JP7813579B2 - 粒子の製造方法 - Google Patents

粒子の製造方法

Info

Publication number
JP7813579B2
JP7813579B2 JP2021510237A JP2021510237A JP7813579B2 JP 7813579 B2 JP7813579 B2 JP 7813579B2 JP 2021510237 A JP2021510237 A JP 2021510237A JP 2021510237 A JP2021510237 A JP 2021510237A JP 7813579 B2 JP7813579 B2 JP 7813579B2
Authority
JP
Japan
Prior art keywords
dispersion medium
layered compound
particles
particle
graphite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2021510237A
Other languages
English (en)
Japanese (ja)
Other versions
JPWO2021141013A1 (https=
Inventor
拓也 工藤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sekisui Chemical Co Ltd
Original Assignee
Sekisui Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sekisui Chemical Co Ltd filed Critical Sekisui Chemical Co Ltd
Publication of JPWO2021141013A1 publication Critical patent/JPWO2021141013A1/ja
Application granted granted Critical
Publication of JP7813579B2 publication Critical patent/JP7813579B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/20Graphite
    • C01B32/21After-treatment
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/04Processes of manufacture in general
    • H01M4/0471Processes of manufacture in general involving thermal treatment, e.g. firing, sintering, backing particulate active material, thermal decomposition, pyrolysis
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/362Composites
    • H01M4/366Composites as layered products
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/38Selection of substances as active materials, active masses, active liquids of elements or alloys
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/38Selection of substances as active materials, active masses, active liquids of elements or alloys
    • H01M4/386Silicon or alloys based on silicon
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/583Carbonaceous material, e.g. graphite-intercalation compounds or CFx
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/62Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/62Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
    • H01M4/624Electric conductive fillers
    • H01M4/625Carbon or graphite
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/02Silicon
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/80Particles consisting of a mixture of two or more inorganic phases
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/80Particles consisting of a mixture of two or more inorganic phases
    • C01P2004/82Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases
    • C01P2004/84Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases one phase coated with the other
    • C01P2004/86Thin layer coatings, i.e. the coating thickness being less than 0.1 time the particle radius
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/10Solid density
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/052Li-accumulators
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/054Accumulators with insertion or intercalation of metals other than lithium, e.g. with magnesium or aluminium
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/021Physical characteristics, e.g. porosity, surface area
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/38Selection of substances as active materials, active masses, active liquids of elements or alloys
    • H01M4/387Tin or alloys based on tin
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/483Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides for non-aqueous cells
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/50Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
    • H01M4/505Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/48Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
    • H01M4/52Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
    • H01M4/525Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Composite Materials (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacturing & Machinery (AREA)
  • Engineering & Computer Science (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Carbon And Carbon Compounds (AREA)
JP2021510237A 2020-01-07 2021-01-05 粒子の製造方法 Active JP7813579B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2020000901 2020-01-07
JP2020000901 2020-01-07
PCT/JP2021/000054 WO2021141013A1 (ja) 2020-01-07 2021-01-05 粒子の製造方法

Publications (2)

Publication Number Publication Date
JPWO2021141013A1 JPWO2021141013A1 (https=) 2021-07-15
JP7813579B2 true JP7813579B2 (ja) 2026-02-13

Family

ID=76788067

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2021510237A Active JP7813579B2 (ja) 2020-01-07 2021-01-05 粒子の製造方法

Country Status (6)

Country Link
US (1) US20230299270A1 (https=)
EP (1) EP4089049A4 (https=)
JP (1) JP7813579B2 (https=)
KR (1) KR20220123651A (https=)
CN (1) CN114981210A (https=)
WO (1) WO2021141013A1 (https=)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014115669A1 (ja) 2013-01-23 2014-07-31 東レ株式会社 正極活物質―グラフェン複合体粒子およびリチウムイオン電池用正極材料ならびに正極活物質―グラフェン複合体粒子の製造方法
JP2016195103A (ja) 2015-03-31 2016-11-17 東レ株式会社 複合導電性粒子およびその製造方法ならびに導電性樹脂
JP2017199670A (ja) 2016-04-21 2017-11-02 東レ株式会社 リチウムイオン電池用正極材料およびその製造方法、リチウムイオン電池用正極、リチウムイオン電池
JP2019052083A (ja) 2017-09-13 2019-04-04 東レ株式会社 グラフェン粉末、グラフェン粉末/有機溶媒分散液、グラフェン−電極活物質複合体粒子および電極ペーストおよび電極

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101752561B (zh) * 2009-12-11 2012-08-22 宁波艾能锂电材料科技股份有限公司 石墨烯改性磷酸铁锂正极活性材料及其制备方法以及锂离子二次电池
JP5329006B1 (ja) * 2011-09-29 2013-10-30 昭和電工株式会社 リチウム二次電池用正極活物質及びその製造方法
CN102983313B (zh) * 2012-12-05 2016-01-27 奇瑞汽车股份有限公司 硅碳复合材料及其制备方法、锂离子电池
CN104638267A (zh) * 2013-11-12 2015-05-20 赵宽 石墨烯包覆钛酸锂负极及其制备方法
WO2015073674A1 (en) * 2013-11-13 2015-05-21 Xg Sciences, Inc. Silicon-graphene nanocomposites for electrochemical applications
US9899672B2 (en) 2016-05-17 2018-02-20 Nanotek Instruments, Inc. Chemical-free production of graphene-encapsulated electrode active material particles for battery applications

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014115669A1 (ja) 2013-01-23 2014-07-31 東レ株式会社 正極活物質―グラフェン複合体粒子およびリチウムイオン電池用正極材料ならびに正極活物質―グラフェン複合体粒子の製造方法
JP2016195103A (ja) 2015-03-31 2016-11-17 東レ株式会社 複合導電性粒子およびその製造方法ならびに導電性樹脂
JP2017199670A (ja) 2016-04-21 2017-11-02 東レ株式会社 リチウムイオン電池用正極材料およびその製造方法、リチウムイオン電池用正極、リチウムイオン電池
JP2019052083A (ja) 2017-09-13 2019-04-04 東レ株式会社 グラフェン粉末、グラフェン粉末/有機溶媒分散液、グラフェン−電極活物質複合体粒子および電極ペーストおよび電極

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
ZHANG, Jiangshan et al.,In Situ synthesis of SiC-graphene core-shell nanoparticles using wet ball milling,Ceramics International,2018年,Vol.44,Issue 7,pp.8283-8289

Also Published As

Publication number Publication date
EP4089049A4 (en) 2024-01-17
JPWO2021141013A1 (https=) 2021-07-15
CN114981210A (zh) 2022-08-30
US20230299270A1 (en) 2023-09-21
WO2021141013A1 (ja) 2021-07-15
EP4089049A1 (en) 2022-11-16
KR20220123651A (ko) 2022-09-08

Similar Documents

Publication Publication Date Title
US11777077B2 (en) Silicon particles for battery electrodes
CN113228346B (zh) 具有预锂化涂层的阴极及其制备方法和用途
TWI558860B (zh) 陽極電池材料及其製造方法
JP6210980B2 (ja) 離散カーボンナノチューブを用いたリチウムイオン電池、その製造方法およびそれから得られる生成物
TWI625885B (zh) 用於多孔性矽顆粒生產之經結合之電化學及化學蝕刻方法
CN112839900B (zh) 石墨烯分散液及其制造方法以及二次电池用电极
CN103647057A (zh) 锂二次电池、负电极、负极活性物质及其制备方法
TWI682577B (zh) 活性物質-薄片化石墨複合體、鋰離子二次電池用負極材料及鋰離子二次電池
EP2715843A1 (en) Electrode material for lithium and lithium ion batteries
KR20220003107A (ko) 저결함 터보스트래틱 탄소를 포함하는 애노드 활성 물질
KR20190047367A (ko) 다층 그래핀과 금속합금분말을 이용하여 제조되는 다공성 실리콘-나노 탄소층-다층 그래핀 복합체 및 그 제조방법
CN106165157A (zh) 用于锂二次电池的负极活性材料的制造方法、和锂二次电池
TW201628236A (zh) 電極組成物、電化學電池及製造電化學電池之方法
KR20220016496A (ko) 실리콘-지배적 배터리 전극
JP7813579B2 (ja) 粒子の製造方法
US20250183272A1 (en) Graphene and silicon based anodes for lithium-ion batteries
JP2025535341A (ja) 新規な結合剤を含むエネルギー貯蔵デバイスのための電極
US12548760B2 (en) Silicon particles for battery electrodes
WO2020189662A1 (ja) 複合材料、蓄電デバイス用電極材料、及び蓄電デバイス
JP2025535397A (ja) 親水性官能基を有する結合剤を含むエネルギー貯蔵デバイス用の電極
JP2025143041A (ja) 複合活物質および電池
HK40025995B (zh) 包含碳化硅和碳颗粒的复合物
HK40032858A (en) Composite comprising silicon carbide and carbon particles
HK40032858B (en) Composite comprising silicon carbide and carbon particles

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20231002

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20250107

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20250303

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20250708

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20250905

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20260106

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20260202

R150 Certificate of patent or registration of utility model

Ref document number: 7813579

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150