JPS60112691A - Substrate supporting device for molecular beam epitaxial growth device - Google Patents
Substrate supporting device for molecular beam epitaxial growth deviceInfo
- Publication number
- JPS60112691A JPS60112691A JP21716883A JP21716883A JPS60112691A JP S60112691 A JPS60112691 A JP S60112691A JP 21716883 A JP21716883 A JP 21716883A JP 21716883 A JP21716883 A JP 21716883A JP S60112691 A JPS60112691 A JP S60112691A
- Authority
- JP
- Japan
- Prior art keywords
- substrate
- heating
- ring
- molecular beam
- epitaxial growth
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B23/00—Single-crystal growth by condensing evaporated or sublimed materials
- C30B23/02—Epitaxial-layer growth
- C30B23/06—Heating of the deposition chamber, the substrate or the materials to be evaporated
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Physical Deposition Of Substances That Are Components Of Semiconductor Devices (AREA)
Abstract
Description
【発明の詳細な説明】
この発明は分子線エピタキンヤル成長装置における化合
物半導体基板の保持装置に関する。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a holding device for a compound semiconductor substrate in a molecular beam epitaxy growth apparatus.
従来この基板の保持は専ら、インジウム、ガリウム等の
低融点金属を基板と基板保持台の間に敷いて熱を加え9
両者を接着する低融点金属接着法か、基板保持台上に基
板を載せ、その縁端部の数ケ所で金属の小片を便ってこ
れを圧接固定する金属小片固足法が採用されて来たが、
これらの方法には次の欠点がある。即ち、低融点金属接
着法では大面積の基板の裏面に均一に低融点金属を敷き
気泡を完全に々くしてむらのない接着を行なうことは困
難であって、このため接着部が不純物ガスの発生源と々
り易く、また接着剤の熱伝導度が高L
いため、気泡等現在の接着の不均一は熱伝導性にむらを
生じ、基板温度の面内分布の均一性が確保され々いうら
みがある。また接着に要する時間が長いため、その間の
基板表面の汚染が大きいという欠点がある。Conventionally, this method of holding the substrate was carried out exclusively by placing a low-melting point metal such as indium or gallium between the substrate and the substrate holder and applying heat.
The low melting point metal adhesion method, in which the two are bonded together, or the metal piece fixation method, in which the board is placed on a board holder and small pieces of metal are pressed and fixed at several points on the edges, has been adopted. However,
These methods have the following drawbacks. In other words, with the low melting point metal bonding method, it is difficult to uniformly spread the low melting point metal on the back surface of a large substrate, completely eliminate air bubbles, and achieve even bonding. Since the source of the adhesive is easily damaged, and the thermal conductivity of the adhesive is high, current non-uniform adhesive bonding such as air bubbles causes uneven thermal conductivity, making it difficult to ensure a uniform in-plane substrate temperature distribution. I'm jealous. Furthermore, since the time required for adhesion is long, there is a drawback that the surface of the substrate is heavily contaminated during that time.
1yにエピタキシャル成長完了後の基板を半導体デバイ
ス製造プロセスに投入使用するためには。In order to use the substrate after epitaxial growth is completed in 1y in a semiconductor device manufacturing process.
基板表面の低融点金属を完全に除去する必姿がおるが、
この除去作業では低融点金稿は酸で除去するため、成長
膜表面がこの金属で汚染する欠点がある。Although it is necessary to completely remove the low melting point metal on the substrate surface,
In this removal process, the low melting point metal is removed with acid, which has the disadvantage that the surface of the grown film is contaminated with this metal.
更Kまた。エピタキシャル膜成長中等に基板温度が例え
ば750°Cを越えるとインジウムでは蒸発が起り、こ
の金属が基板中に不純物として敗り一方、金属小片固定
法では、基板の縁端部の数ケ所を高熱伝導性の金属小片
で圧接固定するものであるため、圧接固定部分の近傍に
て著るしい基板温度の不均一を生ずる。また1機械的に
圧接同定しているため、熱膨張・収縮の際基板にストレ
スが加わり、基板上の成長膜に欠陥が入るという不都合
も生じている。Sara K again. When the substrate temperature exceeds, for example, 750°C during epitaxial film growth, indium evaporates and this metal is lost as an impurity in the substrate.On the other hand, with the metal piece fixing method, several places on the edge of the substrate are made to have high thermal conductivity. Since the substrate is fixed by pressure contact with a small piece of metal, significant non-uniformity in substrate temperature occurs near the pressure and fixation part. In addition, since mechanical pressure bonding is used, stress is applied to the substrate during thermal expansion and contraction, causing defects in the grown film on the substrate.
不発明け、これら従来の欠点を持たがい基板保持装置の
提供を目的とする。本発明は従来よりもけるかに脱着の
4易な簡便で安価な基板保持装置の提供を目的とする。SUMMARY OF THE INVENTION It is an object of the present invention to provide a substrate holding device that overcomes these conventional drawbacks. An object of the present invention is to provide a simple and inexpensive substrate holding device that is much easier to attach and detach than conventional substrate holding devices.
