JPH0525872B2 - - Google Patents
Info
- Publication number
- JPH0525872B2 JPH0525872B2 JP58184357A JP18435783A JPH0525872B2 JP H0525872 B2 JPH0525872 B2 JP H0525872B2 JP 58184357 A JP58184357 A JP 58184357A JP 18435783 A JP18435783 A JP 18435783A JP H0525872 B2 JPH0525872 B2 JP H0525872B2
- Authority
- JP
- Japan
- Prior art keywords
- polyhydric alcohol
- reaction
- aromatic ring
- alcohol
- dac
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 150000005846 sugar alcohols Polymers 0.000 claims description 25
- 238000006243 chemical reaction Methods 0.000 claims description 21
- 125000003118 aryl group Chemical group 0.000 claims description 18
- JKJWYKGYGWOAHT-UHFFFAOYSA-N bis(prop-2-enyl) carbonate Chemical compound C=CCOC(=O)OCC=C JKJWYKGYGWOAHT-UHFFFAOYSA-N 0.000 claims description 17
- 239000003054 catalyst Substances 0.000 claims description 15
- 239000007795 chemical reaction product Substances 0.000 claims description 10
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 150000002484 inorganic compounds Chemical class 0.000 claims description 3
- 229910010272 inorganic material Inorganic materials 0.000 claims description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
- 239000000047 product Substances 0.000 description 11
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 10
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 8
- 239000002994 raw material Substances 0.000 description 6
- 239000011521 glass Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 241001550224 Apha Species 0.000 description 4
- 239000011261 inert gas Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 3
- -1 aliphatic diallyl carbonates Chemical class 0.000 description 3
- 239000012298 atmosphere Substances 0.000 description 3
- 239000000539 dimer Substances 0.000 description 3
- 238000004821 distillation Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000006116 polymerization reaction Methods 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 235000011121 sodium hydroxide Nutrition 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- RVHUMFJSCJBNGS-UHFFFAOYSA-N 2-[2,6-dibromo-4-[2-[3,5-dibromo-4-(2-hydroxyethoxy)phenyl]propan-2-yl]phenoxy]ethanol Chemical compound C=1C(Br)=C(OCCO)C(Br)=CC=1C(C)(C)C1=CC(Br)=C(OCCO)C(Br)=C1 RVHUMFJSCJBNGS-UHFFFAOYSA-N 0.000 description 1
- JWTDCPGVNRBTKT-UHFFFAOYSA-N 2-[2-(2-hydroxyethoxy)phenoxy]ethanol Chemical compound OCCOC1=CC=CC=C1OCCO JWTDCPGVNRBTKT-UHFFFAOYSA-N 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- CLBRCZAHAHECKY-UHFFFAOYSA-N [Co].[Pt] Chemical compound [Co].[Pt] CLBRCZAHAHECKY-UHFFFAOYSA-N 0.000 description 1
- 125000003158 alcohol group Chemical group 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- SYFOAKAXGNMQAX-UHFFFAOYSA-N bis(prop-2-enyl) carbonate;2-(2-hydroxyethoxy)ethanol Chemical compound OCCOCCO.C=CCOC(=O)OCC=C SYFOAKAXGNMQAX-UHFFFAOYSA-N 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- PYGSKMBEVAICCR-UHFFFAOYSA-N hexa-1,5-diene Chemical group C=CCCC=C PYGSKMBEVAICCR-UHFFFAOYSA-N 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 239000012263 liquid product Substances 0.000 description 1
- 150000007530 organic bases Chemical class 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 150000003138 primary alcohols Chemical class 0.000 description 1
- CAEWJEXPFKNBQL-UHFFFAOYSA-N prop-2-enyl carbonochloridate Chemical compound ClC(=O)OCC=C CAEWJEXPFKNBQL-UHFFFAOYSA-N 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 238000001953 recrystallisation Methods 0.000 description 1
- 150000003333 secondary alcohols Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000001308 synthesis method Methods 0.000 description 1
- UWHCKJMYHZGTIT-UHFFFAOYSA-N tetraethylene glycol Chemical compound OCCOCCOCCOCCO UWHCKJMYHZGTIT-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58184357A JPS6075448A (ja) | 1983-10-03 | 1983-10-03 | 芳香環を有する多価アルコ−ルのアリルカ−ボネ−トの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58184357A JPS6075448A (ja) | 1983-10-03 | 1983-10-03 | 芳香環を有する多価アルコ−ルのアリルカ−ボネ−トの製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6075448A JPS6075448A (ja) | 1985-04-27 |
| JPH0525872B2 true JPH0525872B2 (xx) | 1993-04-14 |
Family
ID=16151827
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58184357A Granted JPS6075448A (ja) | 1983-10-03 | 1983-10-03 | 芳香環を有する多価アルコ−ルのアリルカ−ボネ−トの製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6075448A (xx) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101400357B1 (ko) * | 2010-12-28 | 2014-05-27 | 주식회사 케이오씨솔루션 | 알릴카보네이트 화합물의 신규 제조 방법 |
| WO2012091458A2 (ko) * | 2010-12-28 | 2012-07-05 | 주식회사 케이오씨솔루션 | 알릴카보네이트 화합물의 신규 제조 방법 및 이를 이용한 광학용 수지 조성물 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56133246A (en) * | 1980-03-05 | 1981-10-19 | Anic Spa | Manufacture of arylcarbonic ester of polyhydric alcohol |
| JPS57147505A (en) * | 1981-03-09 | 1982-09-11 | Tokuyama Soda Co Ltd | Resin having high refractive index |
| JPS59140214A (ja) * | 1983-01-13 | 1984-08-11 | エニーケム・シンテシース・エセ・ピ・ア | 重合可能な液状組成物 |
-
1983
- 1983-10-03 JP JP58184357A patent/JPS6075448A/ja active Granted
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56133246A (en) * | 1980-03-05 | 1981-10-19 | Anic Spa | Manufacture of arylcarbonic ester of polyhydric alcohol |
| JPS57147505A (en) * | 1981-03-09 | 1982-09-11 | Tokuyama Soda Co Ltd | Resin having high refractive index |
| JPS59140214A (ja) * | 1983-01-13 | 1984-08-11 | エニーケム・シンテシース・エセ・ピ・ア | 重合可能な液状組成物 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6075448A (ja) | 1985-04-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US3091632A (en) | Process for the production of glycol monoesters from aldehydes | |
| JPS6261582B2 (xx) | ||
| JPS61183257A (ja) | Ｎ−メチルカルバメ−トの製法 | |
| JPH0234339B2 (xx) | ||
| JPS6146465B2 (xx) | ||
| JPH0745437B2 (ja) | エステルの製造法 | |
| JPH0525872B2 (xx) | ||
| EP0044510B1 (en) | Process for the preparation of diaryl esters | |
| US4754045A (en) | Method for producing hydroxyphenylpropionic acid ester | |
| US4954613A (en) | Catalytic preparation of polycarbonate from dialkyl carbonate and bis phenol dicarboxylate | |
| JPH02504510A (ja) | フェニルヒドロキノンの合成 | |
| US4002667A (en) | Bis-(2-hydroxyethyl)-terephthalate | |
| JPS63502283A (ja) | スチレン化ヒドロキノンの製造方法 | |
| JPH08295646A (ja) | ビス（ヒドロキシエトキシフェニル）化合物の製造方法 | |
| KR890005300B1 (ko) | 4,4-비스(4-히드록시페닐)시클로헥산카르복실산유도체의 제조방법 | |
| JPH0452259B2 (xx) | ||
| US4418201A (en) | Process for preparation of N-heterocyclic compounds | |
| JPS6218539B2 (xx) | ||
| JPH07113060B2 (ja) | ポリエーテルポリオールの製法 | |
| JP2583241B2 (ja) | ３，３−ビス（４−ヒドロキシフエニル）−シクロヘキサンカルボン酸誘導体およびその製造方法 | |
| JPH0784418B2 (ja) | 芳香族−アルキルカ−ボネ−トの製造方法 | |
| US3148215A (en) | Bis-(aminopropoxyphenyl) alkanes and process for producing the same | |
| JP4168646B2 (ja) | ４，４’−（１−フェニルエチリデン）ビスフェノールの製造方法 | |
| US5856553A (en) | Carbonic acid 3-methoxycarbonyloxy-2,2,4,4-tetramethyl-cyclobutyl ester methyl ester and method of making therefor | |
| EP0813516B1 (en) | Process for the preparation of stilbenedicarboxylate esters |