JPS5920263A - １，１，１−アジドジニトロ化合物の製法 - Google Patents
１，１，１−アジドジニトロ化合物の製法Info
- Publication number
- JPS5920263A JPS5920263A JP58069286A JP6928683A JPS5920263A JP S5920263 A JPS5920263 A JP S5920263A JP 58069286 A JP58069286 A JP 58069286A JP 6928683 A JP6928683 A JP 6928683A JP S5920263 A JPS5920263 A JP S5920263A
- Authority
- JP
- Japan
- Prior art keywords
- compound
- item
- azidodinitro
- manufacturing
- method characterized
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001875 compounds Chemical class 0.000 title claims description 30
- 238000004519 manufacturing process Methods 0.000 title claims description 20
- 238000000034 method Methods 0.000 claims description 20
- 150000001335 aliphatic alkanes Chemical class 0.000 claims description 9
- GUWHRJQTTVADPB-UHFFFAOYSA-N lithium azide Chemical compound [Li+].[N-]=[N+]=[N-] GUWHRJQTTVADPB-UHFFFAOYSA-N 0.000 claims description 8
- -1 4-azidodinitrobutyrate Chemical group 0.000 claims description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 230000007935 neutral effect Effects 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 3
- 239000004202 carbamide Substances 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims 1
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 9
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 6
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- ZQXWPHXDXHONFS-UHFFFAOYSA-N 1-(2,2-dinitropropoxymethoxy)-2,2-dinitropropane Chemical compound [O-][N+](=O)C([N+]([O-])=O)(C)COCOCC(C)([N+]([O-])=O)[N+]([O-])=O ZQXWPHXDXHONFS-UHFFFAOYSA-N 0.000 description 2
- WSZPRLKJOJINEP-UHFFFAOYSA-N 1-fluoro-2-[(2-fluoro-2,2-dinitroethoxy)methoxy]-1,1-dinitroethane Chemical compound [O-][N+](=O)C(F)([N+]([O-])=O)COCOCC(F)([N+]([O-])=O)[N+]([O-])=O WSZPRLKJOJINEP-UHFFFAOYSA-N 0.000 description 2
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 2
- PXIPVTKHYLBLMZ-UHFFFAOYSA-N Sodium azide Chemical compound [Na+].[N-]=[N+]=[N-] PXIPVTKHYLBLMZ-UHFFFAOYSA-N 0.000 description 2
- 125000000217 alkyl group Chemical group 0.000 description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
- 235000013877 carbamide Nutrition 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000002360 explosive Substances 0.000 description 2
- 235000019256 formaldehyde Nutrition 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000001301 oxygen Substances 0.000 description 2
- 229910052760 oxygen Inorganic materials 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- 239000003380 propellant Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- ZDTITQCJOXMEBX-UHFFFAOYSA-N 1-azido-1,1-dinitroethane Chemical compound [O-][N+](=O)C([N+]([O-])=O)(C)N=[N+]=[N-] ZDTITQCJOXMEBX-UHFFFAOYSA-N 0.000 description 1
- 101100181929 Caenorhabditis elegans lin-3 gene Proteins 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- IVRMZWNICZWHMI-UHFFFAOYSA-N azide group Chemical group [N-]=[N+]=[N-] IVRMZWNICZWHMI-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000005457 ice water Substances 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 229910000473 manganese(VI) oxide Inorganic materials 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 150000003672 ureas Chemical class 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C247/00—Compounds containing azido groups
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B25/00—Compositions containing a nitrated organic compound
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US400783 | 1982-07-22 | ||
| US06/400,783 US4472311A (en) | 1982-07-22 | 1982-07-22 | Method of preparing 1,1,1-azidodinitro compounds |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5920263A true JPS5920263A (ja) | 1984-02-01 |
| JPH0379340B2 JPH0379340B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1991-12-18 |
Family
ID=23584989
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58069286A Granted JPS5920263A (ja) | 1982-07-22 | 1983-04-21 | １，１，１−アジドジニトロ化合物の製法 |
Country Status (4)
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4761250A (en) * | 1985-08-09 | 1988-08-02 | Rockwell International Corporation | Process for preparing 1,5-diazido-3-nitrazapentane |
| US4683085A (en) * | 1985-08-19 | 1987-07-28 | Rockwell International Corporation | Polyazido esters |
| US4797168A (en) * | 1986-08-11 | 1989-01-10 | Rockwell International Corporation | Azidodinitro propellants |
| US4900851A (en) * | 1987-08-05 | 1990-02-13 | The United States Of America As Represented By The Secretary Of The Air Force | Synthesis of azidodinitro compounds |
| US4795593A (en) * | 1987-08-05 | 1989-01-03 | The United States Of America As Represented By The Secretary Of The Air Force | 4-azido-4,4-dinitro-1-butanol and derivatives thereof |
| US8841468B2 (en) | 2010-06-23 | 2014-09-23 | Physical Sciences, Inc. | Synthesis of an azido energetic alcohol |
| CN103613512B (zh) * | 2013-11-04 | 2015-08-12 | 西安近代化学研究所 | 3-硝基-5-叠氮基-3-氮杂戊醇硝酸酯及其制备方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3157683A (en) * | 1958-11-26 | 1964-11-17 | Purdue Research Foundation | Beta-nu-nitro-nu-trinitroalkyl isocyanates and derivatives thereof |
| US3317595A (en) * | 1963-09-13 | 1967-05-02 | Kazimiera J L Paciorek | Linear substituted phosphonitrilic derivatives |
| US3883377A (en) * | 1968-11-27 | 1975-05-13 | Us Navy | 1-Azido-1,1-dinitroalkanes, useful as propellants |
-
1982
- 1982-07-22 US US06/400,783 patent/US4472311A/en not_active Expired - Fee Related
-
1983
- 1983-04-21 JP JP58069286A patent/JPS5920263A/ja active Granted
- 1983-07-08 DE DE19833324728 patent/DE3324728A1/de active Granted
- 1983-07-22 GB GB08319859A patent/GB2123829B/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| GB8319859D0 (en) | 1983-08-24 |
| DE3324728C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1992-11-12 |
| JPH0379340B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1991-12-18 |
| DE3324728A1 (de) | 1984-01-26 |
| GB2123829A (en) | 1984-02-08 |
| GB2123829B (en) | 1986-04-03 |
| US4472311A (en) | 1984-09-18 |
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