JPS56164129A - Preparation of allyl alcohol - Google Patents
Preparation of allyl alcoholInfo
- Publication number
- JPS56164129A JPS56164129A JP6688680A JP6688680A JPS56164129A JP S56164129 A JPS56164129 A JP S56164129A JP 6688680 A JP6688680 A JP 6688680A JP 6688680 A JP6688680 A JP 6688680A JP S56164129 A JPS56164129 A JP S56164129A
- Authority
- JP
- Japan
- Prior art keywords
- expressed
- formula
- alkyl
- reaction
- allyl alcohol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To obtain the titled compound in high yield in one reactor, by reacting iodotrimethylsilane with an oxirane, dehydroiodinating the resultant 2-iodoalkoxytrimethylsilane, and treating the reaction product with an acid.
CONSTITUTION: Iodotrimethylsilane expressed by formula III is reacted with an oxirane expressed by formula I (R1 is H, 1W10C alkyl or alkenyl which may have a substituent taking no part in the reaction; R2 is H or 1W4C lower alkyl; R3 is 1W10C alkyl or alkenyl which may have a substituent taking no part in the reaction; the dotted line means that R1 and R3 may link to form 5W20 membered ring) to produce a 2-iodoalkoxylrmethylstlane expressed by formula IV, which is dehydroidinated with a base, e.g. 1,8-diazabicyclo[5.4.0]-undecene-7, etc. The resultant compound is then treated with an acid, to give an allyl alcohol expressed by formula II. The raw material can also be synthesized in the same reactor.
USE: A perfume, a medicine or an intermediate therefor.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP6688680A JPS56164129A (en) | 1980-05-20 | 1980-05-20 | Preparation of allyl alcohol |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP6688680A JPS56164129A (en) | 1980-05-20 | 1980-05-20 | Preparation of allyl alcohol |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS56164129A true JPS56164129A (en) | 1981-12-17 |
JPS637170B2 JPS637170B2 (en) | 1988-02-15 |
Family
ID=13328822
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP6688680A Granted JPS56164129A (en) | 1980-05-20 | 1980-05-20 | Preparation of allyl alcohol |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS56164129A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4935451A (en) * | 1989-09-11 | 1990-06-19 | Syracuse University | Conversion of optically active epoxy alcohols to allylic alcohols |
US5087773A (en) * | 1990-04-23 | 1992-02-11 | Syracuse University | Selective tellurium-mediated synthesis of optically active E- or Z-allyl alcohols from optically active epoxy alcohols |
KR20000063913A (en) * | 2000-08-10 | 2000-11-06 | 하현준 | Process for preparing 1,2-diaminopropane alcohols from aziridines |
-
1980
- 1980-05-20 JP JP6688680A patent/JPS56164129A/en active Granted
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4935451A (en) * | 1989-09-11 | 1990-06-19 | Syracuse University | Conversion of optically active epoxy alcohols to allylic alcohols |
US5087773A (en) * | 1990-04-23 | 1992-02-11 | Syracuse University | Selective tellurium-mediated synthesis of optically active E- or Z-allyl alcohols from optically active epoxy alcohols |
KR20000063913A (en) * | 2000-08-10 | 2000-11-06 | 하현준 | Process for preparing 1,2-diaminopropane alcohols from aziridines |
Also Published As
Publication number | Publication date |
---|---|
JPS637170B2 (en) | 1988-02-15 |
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