JPH0512359B2 - - Google Patents
Info
- Publication number
- JPH0512359B2 JPH0512359B2 JP59045152A JP4515284A JPH0512359B2 JP H0512359 B2 JPH0512359 B2 JP H0512359B2 JP 59045152 A JP59045152 A JP 59045152A JP 4515284 A JP4515284 A JP 4515284A JP H0512359 B2 JPH0512359 B2 JP H0512359B2
- Authority
- JP
- Japan
- Prior art keywords
- saponin
- methanol
- soybean hypocotyl
- butanol
- soybean
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 63
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims description 42
- 229930182490 saponin Natural products 0.000 claims description 42
- 150000007949 saponins Chemical class 0.000 claims description 42
- 235000010469 Glycine max Nutrition 0.000 claims description 31
- 244000068988 Glycine max Species 0.000 claims description 31
- 238000000034 method Methods 0.000 claims description 18
- 239000002904 solvent Substances 0.000 claims description 9
- 238000000605 extraction Methods 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 238000000746 purification Methods 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 238000002203 pretreatment Methods 0.000 claims 1
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 238000011282 treatment Methods 0.000 description 4
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 description 3
- 238000005238 degreasing Methods 0.000 description 3
- 239000000284 extract Substances 0.000 description 3
- 239000000401 methanolic extract Substances 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
- -1 aliphatic alcohols Chemical class 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 150000002632 lipids Chemical class 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- VCUFZILGIRCDQQ-KRWDZBQOSA-N N-[[(5S)-2-oxo-3-(2-oxo-3H-1,3-benzoxazol-6-yl)-1,3-oxazolidin-5-yl]methyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C1O[C@H](CN1C1=CC2=C(NC(O2)=O)C=C1)CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F VCUFZILGIRCDQQ-KRWDZBQOSA-N 0.000 description 1
- 229930187719 Soyasaponin Natural products 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- KTUQUZJOVNIKNZ-UHFFFAOYSA-N butan-1-ol;hydrate Chemical compound O.CCCCO KTUQUZJOVNIKNZ-UHFFFAOYSA-N 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 238000003808 methanol extraction Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 230000000144 pharmacologic effect Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000005292 vacuum distillation Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Saccharide Compounds (AREA)
- Medicines Containing Plant Substances (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59045152A JPS60190788A (ja) | 1984-03-09 | 1984-03-09 | 大豆胚軸からのサポニン成分の抽出・精製法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP59045152A JPS60190788A (ja) | 1984-03-09 | 1984-03-09 | 大豆胚軸からのサポニン成分の抽出・精製法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS60190788A JPS60190788A (ja) | 1985-09-28 |
| JPH0512359B2 true JPH0512359B2 (enExample) | 1993-02-17 |
Family
ID=12711297
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP59045152A Granted JPS60190788A (ja) | 1984-03-09 | 1984-03-09 | 大豆胚軸からのサポニン成分の抽出・精製法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS60190788A (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2707646A1 (fr) * | 1993-07-15 | 1995-01-20 | Univ Toulouse | Procédé d'extraction et de purification de saponines hémolytiques. |
| JP2002173287A (ja) * | 2000-12-08 | 2002-06-21 | Furukawa Co Ltd | 作業車両用のマグネット装置 |
-
1984
- 1984-03-09 JP JP59045152A patent/JPS60190788A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS60190788A (ja) | 1985-09-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |