ATE27697T1 - Herstellung von alkylglyoxylaten grosser reinheit. - Google Patents

Herstellung von alkylglyoxylaten grosser reinheit.

Info

Publication number
ATE27697T1
ATE27697T1 AT84870142T AT84870142T ATE27697T1 AT E27697 T1 ATE27697 T1 AT E27697T1 AT 84870142 T AT84870142 T AT 84870142T AT 84870142 T AT84870142 T AT 84870142T AT E27697 T1 ATE27697 T1 AT E27697T1
Authority
AT
Austria
Prior art keywords
high purity
alkyl
production
glyoxylate
alkyl glyoxylates
Prior art date
Application number
AT84870142T
Other languages
English (en)
Inventor
David Ray Dyroff
Yueting Chou
Dario Ricardo Cova
Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Monsanto Co filed Critical Monsanto Co
Application granted granted Critical
Publication of ATE27697T1 publication Critical patent/ATE27697T1/de

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10—Vacuum distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
AT84870142T 1983-10-06 1984-10-05 Herstellung von alkylglyoxylaten grosser reinheit. ATE27697T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US06/539,506 US4502923A (en) 1983-10-06 1983-10-06 Production of high purity alkyl glyoxylate by plural stage distillation
EP84870142A EP0140866B1 (de) 1983-10-06 1984-10-05 Herstellung von Alkylglyoxylaten grosser Reinheit

Publications (1)

Publication Number Publication Date
ATE27697T1 true ATE27697T1 (de) 1987-06-15

Family

ID=24151510

Family Applications (1)

Application Number Title Priority Date Filing Date
AT84870142T ATE27697T1 (de) 1983-10-06 1984-10-05 Herstellung von alkylglyoxylaten grosser reinheit.

Country Status (6)

Country Link
US (1) US4502923A (de)
EP (1) EP0140866B1 (de)
JP (1) JPS6097936A (de)
AT (1) ATE27697T1 (de)
CA (1) CA1195285A (de)
DE (1) DE3464133D1 (de)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3602274A1 (de) * 1986-01-25 1987-07-30 Hoechst Ag Halbacetale von glyoxylsaeureestern sowie verfahren zur isolierung von glyoxylsaeureestern
US4820385A (en) * 1988-02-18 1989-04-11 Monsanto Company Purification of alkyl glyoxylate in a continuous column by azeotropic distillation
US4867849A (en) * 1988-07-25 1989-09-19 Cova Dario R Purification of alkyl glyoxylate
US4952291A (en) * 1989-12-06 1990-08-28 E. I. Du Pont De Nemours And Company Process for the purification of aldehydes
US5217582A (en) * 1990-06-20 1993-06-08 E. I. Du Pont De Nemours And Company Process for the isolation of alkyl glyoxylate
JP3150909B2 (ja) * 1996-09-05 2001-03-26 株式会社日本触媒 グリオキシル酸エステル類の精製方法
US9114328B2 (en) 2012-05-16 2015-08-25 Eastman Chemical Company Reactive distillation of a carboxylic acid and a glycol
US9040748B2 (en) 2012-06-08 2015-05-26 Eastman Chemical Company Hydrocarboxylation of aqueous formaldehyde using a dehydrating recycle stream to decrease water concentration

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1614195A (en) * 1923-03-05 1927-01-11 Firm Of C H Boehringer & Sohn Process for the manufacture of esters of oxy-acids
FR1575909A (de) * 1968-06-12 1969-07-25
DE2232352B2 (de) * 1972-07-01 1976-12-23 Basf Ag, 6700 Ludwigshafen Verfahren zur gewinnung von glyoxylsaeure bzw. ihres natriumsalzes
IT1027410B (it) * 1974-02-25 1978-11-20 Degussa Procedimento continuc per la produzione di glicide
DE2904775C2 (de) * 1979-02-08 1985-03-21 Hoechst Ag, 6230 Frankfurt Verfahren zur Herstellung von Glyoxylsäureestern
JPS58153575A (ja) * 1982-03-04 1983-09-12 Daicel Chem Ind Ltd 塩化水素の除去方法

Also Published As

Publication number Publication date
JPH0528694B2 (de) 1993-04-27
CA1195285A (en) 1985-10-15
EP0140866A1 (de) 1985-05-08
EP0140866B1 (de) 1987-06-10
DE3464133D1 (en) 1987-07-16
JPS6097936A (ja) 1985-05-31
US4502923A (en) 1985-03-05

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Legal Events

Date Code Title Description
UEP Publication of translation of european patent specification
REN Ceased due to non-payment of the annual fee