloride |
| CA000483987A CA1257069A (en) | 1984-06-30 | 1985-06-14 | Method of purificating titanium tetrachloride |
| EP85850208A EP0170640B1 (en) | 1984-06-30 | 1985-06-18 | Method of purificating titanium tetrachloride |
| DE8585850208T DE3576947D1 (de) | 1984-06-30 | 1985-06-18 | Verfahren zum reinigen von titantetrachlorid. |
| BR8503040A BR8503040A (pt) | 1984-06-30 | 1985-06-25 | Processo de purificacao de tetracloreto de titanio |
| US07/048,491 US4762696A (en) | 1984-06-30 | 1987-05-07 | Method of purificating titanium tetrachloride |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59136036A JPS6114134A (ja) | 1984-06-30 | 1984-06-30 | 四塩化チタンの精製法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6114134A true JPS6114134A (ja) | 1986-01-22 |
| JPH0583488B2 JPH0583488B2 (cg-RX-API-DMAC7.html) | 1993-11-26 |
Family
ID=15165677
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59136036A Granted JPS6114134A (ja) | 1984-06-30 | 1984-06-30 | 四塩化チタンの精製法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4762696A (cg-RX-API-DMAC7.html) |
| EP (1) | EP0170640B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JPS6114134A (cg-RX-API-DMAC7.html) |
| AU (1) | AU580067B2 (cg-RX-API-DMAC7.html) |
| BR (1) | BR8503040A (cg-RX-API-DMAC7.html) |
| CA (1) | CA1257069A (cg-RX-API-DMAC7.html) |
| DE (1) | DE3576947D1 (cg-RX-API-DMAC7.html) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2194782C1 (ru) * | 2001-05-14 | 2002-12-20 | ООО Научно-производственная экологическая фирма "ЭКО-технология" | Способ комплексной переработки и обезвреживания полиметаллических отходов производства |
| FR2836142A1 (fr) * | 2002-02-15 | 2003-08-22 | Rhodia Chimie Sa | Procede de preparation d'une composition liquide d'un compose diphenolique de haute purete et composition obtenue |
| US20060228292A1 (en) * | 2005-04-11 | 2006-10-12 | Cronin James T | Process for purifying titanium chloride-containing feedstock |
| WO2012116118A1 (en) | 2011-02-23 | 2012-08-30 | E. I. Du Pont De Nemours And Company | PURIFICATION OF TiCl4 THROUGH THE PRODUCTION OF NEW CO-PRODUCTS |
| CN112142106B (zh) * | 2020-09-29 | 2022-05-24 | 攀钢集团研究院有限公司 | 从三氯氧钒粗品中分离四氯化钛的方法 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2530735A (en) * | 1946-04-12 | 1950-11-21 | Du Pont | Purification of titanium halides |
| FR1097736A (fr) * | 1954-03-18 | 1955-07-08 | Perfectionnements apportés aux procédés de purification des tétrachlorures de titane et de silicium | |
| FR1133956A (fr) * | 1954-06-18 | 1957-04-04 | Laporte Titanium Ltd | Procédé de purification de tétrahalogénures de titane ou de tétrahalogénures de zirconium |
| US2958574A (en) * | 1955-12-02 | 1960-11-01 | Nat Distillers Chem Corp | Purification of titanium tetrachloride |
| US2871094A (en) * | 1956-01-26 | 1959-01-27 | Titanium Metals Corp | Purification of titanium tetrachloride with copper |
| US3102785A (en) * | 1956-09-21 | 1963-09-03 | Laporte Titanium Ltd | Process for the purification of titanium tetrachloride |
| FR1207631A (fr) * | 1957-07-23 | 1960-02-17 | Columbia Southern Chem Corp | Procédé de purification des halogénures métalliques, notamment du tétrachlorure de titane |
| US3533733A (en) * | 1968-05-09 | 1970-10-13 | Du Pont | Purifying crude ticl4 vapor |
| DE2135250C3 (de) * | 1971-07-14 | 1975-05-22 | Witalij Grigor'ewitsch Bruds' | Verfahren zur Reinigung von technischem Titantetrachlorid von den dieses begleitenden Beimengungen |
| US3729540A (en) * | 1971-07-28 | 1973-04-24 | V Brudz | Purification of titanium tetrachloride from concomitant impurities |
| GB1360587A (en) * | 1971-12-27 | 1974-07-17 | Sir Soc Italiana Resine Spa | Process for the purification of titanium tetrachloride |
| DE2218361A1 (de) * | 1972-04-15 | 1973-10-31 | Bayer Ag | Verfahren zur kontinuierlichen reinigung von titantetrachlorid |
| US3989510A (en) * | 1973-04-20 | 1976-11-02 | Othmer Donald F | Manufacture of titanium chloride and metallic iron from titaniferous materials containing iron oxides |
| GB1481120A (en) * | 1975-07-04 | 1977-07-27 | Laporte Industries Ltd | Recovery of titanium tetrachloride |
| US4070252A (en) * | 1977-04-18 | 1978-01-24 | Scm Corporation | Purification of crude titanium tetrachloride |
| US4244935A (en) * | 1978-04-20 | 1981-01-13 | Aluminum Company Of America | Method of forming metal chlorides |
| US4202866A (en) * | 1978-05-24 | 1980-05-13 | Stauffer Chemical Company | Production of stable vanadium tetrachloride |
| US4279871A (en) * | 1979-10-31 | 1981-07-21 | Scm Corporation | Process for treating chlorinated titaniferous material to remove vanadium |
| US4329322A (en) * | 1979-11-19 | 1982-05-11 | Scm Corporation | Chlorination of titaniferous material using treated coal for vanadium removal |
-
1984
- 1984-06-30 JP JP59136036A patent/JPS6114134A/ja active Granted
-
1985
- 1985-06-12 AU AU43620/85A patent/AU580067B2/en not_active Ceased
- 1985-06-14 CA CA000483987A patent/CA1257069A/en not_active Expired
- 1985-06-18 EP EP85850208A patent/EP0170640B1/en not_active Expired
- 1985-06-18 DE DE8585850208T patent/DE3576947D1/de not_active Expired - Lifetime
- 1985-06-25 BR BR8503040A patent/BR8503040A/pt not_active IP Right Cessation
-
1987
- 1987-05-07 US US07/048,491 patent/US4762696A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0583488B2 (cg-RX-API-DMAC7.html) | 1993-11-26 |
| EP0170640B1 (en) | 1990-04-04 |
| AU580067B2 (en) | 1988-12-22 |
| US4762696A (en) | 1988-08-09 |
| DE3576947D1 (de) | 1990-05-10 |
| AU4362085A (en) | 1986-01-02 |
| EP0170640A3 (en) | 1987-08-05 |
| BR8503040A (pt) | 1986-03-11 |
| EP0170640A2 (en) | 1986-02-05 |
| CA1257069A (en) | 1989-07-11 |
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