JPS55111450A - Preparation of n-(1-phenoxy-2,2,2-trichloroethyl)- salicylamide - Google Patents
Preparation of n-(1-phenoxy-2,2,2-trichloroethyl)- salicylamideInfo
- Publication number
- JPS55111450A JPS55111450A JP1724779A JP1724779A JPS55111450A JP S55111450 A JPS55111450 A JP S55111450A JP 1724779 A JP1724779 A JP 1724779A JP 1724779 A JP1724779 A JP 1724779A JP S55111450 A JPS55111450 A JP S55111450A
- Authority
- JP
- Japan
- Prior art keywords
- trichloroethyl
- phenoxy
- formula
- salicylamide
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To obtain the title compound useful as a soil bactericide, readily in high yield and purity, by hydrolyzing, the protected phenol group.
CONSTITUTION: A compound of formula I (R is lower alkylcarbonyl group; X is halogen) is reacted with phenol in the presence a base, e.g. NaOH, to form an 2-alkylcarbonyloxy-N-(1-phenoxy-2,2,2-trichloroethyl)-benzamide of formula II, which is hydrolyzed in the presence of an acidic catalyst, e.g. sulfuric acid, in a solvent, e.g. methanol, to give the title compound of formula III.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP1724779A JPS6058906B2 (en) | 1979-02-19 | 1979-02-19 | Method for producing N-(1-phenoxy-2,2,2-trichloroethyl)-salicylamide |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP1724779A JPS6058906B2 (en) | 1979-02-19 | 1979-02-19 | Method for producing N-(1-phenoxy-2,2,2-trichloroethyl)-salicylamide |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS55111450A true JPS55111450A (en) | 1980-08-28 |
JPS6058906B2 JPS6058906B2 (en) | 1985-12-23 |
Family
ID=11938613
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP1724779A Expired JPS6058906B2 (en) | 1979-02-19 | 1979-02-19 | Method for producing N-(1-phenoxy-2,2,2-trichloroethyl)-salicylamide |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS6058906B2 (en) |
-
1979
- 1979-02-19 JP JP1724779A patent/JPS6058906B2/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
JPS6058906B2 (en) | 1985-12-23 |
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