JPH0478734B2 - - Google Patents
Info
- Publication number
- JPH0478734B2 JPH0478734B2 JP1014675A JP1467589A JPH0478734B2 JP H0478734 B2 JPH0478734 B2 JP H0478734B2 JP 1014675 A JP1014675 A JP 1014675A JP 1467589 A JP1467589 A JP 1467589A JP H0478734 B2 JPH0478734 B2 JP H0478734B2
- Authority
- JP
- Japan
- Prior art keywords
- component
- solution
- fibers
- general formula
- alkoxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000835 fiber Substances 0.000 claims description 38
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 27
- 239000010936 titanium Substances 0.000 claims description 24
- 239000000243 solution Substances 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 18
- 238000009987 spinning Methods 0.000 claims description 16
- 238000004519 manufacturing process Methods 0.000 claims description 13
- 150000001875 compounds Chemical class 0.000 claims description 11
- 150000007524 organic acids Chemical class 0.000 claims description 11
- 239000007864 aqueous solution Substances 0.000 claims description 8
- 239000002994 raw material Substances 0.000 claims description 8
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 7
- 150000004703 alkoxides Chemical class 0.000 claims description 7
- 229910017053 inorganic salt Inorganic materials 0.000 claims description 7
- 235000002906 tartaric acid Nutrition 0.000 claims description 7
- 239000011975 tartaric acid Substances 0.000 claims description 7
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- 229910052742 iron Inorganic materials 0.000 claims description 6
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 239000002184 metal Substances 0.000 claims description 6
- 229910052719 titanium Inorganic materials 0.000 claims description 6
- -1 titanium alkoxide Chemical class 0.000 claims description 6
- 229910052804 chromium Inorganic materials 0.000 claims description 5
- 238000010304 firing Methods 0.000 claims description 5
- 229910052733 gallium Inorganic materials 0.000 claims description 5
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- 229910052701 rubidium Inorganic materials 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 5
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 4
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 4
- 239000012528 membrane Substances 0.000 claims description 4
- 229910052792 caesium Inorganic materials 0.000 claims description 3
- 238000000034 method Methods 0.000 description 18
- 239000000463 material Substances 0.000 description 9
- 239000011734 sodium Substances 0.000 description 9
- 239000007788 liquid Substances 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 238000007716 flux method Methods 0.000 description 4
- 229910052708 sodium Inorganic materials 0.000 description 4
- VXUYXOFXAQZZMF-UHFFFAOYSA-N titanium(IV) isopropoxide Chemical compound CC(C)O[Ti](OC(C)C)(OC(C)C)OC(C)C VXUYXOFXAQZZMF-UHFFFAOYSA-N 0.000 description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 3
- 239000012153 distilled water Substances 0.000 description 3
- 230000004907 flux Effects 0.000 description 3
- 239000012456 homogeneous solution Substances 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- 239000002243 precursor Substances 0.000 description 3
- 238000007613 slurry method Methods 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000011550 stock solution Substances 0.000 description 3
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 description 2
- FIPWRIJSWJWJAI-UHFFFAOYSA-N Butyl carbitol 6-propylpiperonyl ether Chemical compound C1=C(CCC)C(COCCOCCOCCCC)=CC2=C1OCO2 FIPWRIJSWJWJAI-UHFFFAOYSA-N 0.000 description 2
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- HDYRYUINDGQKMC-UHFFFAOYSA-M acetyloxyaluminum;dihydrate Chemical compound O.O.CC(=O)O[Al] HDYRYUINDGQKMC-UHFFFAOYSA-M 0.000 description 2
- SMZOGRDCAXLAAR-UHFFFAOYSA-N aluminium isopropoxide Chemical compound [Al+3].CC(C)[O-].CC(C)[O-].CC(C)[O-] SMZOGRDCAXLAAR-UHFFFAOYSA-N 0.000 description 2
- 229940009827 aluminum acetate Drugs 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- CHPZKNULDCNCBW-UHFFFAOYSA-N gallium nitrate Chemical compound [Ga+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O CHPZKNULDCNCBW-UHFFFAOYSA-N 0.000 description 2
- 150000002823 nitrates Chemical class 0.000 description 2
- 235000005985 organic acids Nutrition 0.000 description 2
- 229920000620 organic polymer Polymers 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 229960005235 piperonyl butoxide Drugs 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 102000005717 Myeloma Proteins Human genes 0.000 description 1
