JPH0135768B2 - - Google Patents
Info
- Publication number
- JPH0135768B2 JPH0135768B2 JP56157807A JP15780781A JPH0135768B2 JP H0135768 B2 JPH0135768 B2 JP H0135768B2 JP 56157807 A JP56157807 A JP 56157807A JP 15780781 A JP15780781 A JP 15780781A JP H0135768 B2 JPH0135768 B2 JP H0135768B2
- Authority
- JP
- Japan
- Prior art keywords
- graphite
- alf
- ternary
- stage
- intercalation compound
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 88
- 229910002804 graphite Inorganic materials 0.000 claims description 82
- 239000010439 graphite Substances 0.000 claims description 82
- 150000001875 compounds Chemical class 0.000 claims description 72
- 238000009830 intercalation Methods 0.000 claims description 50
- 230000002687 intercalation Effects 0.000 claims description 49
- 229910016569 AlF 3 Inorganic materials 0.000 claims description 36
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 18
- 229910052731 fluorine Inorganic materials 0.000 claims description 18
- 239000011737 fluorine Substances 0.000 claims description 18
- KLZUFWVZNOTSEM-UHFFFAOYSA-K Aluminum fluoride Inorganic materials F[Al](F)F KLZUFWVZNOTSEM-UHFFFAOYSA-K 0.000 claims description 12
- IRPGOXJVTQTAAN-UHFFFAOYSA-N 2,2,3,3,3-pentafluoropropanal Chemical compound FC(F)(F)C(F)(F)C=O IRPGOXJVTQTAAN-UHFFFAOYSA-N 0.000 claims description 10
- 239000004020 conductor Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 description 16
- 238000002441 X-ray diffraction Methods 0.000 description 8
- 239000000126 substance Substances 0.000 description 8
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 description 7
- QLOAVXSYZAJECW-UHFFFAOYSA-N methane;molecular fluorine Chemical compound C.FF QLOAVXSYZAJECW-UHFFFAOYSA-N 0.000 description 6
- 238000001228 spectrum Methods 0.000 description 5
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 239000007770 graphite material Substances 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 230000000737 periodic effect Effects 0.000 description 3
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 229910021383 artificial graphite Inorganic materials 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 229910021382 natural graphite Inorganic materials 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- RGPBQGGBWIMGMA-BJMVGYQFSA-N 5-[(e)-[5-(4-bromophenyl)-6-hydroxy-3,6-dihydro-1,3,4-oxadiazin-2-ylidene]methyl]-1h-pyrimidine-2,4-dione Chemical compound OC1O\C(=C\C=2C(NC(=O)NC=2)=O)NN=C1C1=CC=C(Br)C=C1 RGPBQGGBWIMGMA-BJMVGYQFSA-N 0.000 description 1
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- 229910019080 Mg-H Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 239000011889 copper foil Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000000921 elemental analysis Methods 0.000 description 1
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
- 150000002222 fluorine compounds Chemical class 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- 238000005087 graphitization Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910001512 metal fluoride Inorganic materials 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Substances N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 238000006053 organic reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000002006 petroleum coke Substances 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Carbon And Carbon Compounds (AREA)
- Conductive Materials (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Priority Applications (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP56157807A JPS5860607A (ja) | 1981-10-03 | 1981-10-03 | 黒鉛とフッ化アルミニウム及びフッ素との3成分系黒鉛層間化合物、及びその製造方法ならびにそれから成る電導材料 |
US06/394,530 US4477374A (en) | 1981-10-03 | 1982-07-02 | Ternary intercalation compound of a graphite with a metal fluoride and fluorine, a process for producing the same, and an electrically conductive material comprising the ternary intercalation compound |
