JPH0212460B2 - - Google Patents
Info
- Publication number
- JPH0212460B2 JPH0212460B2 JP23859384A JP23859384A JPH0212460B2 JP H0212460 B2 JPH0212460 B2 JP H0212460B2 JP 23859384 A JP23859384 A JP 23859384A JP 23859384 A JP23859384 A JP 23859384A JP H0212460 B2 JPH0212460 B2 JP H0212460B2
- Authority
- JP
- Japan
- Prior art keywords
- indium
- acetoacetate
- trisalkyl
- triisopropylate
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052738 indium Inorganic materials 0.000 claims description 38
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 claims description 36
- WDJHALXBUFZDSR-UHFFFAOYSA-M acetoacetate Chemical compound CC(=O)CC([O-])=O WDJHALXBUFZDSR-UHFFFAOYSA-M 0.000 claims description 17
- -1 Indium trisbutylacetoacetate Chemical compound 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 10
- 150000001875 compounds Chemical class 0.000 claims description 5
- 125000000217 alkyl group Chemical group 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 24
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 12
- 239000003960 organic solvent Substances 0.000 description 9
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- 239000013522 chelant Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 238000005481 NMR spectroscopy Methods 0.000 description 5
- 239000004020 conductor Substances 0.000 description 5
- 238000007650 screen-printing Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- REIYHFWZISXFKU-UHFFFAOYSA-N Butyl acetoacetate Chemical compound CCCCOC(=O)CC(C)=O REIYHFWZISXFKU-UHFFFAOYSA-N 0.000 description 4
- 150000002472 indium compounds Chemical class 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005530 etching Methods 0.000 description 3
- XYIBRDXRRQCHLP-UHFFFAOYSA-N ethyl acetoacetate Chemical compound CCOC(=O)CC(C)=O XYIBRDXRRQCHLP-UHFFFAOYSA-N 0.000 description 3
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000004973 liquid crystal related substance Substances 0.000 description 2
- 239000011541 reaction mixture Substances 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000004448 titration Methods 0.000 description 2
- 238000001771 vacuum deposition Methods 0.000 description 2
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- JJLKTTCRRLHVGL-UHFFFAOYSA-L [acetyloxy(dibutyl)stannyl] acetate Chemical compound CC([O-])=O.CC([O-])=O.CCCC[Sn+2]CCCC JJLKTTCRRLHVGL-UHFFFAOYSA-L 0.000 description 1
- CUJRVFIICFDLGR-UHFFFAOYSA-N acetylacetonate Chemical compound CC(=O)[CH-]C(C)=O CUJRVFIICFDLGR-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 238000001879 gelation Methods 0.000 description 1
- 229910003437 indium oxide Inorganic materials 0.000 description 1
- PJXISJQVUVHSOJ-UHFFFAOYSA-N indium(iii) oxide Chemical compound [O-2].[O-2].[O-2].[In+3].[In+3] PJXISJQVUVHSOJ-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- DHGFMVMDBNLMKT-UHFFFAOYSA-N propyl 3-oxobutanoate Chemical compound CCCOC(=O)CC(C)=O DHGFMVMDBNLMKT-UHFFFAOYSA-N 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Non-Insulated Conductors (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP23859384A JPS61118338A (ja) | 1984-11-14 | 1984-11-14 | インジウムトリスアルキルアセトアセテ−トおよびその製造方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP23859384A JPS61118338A (ja) | 1984-11-14 | 1984-11-14 | インジウムトリスアルキルアセトアセテ−トおよびその製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS61118338A JPS61118338A (ja) | 1986-06-05 |
JPH0212460B2 true JPH0212460B2 (enrdf_load_stackoverflow) | 1990-03-20 |
Family
ID=17032500
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP23859384A Granted JPS61118338A (ja) | 1984-11-14 | 1984-11-14 | インジウムトリスアルキルアセトアセテ−トおよびその製造方法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS61118338A (enrdf_load_stackoverflow) |
-
1984
- 1984-11-14 JP JP23859384A patent/JPS61118338A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS61118338A (ja) | 1986-06-05 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JPH11349536A (ja) | 9,10―エンドエタノ―9,10―ジハイドロアントラセン―11,11―ジカルボン酸のモノエステルまたはジエステルの合成方法,この合成方法により得られる新規なモノエステルまたはジエステル、及びこれらの、均整または不整メチリデンマロネ―トの合成への応用 | |
JP2551434B2 (ja) | 3,4−ジヒドロキシテトラヒドロフランカーボネート及びその製造方法 | |
JPH0212460B2 (enrdf_load_stackoverflow) | ||
JPH0133108B2 (enrdf_load_stackoverflow) | ||
JPH0212461B2 (enrdf_load_stackoverflow) | ||
JPH0212462B2 (enrdf_load_stackoverflow) | ||
JPH0133109B2 (enrdf_load_stackoverflow) | ||
JP3777408B2 (ja) | カルボン酸誘導体の製造法 | |
JPH0616656A (ja) | 含フッ素無水フタル酸類の製造方法 | |
JPH0610158B2 (ja) | 3−フルオロ安息香酸類の製造方法 | |
JP3457349B2 (ja) | 化学気相析出法による成膜用組成物 | |
JPS62192389A (ja) | 1,1―ジクロロ―1,2,2―トリメチル―2―フェニルジシランの製造方法 | |
JPS6136292A (ja) | タングステンオキシアルコキシド化合物およびその製造方法ならびにエレクトロクロミツク表示素子の製造方法 | |
JP3876933B2 (ja) | 硫酸水素エステルの製造方法 | |
US4026930A (en) | Azeotropic distillation of 1,1,1,3,3,3-hexafluoroisopropyl trifluoroacetate with fluorotrichloromethane | |
JPH0137397B2 (enrdf_load_stackoverflow) | ||
US3990989A (en) | Azeotropic composition containing fluorotrichloromethane and 1,1,1,3,3,3-hexafluoroisopropyl trifluoroacetate | |
JP4502086B2 (ja) | イソシアヌレート誘導体の製造方法 | |
JP2816760B2 (ja) | ビス(アルキルシクロヘキシル)リン酸の製造方法 | |
CN117777016A (zh) | 一种肉豆蔻醇烟酸酯的合成方法 | |
JP3436314B2 (ja) | 2−メルカプト−5−メトキシベンズイミダゾールの製造法 | |
KR820001181B1 (ko) | 벤젠 포스포닉 디할라이드의 제조방법 | |
JPH11158139A (ja) | スルホアニリニウムイソフタル酸ジエステルの製造方法 | |
SU727634A1 (ru) | Способ получени -(2-аза-2-нитроалкил)-амидов | |
JPS5934718B2 (ja) | エチルアセチレンマグネシウムハクイドの製造方法 |