JPH0255419B2 - - Google Patents
Info
- Publication number
- JPH0255419B2 JPH0255419B2 JP25491885A JP25491885A JPH0255419B2 JP H0255419 B2 JPH0255419 B2 JP H0255419B2 JP 25491885 A JP25491885 A JP 25491885A JP 25491885 A JP25491885 A JP 25491885A JP H0255419 B2 JPH0255419 B2 JP H0255419B2
- Authority
- JP
- Japan
- Prior art keywords
- met
- methionine
- acl
- benzoyl
- salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 230000003287 optical effect Effects 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 12
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- PPFRJEXUPZWQPI-UHFFFAOYSA-N 2-benzamido-4-methylsulfanylbutanoic acid Chemical compound CSCCC(C(O)=O)NC(=O)C1=CC=CC=C1 PPFRJEXUPZWQPI-UHFFFAOYSA-N 0.000 claims description 7
- BOWUOGIPSRVRSJ-UHFFFAOYSA-N 2-aminohexano-6-lactam Chemical compound NC1CCCCNC1=O BOWUOGIPSRVRSJ-UHFFFAOYSA-N 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 description 13
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 239000013078 crystal Substances 0.000 description 7
- 239000002904 solvent Substances 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- FFEARJCKVFRZRR-BYPYZUCNSA-N L-methionine Chemical compound CSCC[C@H](N)C(O)=O FFEARJCKVFRZRR-BYPYZUCNSA-N 0.000 description 3
- 229960004452 methionine Drugs 0.000 description 3
- PPFRJEXUPZWQPI-SNVBAGLBSA-N (2r)-2-benzamido-4-methylsulfanylbutanoic acid Chemical compound CSCC[C@H](C(O)=O)NC(=O)C1=CC=CC=C1 PPFRJEXUPZWQPI-SNVBAGLBSA-N 0.000 description 2
- PPFRJEXUPZWQPI-JTQLQIEISA-N (2s)-2-benzamido-4-methylsulfanylbutanoic acid Chemical compound CSCC[C@@H](C(O)=O)NC(=O)C1=CC=CC=C1 PPFRJEXUPZWQPI-JTQLQIEISA-N 0.000 description 2
- FFEARJCKVFRZRR-UHFFFAOYSA-N L-Methionine Natural products CSCCC(N)C(O)=O FFEARJCKVFRZRR-UHFFFAOYSA-N 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 229930182817 methionine Natural products 0.000 description 2
- 125000001360 methionine group Chemical group N[C@@H](CCSC)C(=O)* 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- UQDJGEHQDNVPGU-UHFFFAOYSA-N serine phosphoethanolamine Chemical compound [NH3+]CCOP([O-])(=O)OCC([NH3+])C([O-])=O UQDJGEHQDNVPGU-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 229930195722 L-methionine Natural products 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 244000309464 bull Species 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 102000004196 processed proteins & peptides Human genes 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP25491885A JPS62114954A (ja) | 1985-11-15 | 1985-11-15 | Ｎ−ベンゾイル−ｄｌ−メチオニンの光学分割方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP25491885A JPS62114954A (ja) | 1985-11-15 | 1985-11-15 | Ｎ−ベンゾイル−ｄｌ−メチオニンの光学分割方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS62114954A JPS62114954A (ja) | 1987-05-26 |
| JPH0255419B2 true JPH0255419B2 (xx) | 1990-11-27 |
Family
ID=17271664
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP25491885A Granted JPS62114954A (ja) | 1985-11-15 | 1985-11-15 | Ｎ−ベンゾイル−ｄｌ−メチオニンの光学分割方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS62114954A (xx) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5122871B2 (ja) * | 2007-06-01 | 2013-01-16 | 大東化学株式会社 | 光学活性ｎ−ベンジルオキシカルボニルアミノ酸の製造方法およびジアステレオマー塩 |
-
1985
- 1985-11-15 JP JP25491885A patent/JPS62114954A/ja active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS62114954A (ja) | 1987-05-26 |
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