JPS5918108A - 改質フツ化黒鉛の製造法 - Google Patents
改質フツ化黒鉛の製造法Info
- Publication number
- JPS5918108A JPS5918108A JP58088947A JP8894783A JPS5918108A JP S5918108 A JPS5918108 A JP S5918108A JP 58088947 A JP58088947 A JP 58088947A JP 8894783 A JP8894783 A JP 8894783A JP S5918108 A JPS5918108 A JP S5918108A
- Authority
- JP
- Japan
- Prior art keywords
- modified
- discharge
- graphite fluoride
- fluorine
- graphite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 239000007864 aqueous solution Substances 0.000 claims abstract description 12
- 230000001678 irradiating effect Effects 0.000 claims abstract description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical class [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 29
- 238000004519 manufacturing process Methods 0.000 claims description 6
- QLOAVXSYZAJECW-UHFFFAOYSA-N methane;molecular fluorine Chemical class C.FF QLOAVXSYZAJECW-UHFFFAOYSA-N 0.000 abstract description 99
- 238000000354 decomposition reaction Methods 0.000 abstract description 43
- 239000000243 solution Substances 0.000 abstract description 7
- 239000002245 particle Substances 0.000 abstract description 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 208000028659 discharge Diseases 0.000 description 53
- 229910052731 fluorine Inorganic materials 0.000 description 45
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 42
- 239000011737 fluorine Substances 0.000 description 42
- 230000000052 comparative effect Effects 0.000 description 23
- 239000002612 dispersion medium Substances 0.000 description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 21
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 12
- 239000011149 active material Substances 0.000 description 9
- 239000000203 mixture Substances 0.000 description 8
- 229910002804 graphite Inorganic materials 0.000 description 7
- 239000010439 graphite Substances 0.000 description 7
- 229910021383 artificial graphite Inorganic materials 0.000 description 6
- 239000003575 carbonaceous material Substances 0.000 description 6
- 238000006243 chemical reaction Methods 0.000 description 5
- 239000003792 electrolyte Substances 0.000 description 5
- 238000003682 fluorination reaction Methods 0.000 description 5
- 239000010410 layer Substances 0.000 description 5
- 229910021382 natural graphite Inorganic materials 0.000 description 5
- 239000003921 oil Substances 0.000 description 5
- 239000011230 binding agent Substances 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- 239000006258 conductive agent Substances 0.000 description 4
- 239000013078 crystal Substances 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 238000012986 modification Methods 0.000 description 4
- 230000004048 modification Effects 0.000 description 4
- 239000002994 raw material Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- -1 for example Chemical compound 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 238000004448 titration Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- 239000002194 amorphous carbon material Substances 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 239000002180 crystalline carbon material Substances 0.000 description 2
- 125000001153 fluoro group Chemical group F* 0.000 description 2
- 230000004907 flux Effects 0.000 description 2
- 239000007770 graphite material Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011229 interlayer Substances 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- 239000008188 pellet Substances 0.000 description 2
- 239000002006 petroleum coke Substances 0.000 description 2
- 238000006552 photochemical reaction Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004094 surface-active agent Substances 0.000 description 2
- JKYKXTRKURYNGW-UHFFFAOYSA-N 3,4-dihydroxy-9,10-dioxo-9,10-dihydroanthracene-2-sulfonic acid Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C(O)=C(O)C(S(O)(=O)=O)=C2 JKYKXTRKURYNGW-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 241001474791 Proboscis Species 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 150000001342 alkaline earth metals Chemical class 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000002519 antifouling agent Substances 0.000 description 1
