JPH0323557B2 - - Google Patents
Info
- Publication number
- JPH0323557B2 JPH0323557B2 JP11905381A JP11905381A JPH0323557B2 JP H0323557 B2 JPH0323557 B2 JP H0323557B2 JP 11905381 A JP11905381 A JP 11905381A JP 11905381 A JP11905381 A JP 11905381A JP H0323557 B2 JPH0323557 B2 JP H0323557B2
- Authority
- JP
- Japan
- Prior art keywords
- phenyldisilane
- formula
- novel
- general formula
- present
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- -1 phenyldisilane compound Chemical class 0.000 claims description 8
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 4
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 125000001309 chloro group Chemical group Cl* 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 6
- MZRVEZGGRBJDDB-UHFFFAOYSA-N N-Butyllithium Chemical compound [Li]CCCC MZRVEZGGRBJDDB-UHFFFAOYSA-N 0.000 description 6
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 6
- 238000003756 stirring Methods 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- QHXSSKNXFGRFAI-UHFFFAOYSA-N 5,5,6,6-tetramethylbenzo[c][1,2]benzodisiline Chemical compound C1=CC=C2[Si](C)(C)[Si](C)(C)C3=CC=CC=C3C2=C1 QHXSSKNXFGRFAI-UHFFFAOYSA-N 0.000 description 3
- 229910052786 argon Inorganic materials 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- RQJRLVCBMAKXFG-UHFFFAOYSA-N phenyl(silyl)silane Chemical class [SiH3][SiH2]C1=CC=CC=C1 RQJRLVCBMAKXFG-UHFFFAOYSA-N 0.000 description 3
- DRKHIWKXLZCAKP-UHFFFAOYSA-N 1-bromo-2-(2-bromophenyl)benzene Chemical group BrC1=CC=CC=C1C1=CC=CC=C1Br DRKHIWKXLZCAKP-UHFFFAOYSA-N 0.000 description 2
- SFAZXBAPWCPIER-UHFFFAOYSA-N chloro-[chloro(dimethyl)silyl]-dimethylsilane Chemical compound C[Si](C)(Cl)[Si](C)(C)Cl SFAZXBAPWCPIER-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
- 238000002329 infrared spectrum Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000001819 mass spectrum Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- YJQFTKVGILQPMC-UHFFFAOYSA-N 5,5-dimethylbenzo[b][1]benzosilole Chemical compound C1=CC=C2[Si](C)(C)C3=CC=CC=C3C2=C1 YJQFTKVGILQPMC-UHFFFAOYSA-N 0.000 description 1
- 238000005481 NMR spectroscopy Methods 0.000 description 1
- 229910018540 Si C Inorganic materials 0.000 description 1
- DZCSELWKKDJVEK-UHFFFAOYSA-N [Li]C1=CC=CC=C1C1=CC=CC=C1[Li] Chemical group [Li]C1=CC=CC=C1C1=CC=CC=C1[Li] DZCSELWKKDJVEK-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- RGDZHSGMSWHBAK-UHFFFAOYSA-N chloro-[chloro(diethyl)silyl]-diethylsilane Chemical compound CC[Si](Cl)(CC)[Si](Cl)(CC)CC RGDZHSGMSWHBAK-UHFFFAOYSA-N 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 238000004811 liquid chromatography Methods 0.000 description 1
- 125000000962 organic group Chemical group 0.000 description 1
- 238000006303 photolysis reaction Methods 0.000 description 1
- 230000015843 photosynthesis, light reaction Effects 0.000 description 1
- 229920000548 poly(silane) polymer Polymers 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11905381A JPS5821684A (ja) | 1981-07-31 | 1981-07-31 | 新規フェニルジシラン系化合物とそれを製造する方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP11905381A JPS5821684A (ja) | 1981-07-31 | 1981-07-31 | 新規フェニルジシラン系化合物とそれを製造する方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5821684A JPS5821684A (ja) | 1983-02-08 |
| JPH0323557B2 true JPH0323557B2 (zh) | 1991-03-29 |
Family
ID=14751733
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP11905381A Granted JPS5821684A (ja) | 1981-07-31 | 1981-07-31 | 新規フェニルジシラン系化合物とそれを製造する方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5821684A (zh) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SG124249A1 (en) | 2001-12-07 | 2006-08-30 | Sumitomo Chemical Co | New polymer and polymer light-emitting device using the same |
-
1981
- 1981-07-31 JP JP11905381A patent/JPS5821684A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5821684A (ja) | 1983-02-08 |
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