JPS5620182A - Electrodeposition method for lead dioxide on surface of anode plate built in electrolytic bath - Google Patents

Electrodeposition method for lead dioxide on surface of anode plate built in electrolytic bath

Info

Publication number
JPS5620182A
JPS5620182A JP9635879A JP9635879A JPS5620182A JP S5620182 A JPS5620182 A JP S5620182A JP 9635879 A JP9635879 A JP 9635879A JP 9635879 A JP9635879 A JP 9635879A JP S5620182 A JPS5620182 A JP S5620182A
Authority
JP
Japan
Prior art keywords
pbo
anode
room
cathode
electrolytic bath
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP9635879A
Other languages
Japanese (ja)
Inventor
Kenjiro Yanagase
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to JP9635879A priority Critical patent/JPS5620182A/en
Publication of JPS5620182A publication Critical patent/JPS5620182A/en
Pending legal-status Critical Current

Links

Abstract

PURPOSE: To obtain PbO2 coat not generating exfoliation or crack, by filling up PbO2 plating solution in the electrolytic bath which can perform power supply operation immediately and turning on an electric current and then, forming PbO2 thin film on the anode plate.
CONSTITUTION: PbO2 plating solution is put in the electrolytic bath regulated and fixed so as to operate immediately and thin PbO2 film is formed on the anode by electrolyzing by the same system direct current in a short time. Then, product on the cathode is dissolved by disscolution solution and is washed by water after discharging and flushing. Hereby, strong PbO2 coat is made on the surface of the anode plate. For example, plating solution containing 10wt% lead nitrate and 1.5wt% copper nitrate, is filled up in the anode room composed of the anode 1, the porous diaphragm 4, the cation exchange membrane 3 and the cathode 2 and middle room and also, cathode room and then, an electric current is turned on at 4A/dm2 current density for two minutes. Inner part is washed by water after discharge. Next, solution containing 3wt% antimony and 0.5wt% ammonium persulfate, is filled up in the cathode room and middle room and is discharged after 4 hours and then, is washed by water. Then, electrolysis of the solution containing Glauber's salt, is immediately performed.
COPYRIGHT: (C)1981,JPO&Japio
JP9635879A 1979-07-27 1979-07-27 Electrodeposition method for lead dioxide on surface of anode plate built in electrolytic bath Pending JPS5620182A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP9635879A JPS5620182A (en) 1979-07-27 1979-07-27 Electrodeposition method for lead dioxide on surface of anode plate built in electrolytic bath

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP9635879A JPS5620182A (en) 1979-07-27 1979-07-27 Electrodeposition method for lead dioxide on surface of anode plate built in electrolytic bath

Publications (1)

Publication Number Publication Date
JPS5620182A true JPS5620182A (en) 1981-02-25

Family

ID=14162764

Family Applications (1)

Application Number Title Priority Date Filing Date
JP9635879A Pending JPS5620182A (en) 1979-07-27 1979-07-27 Electrodeposition method for lead dioxide on surface of anode plate built in electrolytic bath

Country Status (1)

Country Link
JP (1) JPS5620182A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS57199639A (en) * 1981-06-01 1982-12-07 Mitsubishi Heavy Ind Ltd Method of pre-expansion of green tyre in tyre vulcanizer
CN110468279A (en) * 2019-09-09 2019-11-19 赵坤 A method of recycling lead from the lead plaster material of waste lead storage battery

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS53135834A (en) * 1977-04-29 1978-11-27 Olin Corp Method of lowering overvoltage in electrolyte tank and its device
JPS5425275A (en) * 1977-07-27 1979-02-26 Diamond Shamrock Corp Method of plating active coat over cathod of halogenation alkali electrolytic cell there

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS53135834A (en) * 1977-04-29 1978-11-27 Olin Corp Method of lowering overvoltage in electrolyte tank and its device
JPS5425275A (en) * 1977-07-27 1979-02-26 Diamond Shamrock Corp Method of plating active coat over cathod of halogenation alkali electrolytic cell there

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS57199639A (en) * 1981-06-01 1982-12-07 Mitsubishi Heavy Ind Ltd Method of pre-expansion of green tyre in tyre vulcanizer
CN110468279A (en) * 2019-09-09 2019-11-19 赵坤 A method of recycling lead from the lead plaster material of waste lead storage battery
CN110468279B (en) * 2019-09-09 2021-04-06 赵坤 Method for recovering lead from lead plaster material of waste lead storage battery

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