JPS55111450A - Preparation of n-(1-phenoxy-2,2,2-trichloroethyl)- salicylamide - Google Patents

Preparation of n-(1-phenoxy-2,2,2-trichloroethyl)- salicylamide

Info

Publication number
JPS55111450A
JPS55111450A JP1724779A JP1724779A JPS55111450A JP S55111450 A JPS55111450 A JP S55111450A JP 1724779 A JP1724779 A JP 1724779A JP 1724779 A JP1724779 A JP 1724779A JP S55111450 A JPS55111450 A JP S55111450A
Authority
JP
Japan
Prior art keywords
trichloroethyl
phenoxy
formula
salicylamide
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP1724779A
Other languages
Japanese (ja)
Other versions
JPS6058906B2 (en
Inventor
Kengo Koike
Mineo Maruyama
Shizuo Shimano
Eiichi Tanaka
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Kayaku Co Ltd
Original Assignee
Nippon Kayaku Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Kayaku Co Ltd filed Critical Nippon Kayaku Co Ltd
Priority to JP1724779A priority Critical patent/JPS6058906B2/en
Publication of JPS55111450A publication Critical patent/JPS55111450A/en
Publication of JPS6058906B2 publication Critical patent/JPS6058906B2/en
Expired legal-status Critical Current

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  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

PURPOSE: To obtain the title compound useful as a soil bactericide, readily in high yield and purity, by hydrolyzing, the protected phenol group.
CONSTITUTION: A compound of formula I (R is lower alkylcarbonyl group; X is halogen) is reacted with phenol in the presence a base, e.g. NaOH, to form an 2-alkylcarbonyloxy-N-(1-phenoxy-2,2,2-trichloroethyl)-benzamide of formula II, which is hydrolyzed in the presence of an acidic catalyst, e.g. sulfuric acid, in a solvent, e.g. methanol, to give the title compound of formula III.
COPYRIGHT: (C)1980,JPO&Japio
JP1724779A 1979-02-19 1979-02-19 Method for producing N-(1-phenoxy-2,2,2-trichloroethyl)-salicylamide Expired JPS6058906B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP1724779A JPS6058906B2 (en) 1979-02-19 1979-02-19 Method for producing N-(1-phenoxy-2,2,2-trichloroethyl)-salicylamide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP1724779A JPS6058906B2 (en) 1979-02-19 1979-02-19 Method for producing N-(1-phenoxy-2,2,2-trichloroethyl)-salicylamide

Publications (2)

Publication Number Publication Date
JPS55111450A true JPS55111450A (en) 1980-08-28
JPS6058906B2 JPS6058906B2 (en) 1985-12-23

Family

ID=11938613

Family Applications (1)

Application Number Title Priority Date Filing Date
JP1724779A Expired JPS6058906B2 (en) 1979-02-19 1979-02-19 Method for producing N-(1-phenoxy-2,2,2-trichloroethyl)-salicylamide

Country Status (1)

Country Link
JP (1) JPS6058906B2 (en)

Also Published As

Publication number Publication date
JPS6058906B2 (en) 1985-12-23

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