- 108010045503 Myeloma Proteins Proteins 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- JPUHCPXFQIXLMW-UHFFFAOYSA-N aluminium triethoxide Chemical compound CCO[Al](OCC)OCC JPUHCPXFQIXLMW-UHFFFAOYSA-N 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000000578 dry spinning Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229940044658 gallium nitrate Drugs 0.000 description 1
- 238000001879 gelation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000012784 inorganic fiber Substances 0.000 description 1
- 229920000592 inorganic polymer Polymers 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000012774 insulation material Substances 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910001629 magnesium chloride Inorganic materials 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- MEFBJEMVZONFCJ-UHFFFAOYSA-N molybdate Chemical compound [O-][Mo]([O-])(=O)=O MEFBJEMVZONFCJ-UHFFFAOYSA-N 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- IKNCGYCHMGNBCP-UHFFFAOYSA-N propan-1-olate Chemical compound CCC[O-] IKNCGYCHMGNBCP-UHFFFAOYSA-N 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 239000012779 reinforcing material Substances 0.000 description 1
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
Landscapes
- Inorganic Compounds Of Heavy Metals (AREA)
- Inorganic Fibers (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1467589A JPH02196027A (ja) | 1989-01-24 | 1989-01-24 | Ａ↓１↓−↓ｘＴｉ↓２↓＋↓ｘＭ↓５↓−↓ｘＯ↓１↓２で示される斜方晶系トンネル構造化合物の繊維又は膜状物の製造法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1467589A JPH02196027A (ja) | 1989-01-24 | 1989-01-24 | Ａ↓１↓−↓ｘＴｉ↓２↓＋↓ｘＭ↓５↓−↓ｘＯ↓１↓２で示される斜方晶系トンネル構造化合物の繊維又は膜状物の製造法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH02196027A JPH02196027A (ja) | 1990-08-02 |
| JPH0478734B2 true JPH0478734B2 (US06521211-20030218-C00004.png) | 1992-12-14 |
Family
ID=11867796
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1467589A Granted JPH02196027A (ja) | 1989-01-24 | 1989-01-24 | Ａ↓１↓−↓ｘＴｉ↓２↓＋↓ｘＭ↓５↓−↓ｘＯ↓１↓２で示される斜方晶系トンネル構造化合物の繊維又は膜状物の製造法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH02196027A (US06521211-20030218-C00004.png) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63165435A (ja) * | 1986-12-27 | 1988-07-08 | Nippon Steel Corp | 有機金属重合組成物の製造方法 |
| JPS63210026A (ja) * | 1987-02-24 | 1988-08-31 | Natl Inst For Res In Inorg Mater | Ａ↓１↓−↓ｘＴｉ↓２↓＋↓ｘＭ↓５↓−↓ｘＯ↓１↓２で示される斜方晶系のトンネル構造を有する繊維状化合物およびその製造方法 |
-
1989
- 1989-01-24 JP JP1467589A patent/JPH02196027A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63165435A (ja) * | 1986-12-27 | 1988-07-08 | Nippon Steel Corp | 有機金属重合組成物の製造方法 |
| JPS63210026A (ja) * | 1987-02-24 | 1988-08-31 | Natl Inst For Res In Inorg Mater | Ａ↓１↓−↓ｘＴｉ↓２↓＋↓ｘＭ↓５↓−↓ｘＯ↓１↓２で示される斜方晶系のトンネル構造を有する繊維状化合物およびその製造方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH02196027A (ja) | 1990-08-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US3322865A (en) | Process of manufacturing refractory fibers | |
| US4180409A (en) | Thermally stable quartz glass | |
| US3704147A (en) | Fibrous inorganic materials | |
| JP2010505047A (ja) | 多結晶コランダム繊維及びその製造方法 | |
| US4104045A (en) | Thermally stable quartz glass | |
| JPH0478734B2 (US06521211-20030218-C00004.png) | ||
| JPH0478731B2 (US06521211-20030218-C00004.png) | ||
| DE2339848A1 (de) | Verfahren zur herstellung poroeser, verkitteter massen aus anorganischen fasern | |
| JPH0478735B2 (US06521211-20030218-C00004.png) | ||
| JPH0478736B2 (US06521211-20030218-C00004.png) | ||
| US5507986A (en) | Method of making a ceramic tube | |
| JPH05331712A (ja) | Ｎａ１−ｘ Ｔｉ２＋ｘ Ａｌ５−ｘ Ｏ１２斜方晶系トンネル構造 化合物の繊維または膜状物の製造方法 | |
| JPH0274526A (ja) | ホーランダイト型構造を有するチタン酸塩の繊維または膜状物の製造法 | |
| Vancso‐Szmercsanyi et al. | Coordination polymers. XIII. Synthesis and investigation of polymers obtained by the reaction of maleic acid with ZnO | |
| JPH0476332B2 (US06521211-20030218-C00004.png) | ||
| JPH0478732B2 (US06521211-20030218-C00004.png) | ||
| JPH078725B2 (ja) | ムライト繊維又は膜状物の製造法 | |
| DE3810523C2 (de) | Eine Zirkoniumverbindung enthaltende wäßrige Lösung | |
| JPH03161522A (ja) | アルミナ繊維又は膜状物の製造法 | |
| JPH0478733B2 (US06521211-20030218-C00004.png) | ||
| EP1264807A1 (de) | Mullithaltiger Stoff, dessen Herstellung und Verwendung | |
| JP2007008799A (ja) | 希土類元素ドープＣｅＯ２微粒子の製造方法 | |
| JPH05321036A (ja) | ジルコニア繊維の製造法 | |
| JPH05124810A (ja) | ムライト焼結体原料、ムライト焼結体及びその製造方法 | |
| JPH01192707A (ja) | 酸化物成形体の製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |