JPS5782110A - Preparation of titanium nitride and titanium carbide - Google Patents
Preparation of titanium nitride and titanium carbideInfo
- Publication number
- JPS5782110A JPS5782110A JP55159187A JP15918780A JPS5782110A JP S5782110 A JPS5782110 A JP S5782110A JP 55159187 A JP55159187 A JP 55159187A JP 15918780 A JP15918780 A JP 15918780A JP S5782110 A JPS5782110 A JP S5782110A
- Authority
- JP
- Japan
- Prior art keywords
- titanium
- carbide
- titanium oxide
- heat
- gas containing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/076—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with titanium or zirconium or hafnium
Abstract
PURPOSE: To prepare high purity titanium nitride or titanium carbide, easily, at low cost, by mixing fine powder of anatase TiO2 with carbon powder having finer particle size, and heat-treating the mixture in N2 gas or an inert gas containing methane.
CONSTITUTION: Anatase titanium oxide having an average particle diameter of ≤0.5μm is mixed with carbon powder having finer particle size than the titanium oxide. The amount of the carbon powder is 2 times mol which corresponds to the amount necessary to reduce the titanium oxide to metallic Ti or 3 times mol which corresponds to the amount necessary to reduce the titanium oxide to metal and convert to carbide. In the former case, the objective titanium nitride is prepared by heat-treating at 1,300W1,500°C in N2 gas containing methane, and in the latter case, the titanium carbide is obtained by the heat-treatment at a temperature above 1,350°C and below the melting temperature of titanium carbide, in an inert gas containing methane.
COPYRIGHT: (C)1982,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55159187A JPS5782110A (en) | 1980-11-12 | 1980-11-12 | Preparation of titanium nitride and titanium carbide |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55159187A JPS5782110A (en) | 1980-11-12 | 1980-11-12 | Preparation of titanium nitride and titanium carbide |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5782110A true JPS5782110A (en) | 1982-05-22 |
JPS6144801B2 JPS6144801B2 (en) | 1986-10-04 |
Family
ID=15688208
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP55159187A Granted JPS5782110A (en) | 1980-11-12 | 1980-11-12 | Preparation of titanium nitride and titanium carbide |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5782110A (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58213606A (en) * | 1982-06-07 | 1983-12-12 | Mitsubishi Metal Corp | Preparation of titanium nitride powder |
JPS61232211A (en) * | 1985-04-08 | 1986-10-16 | Kogyo Kaihatsu Kenkyusho | Production of titanium carbide |
JPH0196005A (en) * | 1987-10-09 | 1989-04-14 | Nippon Rejibon Kk | Production of titanium nitride |
US4975260A (en) * | 1988-04-18 | 1990-12-04 | Toshiba Ceramics Co., Ltd. | Process for preparing metal nitride powder |
CN102995004A (en) * | 2012-12-24 | 2013-03-27 | 常州大学 | Method for strengthening compounding of TiC on laser-induced metal surface layer by taking TiO2 and methane as components |
RU2627142C1 (en) * | 2016-05-10 | 2017-08-03 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Челябинский государственный педагогический университет" (ФГБОУ ВПО "ЧГПУ") | Method of producing ultra-dispersed titanium carbide powder |
-
1980
- 1980-11-12 JP JP55159187A patent/JPS5782110A/en active Granted
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58213606A (en) * | 1982-06-07 | 1983-12-12 | Mitsubishi Metal Corp | Preparation of titanium nitride powder |
JPS6221723B2 (en) * | 1982-06-07 | 1987-05-14 | Mitsubishi Kinzoku Kk | |
JPS61232211A (en) * | 1985-04-08 | 1986-10-16 | Kogyo Kaihatsu Kenkyusho | Production of titanium carbide |
JPH0140766B2 (en) * | 1985-04-08 | 1989-08-31 | Kaihatsu Kenkyusho Ind Res | |
JPH0196005A (en) * | 1987-10-09 | 1989-04-14 | Nippon Rejibon Kk | Production of titanium nitride |
US4975260A (en) * | 1988-04-18 | 1990-12-04 | Toshiba Ceramics Co., Ltd. | Process for preparing metal nitride powder |
CN102995004A (en) * | 2012-12-24 | 2013-03-27 | 常州大学 | Method for strengthening compounding of TiC on laser-induced metal surface layer by taking TiO2 and methane as components |
RU2627142C1 (en) * | 2016-05-10 | 2017-08-03 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Челябинский государственный педагогический университет" (ФГБОУ ВПО "ЧГПУ") | Method of producing ultra-dispersed titanium carbide powder |
Also Published As
Publication number | Publication date |
---|---|
JPS6144801B2 (en) | 1986-10-04 |
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