JPS60103033A - ジルコニア系超微粉末の製造方法 - Google Patents
ジルコニア系超微粉末の製造方法Info
- Publication number
- JPS60103033A JPS60103033A JP58203722A JP20372283A JPS60103033A JP S60103033 A JPS60103033 A JP S60103033A JP 58203722 A JP58203722 A JP 58203722A JP 20372283 A JP20372283 A JP 20372283A JP S60103033 A JPS60103033 A JP S60103033A
- Authority
- JP
- Japan
- Prior art keywords
- powder
- autoclave
- zirconium salt
- soln
- zirconia
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 26
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 9
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 16
- 150000003754 zirconium Chemical class 0.000 claims abstract description 10
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 8
- 229910052751 metal Inorganic materials 0.000 claims abstract description 5
- 239000002184 metal Substances 0.000 claims abstract description 5
- 150000003839 salts Chemical class 0.000 claims abstract description 5
- 229910017464 nitrogen compound Inorganic materials 0.000 claims abstract 4
- 150000002830 nitrogen compounds Chemical class 0.000 claims abstract 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 28
- 239000000243 solution Substances 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 2
- 229920006395 saturated elastomer Polymers 0.000 claims 1
- 239000002245 particle Substances 0.000 abstract description 7
- 238000006243 chemical reaction Methods 0.000 abstract description 5
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 abstract description 4
- 239000004202 carbamide Substances 0.000 abstract description 4
- 150000001875 compounds Chemical class 0.000 abstract description 3
- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 abstract description 3
- 229910052791 calcium Inorganic materials 0.000 abstract description 2
- XLJMAIOERFSOGZ-UHFFFAOYSA-M cyanate Chemical compound [O-]C#N XLJMAIOERFSOGZ-UHFFFAOYSA-M 0.000 abstract description 2
- 229910052749 magnesium Inorganic materials 0.000 abstract description 2
- 229910052727 yttrium Inorganic materials 0.000 abstract description 2
- 238000000354 decomposition reaction Methods 0.000 abstract 3
- 230000015271 coagulation Effects 0.000 abstract 1
- 238000005345 coagulation Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 description 7
- 239000002994 raw material Substances 0.000 description 4
- 230000002776 aggregation Effects 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000001354 calcination Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000010959 steel Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- OBOSXEWFRARQPU-UHFFFAOYSA-N 2-n,2-n-dimethylpyridine-2,5-diamine Chemical compound CN(C)C1=CC=C(N)C=N1 OBOSXEWFRARQPU-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 244000062793 Sorghum vulgare Species 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 239000010987 cubic zirconia Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000001493 electron microscopy Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 235000019713 millet Nutrition 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000011819 refractory material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000006104 solid solution Substances 0.000 description 1
- 230000002747 voluntary effect Effects 0.000 description 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Compositions Of Oxide Ceramics (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58203722A JPS60103033A (ja) | 1983-11-01 | 1983-11-01 | ジルコニア系超微粉末の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58203722A JPS60103033A (ja) | 1983-11-01 | 1983-11-01 | ジルコニア系超微粉末の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60103033A true JPS60103033A (ja) | 1985-06-07 |
| JPH0232216B2 JPH0232216B2 (enrdf_load_stackoverflow) | 1990-07-19 |
Family
ID=16478762
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58203722A Granted JPS60103033A (ja) | 1983-11-01 | 1983-11-01 | ジルコニア系超微粉末の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60103033A (enrdf_load_stackoverflow) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62260718A (ja) * | 1986-05-06 | 1987-11-13 | Shigeyuki Somiya | 水熱法による高純度ジルコニア−アルミナ系超微粉末の製造方法 |
| WO1994004459A1 (en) * | 1992-08-18 | 1994-03-03 | Worcester Polytechnic Institute | Preparation of nanophase solid state materials |
| US5466646A (en) * | 1992-08-18 | 1995-11-14 | Worcester Polytechnic Institute | Process for the preparation of solid state materials and said materials |
| US6899948B2 (en) | 1999-10-28 | 2005-05-31 | 3M Innovative Properties Company | Dental materials with nano-sized silica particles |
| US7393882B2 (en) | 2002-01-31 | 2008-07-01 | 3M Innovative Properties Company | Dental pastes, dental articles, and methods |
-
1983
- 1983-11-01 JP JP58203722A patent/JPS60103033A/ja active Granted
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62260718A (ja) * | 1986-05-06 | 1987-11-13 | Shigeyuki Somiya | 水熱法による高純度ジルコニア−アルミナ系超微粉末の製造方法 |
| DE3714911A1 (de) * | 1986-05-06 | 1987-11-19 | Soumiya Shigeyuki | Verfahren zum herstellen einer aufschlaemmung eines ultrafeinen pulvers auf zirkoniumoxid-aluminiumoxid-basis |
| DE3714911C2 (de) * | 1986-05-06 | 1994-08-25 | Soumiya Shigeyuki | Verfahren zum Herstellen einer Aufschlämmung eines ultrafeinen Pulvers auf Zirkoniumoxid-Aluminiumoxid-Basis |
| WO1994004459A1 (en) * | 1992-08-18 | 1994-03-03 | Worcester Polytechnic Institute | Preparation of nanophase solid state materials |
| US5417956A (en) * | 1992-08-18 | 1995-05-23 | Worcester Polytechnic Institute | Preparation of nanophase solid state materials |
| US5466646A (en) * | 1992-08-18 | 1995-11-14 | Worcester Polytechnic Institute | Process for the preparation of solid state materials and said materials |
| US6899948B2 (en) | 1999-10-28 | 2005-05-31 | 3M Innovative Properties Company | Dental materials with nano-sized silica particles |
| US7393882B2 (en) | 2002-01-31 | 2008-07-01 | 3M Innovative Properties Company | Dental pastes, dental articles, and methods |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0232216B2 (enrdf_load_stackoverflow) | 1990-07-19 |
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