更VCまた1本発明は、ガス抜きが容易で、冒温の処理
にもストレスを生ぜず。In addition, the present invention allows easy degassing and does not cause stress during high-temperature processing.
基板に温t#′不均一を生むことのない新規の基板保持
装置の提供全目的とする。It is an object of the present invention to provide a novel substrate holding device that does not cause temperature t#' non-uniformity on the substrate.
以下図を用い、実施例によって本発明を説明する。The present invention will be explained below by way of examples using the figures.
第1図社本発明の実施例であって1111’!1′はそ
れぞれ基板等落下防止用CIJング(C型止め輪)で、
高融点金属であるタングステンまたはモリブデ/を素材
とした線材で作られている。Figure 1 is an embodiment of the present invention and is 1111'! 1' is a CIJ ring (C-type retaining ring) for preventing the board from falling,
It is made of wire made from tungsten or molybdenum, which are high-melting point metals.
2はこれも高融点金属のモリブデン製の基板保持台、3
は円板状の加熱均一化部材で窩輻射率かつ高熱伝導度の
パイロリティックグラファイトを素材々する。5は基板
加熱用ヒーター、6は分子線り飛来方向である。2 is a substrate holding stand also made of molybdenum, a high melting point metal, 3
is a disc-shaped heating uniformity member made of pyrolytic graphite, which has high cavity emissivity and high thermal conductivity. 5 is a heater for heating the substrate, and 6 is the direction in which the molecular beam comes.
本発明で1l−j基板保持台2の上に円板状の加熱均一
化部材3を熱変化分以上の間隙を持たせて設置したのち
基板保持台2のClフグ溝10′ にCリング1′を挿
入してこれを係止し、更に同様にCリング1′をCリン
グ溝10′ に挿入したのち。In the present invention, after installing the disc-shaped heating uniformity member 3 on the 1l-j substrate holding table 2 with a gap equal to or larger than the thermal change, the C ring 1 is placed in the Cl blow groove 10' of the substrate holding table 2. ' and lock it, and then similarly insert C-ring 1' into C-ring groove 10'.
円板上基板4をやはり間隙をもたせて挿入し、更に、基
板保持台2の開孔部の内壁のCIJング溝10に基板落
下防止リング】をはめ込んでいる。The disk-top substrate 4 is also inserted with a gap, and a substrate fall prevention ring is fitted into the CIJ groove 10 on the inner wall of the opening of the substrate holder 2.
従って円板状基板4と加熱均一化部材30間には真空空
間30が設けられている。Therefore, a vacuum space 30 is provided between the disc-shaped substrate 4 and the heating uniformity member 30.
このとき基板4に、その面に垂直な方向についても遊隙
を与えられている。即ち2本発明の基板保持(L−’r
、板面に沿う方向ICついても、板面に唾直な方向l
(ついても、すべて若干の間隙を有して無圧力状態で行
われるものである。従って、基板は自重で自らの位1〃
を占め、高温に加熱してもストレスを生ず乙ことにかい
。基板4は真空空間30を経由する加熱l匂一部材3の
赤外線で加熱されるがこの加熱均一化部材3はパイロリ
ティクグラファイト製であってその冨輻射率かつ高熱伝
導度のために厚みをある桿げもたせることでその全面に
暇ってit ff均一な酩度を有することとなる。かく
て基板加熱ヒーター5の白熱部の形状は加熱均一部材3
で充分に拡散されるが、その部材3の表面から輻射され
る赤外線によってはじめて基板4の加熱が行われる。そ
のため、基板4ではその全面に亘って均一な温JW4+
布が確保される。温度分布の均一性の確保のためには、
基板4に接近する加熱均一化部材3の面は平滑で凹凸を
持た′ないのを理想とする。At this time, the substrate 4 is also given clearance in the direction perpendicular to its surface. That is, the substrate holding (L-'r) of the present invention is
, Even if the direction IC is along the board surface, the direction perpendicular to the board surface l
(However, all of this is done in a no-pressure state with a slight gap between them. Therefore, the board is able to lift itself by its own weight.)
It occupies a large area and does not cause stress even when heated to high temperatures. The substrate 4 is heated by the infrared rays of the heating element 3 passing through the vacuum space 30, and the heating uniformity member 3 is made of pyrolytic graphite and is thick due to its high emissivity and high thermal conductivity. By allowing the rod to stand up, the entire surface of the drink will be free and it will have a uniform level of intoxication. Thus, the shape of the incandescent part of the substrate heating heater 5 is the same as that of the heating uniform member 3.
However, the substrate 4 is heated only by the infrared rays radiated from the surface of the member 3. Therefore, the substrate 4 has a uniform temperature JW4+ over its entire surface.
Cloth is secured. To ensure uniformity of temperature distribution,
Ideally, the surface of the heating equalizing member 3 that approaches the substrate 4 is smooth and has no irregularities.
なお1本発明の加熱均一化部材は実施例のパイロリティ
クグラファイトヲ素材とするものに限定素材とすること
ができる。Note that the heating uniformity member of the present invention may be made of a limited material such as the pyrolytic graphite of the embodiment.
