JPS6097936A - 高純度アルキルグリオキシレートの製造法 - Google Patents

高純度アルキルグリオキシレートの製造法

Info

Publication number
JPS6097936A
JPS6097936A JP59208461A JP20846184A JPS6097936A JP S6097936 A JPS6097936 A JP S6097936A JP 59208461 A JP59208461 A JP 59208461A JP 20846184 A JP20846184 A JP 20846184A JP S6097936 A JPS6097936 A JP S6097936A
Authority
JP
Japan
Prior art keywords
alkyl
glyoxylate
glycolate
alcohol
torr
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP59208461A
Other languages
English (en)
Japanese (ja)
Other versions
JPH0528694B2 (enExample
Inventor
デビツド　レイ　ダイロフ
ユエテイング　チヨウ
ダリオ　リカルド　コバ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Monsanto Co
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Publication of JPS6097936A publication Critical patent/JPS6097936A/ja
Publication of JPH0528694B2 publication Critical patent/JPH0528694B2/ja
Granted legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10—Vacuum distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP59208461A 1983-10-06 1984-10-05 高純度アルキルグリオキシレートの製造法 Granted JPS6097936A (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US539506 1983-10-06
US06/539,506 US4502923A (en) 1983-10-06 1983-10-06 Production of high purity alkyl glyoxylate by plural stage distillation

Publications (2)

Publication Number Publication Date
JPS6097936A true JPS6097936A (ja) 1985-05-31
JPH0528694B2 JPH0528694B2 (enExample) 1993-04-27

Family

ID=24151510

Family Applications (1)

Application Number Title Priority Date Filing Date
JP59208461A Granted JPS6097936A (ja) 1983-10-06 1984-10-05 高純度アルキルグリオキシレートの製造法

Country Status (6)

Country Link
US (1) US4502923A (enExample)
EP (1) EP0140866B1 (enExample)
JP (1) JPS6097936A (enExample)
AT (1) ATE27697T1 (enExample)
CA (1) CA1195285A (enExample)
DE (1) DE3464133D1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0273040A (ja) * 1988-07-25 1990-03-13 Monsanto Co グリオキシル酸アルキルの回収方法

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3602274A1 (de) * 1986-01-25 1987-07-30 Hoechst Ag Halbacetale von glyoxylsaeureestern sowie verfahren zur isolierung von glyoxylsaeureestern
US4820385A (en) * 1988-02-18 1989-04-11 Monsanto Company Purification of alkyl glyoxylate in a continuous column by azeotropic distillation
US4952291A (en) * 1989-12-06 1990-08-28 E. I. Du Pont De Nemours And Company Process for the purification of aldehydes
US5217582A (en) * 1990-06-20 1993-06-08 E. I. Du Pont De Nemours And Company Process for the isolation of alkyl glyoxylate
JP3150909B2 (ja) * 1996-09-05 2001-03-26 株式会社日本触媒 グリオキシル酸エステル類の精製方法
US9114328B2 (en) 2012-05-16 2015-08-25 Eastman Chemical Company Reactive distillation of a carboxylic acid and a glycol
US9040748B2 (en) 2012-06-08 2015-05-26 Eastman Chemical Company Hydrocarboxylation of aqueous formaldehyde using a dehydrating recycle stream to decrease water concentration
US10653904B2 (en) 2017-12-02 2020-05-19 M-Fire Holdings, Llc Methods of suppressing wild fires raging across regions of land in the direction of prevailing winds by forming anti-fire (AF) chemical fire-breaking systems using environmentally clean anti-fire (AF) liquid spray applied using GPS-tracking techniques
US11865390B2 (en) 2017-12-03 2024-01-09 Mighty Fire Breaker Llc Environmentally-clean water-based fire inhibiting biochemical compositions, and methods of and apparatus for applying the same to protect property against wildfire
US20240157180A1 (en) 2021-02-04 2024-05-16 Mighty Fire Breaker Llc Method of and kit for installing and operating a wildfire defense spraying system on a property parcel for proactively spraying environmentally-clean liquid fire inhibitor thereover to inhibit fire ignition and flame spread caused by wind-driven wildfire embers
US11826592B2 (en) 2018-01-09 2023-11-28 Mighty Fire Breaker Llc Process of forming strategic chemical-type wildfire breaks on ground surfaces to proactively prevent fire ignition and flame spread, and reduce the production of smoke in the presence of a wild fire

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1614195A (en) * 1923-03-05 1927-01-11 Firm Of C H Boehringer & Sohn Process for the manufacture of esters of oxy-acids
FR1575909A (enExample) * 1968-06-12 1969-07-25
DE2232352B2 (de) * 1972-07-01 1976-12-23 Basf Ag, 6700 Ludwigshafen Verfahren zur gewinnung von glyoxylsaeure bzw. ihres natriumsalzes
IT1027410B (it) * 1974-02-25 1978-11-20 Degussa Procedimento continuc per la produzione di glicide
DE2904775C2 (de) * 1979-02-08 1985-03-21 Hoechst Ag, 6230 Frankfurt Verfahren zur Herstellung von Glyoxylsäureestern
JPS58153575A (ja) * 1982-03-04 1983-09-12 Daicel Chem Ind Ltd 塩化水素の除去方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0273040A (ja) * 1988-07-25 1990-03-13 Monsanto Co グリオキシル酸アルキルの回収方法

Also Published As

Publication number Publication date
DE3464133D1 (en) 1987-07-16
US4502923A (en) 1985-03-05
CA1195285A (en) 1985-10-15
EP0140866B1 (en) 1987-06-10
EP0140866A1 (en) 1985-05-08
ATE27697T1 (de) 1987-06-15
JPH0528694B2 (enExample) 1993-04-27

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