GB08219748A GB2107296B (en) | 1981-10-03 | 1982-07-08 | A ternary intercalation compound of graphite with a metal fluoride and fluorine a process for producing the same and an electrically conductive material comprising the ternary intercalation compound |
IT22633/82A IT1152305B (it) | 1981-10-03 | 1982-07-29 | Composto ternario intercalare di grafite con un fluoruro metallico e fluoro,procedimento per la sua produzione e materiale elettroconduttore comprendente il composto ternario intercalare |
FR8213413A FR2513981B1 (fr) | 1981-10-03 | 1982-07-30 | Compose ternaire d'intercalation d'un graphite avec un fluorure d'un metal et du fluor, procede pour sa production et materiau electriquement conducteur le contenant |
NL8203056A NL8203056A (nl) | 1981-10-03 | 1982-07-30 | Nieuwe intercalaire verbinding van grafiet. |
DE3235596A DE3235596A1 (de) | 1981-10-03 | 1982-09-25 | Ternaere einlagerungsverbindung, verfahren zu ihrer herstellung und elektrisch leitendes material, enthaltend die verbindung |
NL8603066A NL8603066A (nl) | 1981-10-03 | 1986-12-01 | Nieuwe intercalatieverbindingen van grafiet. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP56157807A JPS5860607A (ja) | 1981-10-03 | 1981-10-03 | 黒鉛とフッ化アルミニウム及びフッ素との3成分系黒鉛層間化合物、及びその製造方法ならびにそれから成る電導材料 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5860607A JPS5860607A (ja) | 1983-04-11 |
JPH0135768B2 true JPH0135768B2 (enrdf_load_stackoverflow) | 1989-07-27 |
Family
ID=15657711
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP56157807A Granted JPS5860607A (ja) | 1981-10-03 | 1981-10-03 | 黒鉛とフッ化アルミニウム及びフッ素との3成分系黒鉛層間化合物、及びその製造方法ならびにそれから成る電導材料 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5860607A (enrdf_load_stackoverflow) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6287407A (ja) * | 1985-10-12 | 1987-04-21 | Res Dev Corp Of Japan | フイルム状グラフアイト層間化合物及びその製造方法 |
EP4264641A1 (de) | 2020-12-15 | 2023-10-25 | Robert Bosch GmbH | Verfahren zum herstellen eines elektrisch leitfähigen leiterstrangs mit zumindest einem kohlenstoffleiter |
-
1981
- 1981-10-03 JP JP56157807A patent/JPS5860607A/ja active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS5860607A (ja) | 1983-04-11 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US5286471A (en) | Graphite flouride from iodine intercalated graphitized carbon | |
JPH0413289B2 (enrdf_load_stackoverflow) | ||
US4477374A (en) | Ternary intercalation compound of a graphite with a metal fluoride and fluorine, a process for producing the same, and an electrically conductive material comprising the ternary intercalation compound | |
JPH0139965B2 (enrdf_load_stackoverflow) | ||
JPS6362446B2 (enrdf_load_stackoverflow) | ||
US4128499A (en) | Lewis acid-fluorine compounds of carbon | |
JP2608515B2 (ja) | フッ化ピッチ | |
JPH09124395A (ja) | ダイヤモンド層、界面相及び金属基板を含んでなる多層系並びにそれらの層を得る方法 | |
JPH0135768B2 (enrdf_load_stackoverflow) | ||
JPH0135769B2 (enrdf_load_stackoverflow) | ||
JPH0329002B2 (enrdf_load_stackoverflow) | ||
Fujimoto et al. | New fluorine-carbon compound prepared by the direct fluorination of mesophase pitch | |
Nakajima et al. | Synthesis of fluorine-graphite intercalation compounds by elemental fluorine and high oxidation-state transition-metal fluorides | |
El’tsov et al. | Modification of porous silicon in ultrahigh vacuum and contribution of graphite nanocrystallites to photoluminescence | |
JP3010532B2 (ja) | 液状フルオロカーボン及びその製造方法 | |
KR102529546B1 (ko) | 저분자량의 유기 화합물을 이용한 그래핀의 제조방법 | |
US4950814A (en) | Liquid fluorocarbon and a method for producing the same | |
JP2526311B2 (ja) | 黒鉛層間化合物の安定化法 | |
JPS63295412A (ja) | 新規な黒鉛層間化合物およびその製造方法 | |
JPH1160222A (ja) | ホウ素及び/又は窒素置換フラーレンの製造方法 | |
JP2000026985A (ja) | 炭素材料の製法 | |
JPS63260807A (ja) | 被覆層を備えた黒鉛層間化合物及びその製造方法 | |
JPH04300205A (ja) | 黒鉛層間化合物 | |
JPH04202056A (ja) | グラファイトの製造方法 | |
JPS6355196A (ja) | 高熱伝導性ダイヤモンドの製造方法 |