々おfた。保持部材の形状、←jq成1個数も実施例の
ものに限定されるものではなく、不発明の趣旨を尊重し
た応用変形が可能である。Thank you very much. The shape and number of the holding members are not limited to those in the embodiments, and may be modified while respecting the spirit of the invention.
本発明の基板保持装置・7tは上記の通りであるだめ。The substrate holding device 7t of the present invention is as described above.
品温の熱サイクルに対(7ても基板にストレス1に発生
せず、均−VC分布した基板温度を4易に確保できる。Even with a thermal cycle of product temperature (7), stress does not occur on the board, and a board temperature with an even -VC distribution can be easily ensured.
装置が簡単であるため半導体デバイス製遺プロセスでの
基板の増扱いが簡単になって自動化を可能にする利点も
あり、工業と頂めて有仝な発明ということができる。Since the apparatus is simple, it is easy to increase the number of substrates in the semiconductor device fabrication process, and there is also the advantage that automation is possible, so it can be said to be a valuable invention in industry.
4、第1図簡単な説明
第1図は本発明の実施例の基板保持装置の側断面図であ
る。第2図はその平面図である。4. FIG. 1 Brief Description FIG. 1 is a side sectional view of a substrate holding device according to an embodiment of the present invention. FIG. 2 is a plan view thereof.
1.1’、’:Cリング、IQ、 ](1’、 10’
:Cリング溝 2:基板保持台、 3:加熱均一化部材
。1.1', ': C ring, IQ, ](1', 10'
: C-ring groove 2: Substrate holding stand, 3: Heating uniformity member.
4:椛板、 5:基板加熱用ヒーター。4: Board plate, 5: Heater for heating the substrate.
Claims (2)
をその周辺で支持するとともに、該基板の裏面とそれを
加熱する基板加−熱用ヒーターとの間に高熱伝導度およ
び、あるいは高輻射率を有する耐熱性加熱均−化部利を
設備しかつ該基板の裏面と該加熱均−世部材の間には該
基板の加熱を均一化する真空空間を設けたことを特徴と
する分子線エピタキシャル成長装置用の基板保持装置。(1) Support the compound semiconductor substrate for molecular beam epitaxial growth around the substrate, and have high thermal conductivity and/or high emissivity between the back surface of the substrate and the substrate heating heater that heats it. For use in a molecular beam epitaxial growth apparatus, characterized in that a heat-resistant heating equalization member is provided and a vacuum space is provided between the back surface of the substrate and the heating equalization member to uniformize the heating of the substrate. substrate holding device.
イトで作られている第一項記載の分子線エピタキシャル
成長装置用の基板保持装置。(2) The substrate holding device for a molecular beam epitaxial growth apparatus according to item 1, wherein the heating uniformity member is made of pyrolytic graphite.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP21716883A JPS60112691A (en) | 1983-11-18 | 1983-11-18 | Substrate supporting device for molecular beam epitaxial growth device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP21716883A JPS60112691A (en) | 1983-11-18 | 1983-11-18 | Substrate supporting device for molecular beam epitaxial growth device |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS60112691A true JPS60112691A (en) | 1985-06-19 |
JPS636520B2 JPS636520B2 (en) | 1988-02-10 |
Family
ID=16699920
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP21716883A Granted JPS60112691A (en) | 1983-11-18 | 1983-11-18 | Substrate supporting device for molecular beam epitaxial growth device |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS60112691A (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61195042U (en) * | 1985-05-25 | 1986-12-04 | ||
JPS6244433U (en) * | 1985-09-06 | 1987-03-17 | ||
EP0227228A2 (en) * | 1985-12-19 | 1987-07-01 | Litton Systems, Inc. | Substrate holder for wafers during MBE growth |
US4777022A (en) * | 1984-08-28 | 1988-10-11 | Stephen I. Boldish | Epitaxial heater apparatus and process |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP4311051B2 (en) * | 2003-03-19 | 2009-08-12 | 東レ株式会社 | Hollow fiber membrane module manufacturing method and hollow fiber membrane module manufacturing apparatus used therefor |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5730320A (en) * | 1980-07-29 | 1982-02-18 | Fujitsu Ltd | Substrate holder for molecular beam epitaxy |
-
1983
- 1983-11-18 JP JP21716883A patent/JPS60112691A/en active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5730320A (en) * | 1980-07-29 | 1982-02-18 | Fujitsu Ltd | Substrate holder for molecular beam epitaxy |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4777022A (en) * | 1984-08-28 | 1988-10-11 | Stephen I. Boldish | Epitaxial heater apparatus and process |
JPS61195042U (en) * | 1985-05-25 | 1986-12-04 | ||
JPS6244433U (en) * | 1985-09-06 | 1987-03-17 | ||
JPH0325402Y2 (en) * | 1985-09-06 | 1991-06-03 | ||
EP0227228A2 (en) * | 1985-12-19 | 1987-07-01 | Litton Systems, Inc. | Substrate holder for wafers during MBE growth |
Also Published As
Publication number | Publication date |
---|---|
JPS636520B2 (en) | 1988-02-10 |
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