JPS5481131A - Process for reducting hydrogen permeating quantity in metal surface - Google Patents
Process for reducting hydrogen permeating quantity in metal surfaceInfo
- Publication number
- JPS5481131A JPS5481131A JP14900377A JP14900377A JPS5481131A JP S5481131 A JPS5481131 A JP S5481131A JP 14900377 A JP14900377 A JP 14900377A JP 14900377 A JP14900377 A JP 14900377A JP S5481131 A JPS5481131 A JP S5481131A
- Authority
- JP
- Japan
- Prior art keywords
- hydrogen
- treatment
- gas loop
- calorizing
- permeating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title abstract 6
- 239000001257 hydrogen Substances 0.000 title abstract 4
- 229910052739 hydrogen Inorganic materials 0.000 title abstract 4
- 239000002184 metal Substances 0.000 title abstract 4
- 229910052751 metal Inorganic materials 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 2
- 230000005540 biological transmission Effects 0.000 abstract 3
- 239000007789 gas Substances 0.000 abstract 3
- 238000009792 diffusion process Methods 0.000 abstract 2
- 239000001307 helium Substances 0.000 abstract 2
- 229910052734 helium Inorganic materials 0.000 abstract 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 abstract 2
- 239000010410 layer Substances 0.000 abstract 2
- 239000000919 ceramic Substances 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 239000011247 coating layer Substances 0.000 abstract 1
- 238000000576 coating method Methods 0.000 abstract 1
- 230000006866 deterioration Effects 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- 238000007750 plasma spraying Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C10/00—Solid state diffusion of only metal elements or silicon into metallic material surfaces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Coating By Spraying Or Casting (AREA)
- Other Surface Treatments For Metallic Materials (AREA)
Abstract
PURPOSE: To provide the subject process comprising applying a calorizing coating treatment on a metal surface to form a diffusion layer, thereby to reduce greatly the hydrogen permeating quantity.
CONSTITUTION: A calorizing treatment is applied to a heat transmission pipe of a heat exchanger having a heat transmission area of 1 m2, placed at the intermediate part of, for example, a helium gas loop (temperature : 1000°C, pressure : 40 atm., flow quantity : 100 g/sec.) and a hydrogen gas loop (900°C, 40 atm., 30 g/sec.), thereby to form a diffusion layer of a thickness of about 100 to 200 microns. Then, the quantity of hydrogen gas permeating from the hydrogent gas loop side through a the wall of the heat transmission pipe to the helium gas loop side is measured. Then, the reducitin ratio of the hydrogen permeating quantity is not only reduced greatly, for example, about 1/50 with respect to a pure metal mother body which has been subjected no treatment by the driving of about 900 hours but no deterioration of the coating layer is recognized. Further, when a calorizing treatment is applied to the metal mother body and further plasma spraying of W, Mo or ceramics is applied thereto, the effect of reducing the hydrogen permeating quantity is further maintained for a long period of time.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP52149003A JPS6018748B2 (en) | 1977-12-12 | 1977-12-12 | Method for reducing hydrogen permeation through steel materials |
DE19782836745 DE2836745A1 (en) | 1977-12-12 | 1978-08-22 | Reducing the permeability of metal surfaces to hydrogen - esp. metals employed in nuclear reactors contg. hydrogen or its isotopes |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP52149003A JPS6018748B2 (en) | 1977-12-12 | 1977-12-12 | Method for reducing hydrogen permeation through steel materials |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5481131A true JPS5481131A (en) | 1979-06-28 |
JPS6018748B2 JPS6018748B2 (en) | 1985-05-11 |
Family
ID=15465525
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP52149003A Expired JPS6018748B2 (en) | 1977-12-12 | 1977-12-12 | Method for reducing hydrogen permeation through steel materials |
Country Status (2)
Country | Link |
---|---|
JP (1) | JPS6018748B2 (en) |
DE (1) | DE2836745A1 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006028566A (en) * | 2004-07-14 | 2006-02-02 | Mitsubishi Kakoki Kaisha Ltd | Member for hydrocarbon reforming device |
CN111739672A (en) * | 2020-05-13 | 2020-10-02 | 中国核电工程有限公司 | Structure for reducing tritium permeation rate |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3029488A1 (en) * | 1980-08-02 | 1982-03-04 | GHT Gesellschaft für Hochtemperaturreaktor-Technik mbH, 5060 Bergisch Gladbach | METHOD FOR PRODUCING A PROTECTIVE LAYER ON METAL WORKPIECES |
DE3438339C1 (en) * | 1984-10-19 | 1986-01-30 | Nukem Gmbh, 6450 Hanau | Process for the production of construction parts for media containing gaseous hydrogen isotopes |
JPH02118711U (en) * | 1989-03-13 | 1990-09-25 |
-
1977
- 1977-12-12 JP JP52149003A patent/JPS6018748B2/en not_active Expired
-
1978
- 1978-08-22 DE DE19782836745 patent/DE2836745A1/en active Pending
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006028566A (en) * | 2004-07-14 | 2006-02-02 | Mitsubishi Kakoki Kaisha Ltd | Member for hydrocarbon reforming device |
JP4539907B2 (en) * | 2004-07-14 | 2010-09-08 | 三菱化工機株式会社 | Components for hydrocarbon reformers |
CN111739672A (en) * | 2020-05-13 | 2020-10-02 | 中国核电工程有限公司 | Structure for reducing tritium permeation rate |
CN111739672B (en) * | 2020-05-13 | 2023-12-22 | 中国核电工程有限公司 | Structure for reducing tritium permeation rate |
Also Published As
Publication number | Publication date |
---|---|
DE2836745A1 (en) | 1979-06-13 |
JPS6018748B2 (en) | 1985-05-11 |
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