JPS5818349A

JPS5818349A - エステル化合物

エステル化合物

Info

Publication number: JPS5818349A
Authority: JP; Japan
Prior art keywords: compound; liquid crystal; dielectric anisotropy; solvent; formulai
Prior art date: 1981-07-24
Legal status : Granted

Application number

JP11600781A

Other languages

English (en)

Japanese (ja)

Other versions

JPS6124381B2 (enrdf_load_stackoverflow

Inventor

Sadao Kanbe

貞男神戸

Yoshitake Shionozaki

塩野崎　由勇

Motoyuki Toki

元幸土岐

Current Assignee

Seiko Epson Corp

Suwa Seikosha KK

Original Assignee

Seiko Epson Corp

Suwa Seikosha KK

Priority date

1981-07-24

Filing date

1981-07-24

Publication date

1983-02-02

1981-07-24 Application filed by Seiko Epson Corp, Suwa Seikosha KK filed Critical Seiko Epson Corp

1981-07-24 Priority to JP11600781A priority Critical patent/JPS5818349A/ja

1983-02-02 Publication of JPS5818349A publication Critical patent/JPS5818349A/ja

1986-06-10 Publication of JPS6124381B2 publication Critical patent/JPS6124381B2/ja

Status Granted legal-status Critical Current

Links

-1 Ester compound Chemical class 0.000 title abstract description 4
150000001875 compounds Chemical class 0.000 claims abstract description 26
125000000217 alkyl group Chemical group 0.000 claims abstract description 4
125000004432 carbon atom Chemical group C* 0.000 claims description 2
239000004973 liquid crystal related substance Substances 0.000 abstract description 26
239000000203 mixture Substances 0.000 abstract description 9
238000000034 method Methods 0.000 abstract description 7
239000002904 solvent Substances 0.000 abstract description 7
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract description 6
238000005406 washing Methods 0.000 abstract description 4
150000007514 bases Chemical class 0.000 abstract description 2
238000001953 recrystallisation Methods 0.000 abstract description 2
MPAIWVOBMLSHQA-UHFFFAOYSA-N 3,6-dihydroxybenzene-1,2-dicarbonitrile Chemical compound OC1=CC=C(O)C(C#N)=C1C#N MPAIWVOBMLSHQA-UHFFFAOYSA-N 0.000 abstract 1
239000003513 alkali Substances 0.000 abstract 1
239000011541 reaction mixture Substances 0.000 abstract 1
LMBFAGIMSUYTBN-MPZNNTNKSA-N teixobactin Chemical compound C([C@H](C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H](CCC(N)=O)C(=O)N[C@H]([C@@H](C)CC)C(=O)N[C@@H]([C@@H](C)CC)C(=O)N[C@@H](CO)C(=O)N[C@H]1C(N[C@@H](C)C(=O)N[C@@H](C[C@@H]2NC(=N)NC2)C(=O)N[C@H](C(=O)O[C@H]1C)[C@@H](C)CC)=O)NC)C1=CC=CC=C1 LMBFAGIMSUYTBN-MPZNNTNKSA-N 0.000 abstract 1
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
238000000605 extraction Methods 0.000 description 4
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
238000010586 diagram Methods 0.000 description 3
239000000975 dye Substances 0.000 description 3
239000007788 liquid Substances 0.000 description 3
239000000463 material Substances 0.000 description 3
238000002844 melting Methods 0.000 description 3
230000008018 melting Effects 0.000 description 3
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
239000000047 product Substances 0.000 description 2
229910000029 sodium carbonate Inorganic materials 0.000 description 2
238000002834 transmittance Methods 0.000 description 2
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
235000017166 Bambusa arundinacea Nutrition 0.000 description 1
235000017491 Bambusa tulda Nutrition 0.000 description 1
241001330002 Bambuseae Species 0.000 description 1
235000015334 Phyllostachys viridis Nutrition 0.000 description 1
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
238000000862 absorption spectrum Methods 0.000 description 1
239000011425 bamboo Substances 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
AOGYCOYQMAVAFD-UHFFFAOYSA-M carbonochloridate Chemical compound [O-]C(Cl)=O AOGYCOYQMAVAFD-UHFFFAOYSA-M 0.000 description 1
238000006243 chemical reaction Methods 0.000 description 1
239000002131 composite material Substances 0.000 description 1
239000012769 display material Substances 0.000 description 1
238000004090 dissolution Methods 0.000 description 1
239000004744 fabric Substances 0.000 description 1
PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
239000010931 gold Substances 0.000 description 1
229910052737 gold Inorganic materials 0.000 description 1
238000005259 measurement Methods 0.000 description 1
238000002156 mixing Methods 0.000 description 1
231100000989 no adverse effect Toxicity 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
238000011084 recovery Methods 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
239000007858 starting material Substances 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1
210000000689 upper leg Anatomy 0.000 description 1