- 239000012298 atmosphere Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003631 expected effect Effects 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 239000012212 insulator Substances 0.000 description 1
- MHCFAGZWMAWTNR-UHFFFAOYSA-M lithium perchlorate Chemical group [Li+].[O-]Cl(=O)(=O)=O MHCFAGZWMAWTNR-UHFFFAOYSA-M 0.000 description 1
- 229910001486 lithium perchlorate Inorganic materials 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000002940 repellent Effects 0.000 description 1
- 239000005871 repellent Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 239000012086 standard solution Substances 0.000 description 1
- VGBPIHVLVSGJGR-UHFFFAOYSA-N thorium(4+);tetranitrate Chemical compound [Th+4].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O VGBPIHVLVSGJGR-UHFFFAOYSA-N 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Battery Electrode And Active Subsutance (AREA)
- Carbon And Carbon Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58088947A JPS5918108A (ja) | 1983-05-20 | 1983-05-20 | 改質フツ化黒鉛の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58088947A JPS5918108A (ja) | 1983-05-20 | 1983-05-20 | 改質フツ化黒鉛の製造法 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP57125370A Division JPS5918107A (ja) | 1982-07-19 | 1982-07-19 | 改質されたフッ化黒鉛からなる固体潤滑剤 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5918108A true JPS5918108A (ja) | 1984-01-30 |
| JPH0143682B2 JPH0143682B2 (enrdf_load_stackoverflow) | 1989-09-22 |
Family
ID=13957063
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58088947A Granted JPS5918108A (ja) | 1983-05-20 | 1983-05-20 | 改質フツ化黒鉛の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5918108A (enrdf_load_stackoverflow) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014141789A1 (ja) * | 2013-03-11 | 2014-09-18 | Jx日鉱日石金属株式会社 | 磁気記録膜形成用スパッタリングターゲット及び該ターゲットの製造に用いる炭素原料 |
| CN117585666A (zh) * | 2023-10-31 | 2024-02-23 | 山东重山光电材料股份有限公司 | 一种水热改性氟化石墨及其制备方法和应用 |
-
1983
- 1983-05-20 JP JP58088947A patent/JPS5918108A/ja active Granted
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014141789A1 (ja) * | 2013-03-11 | 2014-09-18 | Jx日鉱日石金属株式会社 | 磁気記録膜形成用スパッタリングターゲット及び該ターゲットの製造に用いる炭素原料 |
| JP5973056B2 (ja) * | 2013-03-11 | 2016-08-23 | Ｊｘ金属株式会社 | 磁気記録膜形成用スパッタリングターゲットの製造方法 |
| JP2016173871A (ja) * | 2013-03-11 | 2016-09-29 | Ｊｘ金属株式会社 | 磁気記録膜形成用スパッタリングターゲット及び該ターゲットの製造に用いる炭素原料 |
| CN117585666A (zh) * | 2023-10-31 | 2024-02-23 | 山东重山光电材料股份有限公司 | 一种水热改性氟化石墨及其制备方法和应用 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0143682B2 (enrdf_load_stackoverflow) | 1989-09-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Saroja et al. | Facile synthesis of heteroatom doped and undoped graphene quantum dots as active materials for reversible lithium and sodium ions storage | |
| JP7294334B2 (ja) | Ｌｇｐｓ系固体電解質および製造方法 | |
| US5168018A (en) | Method of manufacturing zinc-alkaline batteries | |
| NuLi et al. | Shape evolution of α-Fe2O3 and its size-dependent electrochemical properties for lithium-ion batteries | |
| JPS5918107A (ja) | 改質されたフッ化黒鉛からなる固体潤滑剤 | |
| JPWO2016047491A1 (ja) | 二次電池用正極活物質及びその製造方法 | |
| JPS61295238A (ja) | 非水性二次電池 | |
| JPS62290060A (ja) | 電圧遅延のないリチウム／弗素化炭素電池 | |
| US20240145768A1 (en) | Solid electrolyte, and electrode mixture and battery containing the same | |
| US4737423A (en) | Cathode active material for metal of CFX battery | |
| JP2017157414A (ja) | ポリアニオン正極活物質及びその製造方法 | |
| JPS5918108A (ja) | 改質フツ化黒鉛の製造法 | |
| Purwamargapratala et al. | Synthesis of Li4Ti5O12 (LTO) by sol-gel method for lithium ion battery anode | |
| CN112573503B (zh) | 氮掺杂多孔碳材料的制备方法、制得的多孔碳材料及其应用 | |
| JP3086029B2 (ja) | 電池用のアルカリ電解質 | |
| JPS5916273A (ja) | 改質フッ化黒鉛を用いた水溶液系一次電池 | |
| JPH06342655A (ja) | 電極及びこれを備えている電池 | |
| JPS5846453B2 (ja) | 過酸化銀の製造方法 | |
| JP2001291516A (ja) | 非水系二次電池の負極用黒鉛粒子 | |
| Nakajima et al. | Discharge characteristics of graphite fluoride prepared via graphite oxide | |
| JP2023545343A (ja) | 固体電解質およびそれを含む全固体電池 | |
| JP6836721B2 (ja) | 非水系二次電池用のリン酸三リチウムの製造方法 | |
| JP2000082468A (ja) | 電池正極用リチウムチオレ―トとそれを使用したリチウム二次電池 | |
| JP2000040505A (ja) | リチウム二次電池用の正極体 | |
| JPH10182118A (ja) | 炭素材料およびその製造方法 |