JP7379862B2 - 短鎖塩素化パラフィンの同族体の検出方法 - Google Patents

短鎖塩素化パラフィンの同族体の検出方法 Download PDF

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JP7379862B2
JP7379862B2 JP2019089135A JP2019089135A JP7379862B2 JP 7379862 B2 JP7379862 B2 JP 7379862B2 JP 2019089135 A JP2019089135 A JP 2019089135A JP 2019089135 A JP2019089135 A JP 2019089135A JP 7379862 B2 JP7379862 B2 JP 7379862B2
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congener
relative
column
sccps
formula
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JP2020183924A5 (enExample
JP2020183924A (ja
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ユン ゾウ
尚樹 濱田
リャン ドン
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Shimadzu Corp
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/282—Porous sorbents
    • B01J20/285—Porous sorbents based on polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/26—Synthetic macromolecular compounds
    • B01J20/262—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon to carbon unsaturated bonds, e.g. obtained by polycondensation
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • G01N30/52—Physical parameters
    • G01N30/54—Temperature
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/62—Detectors specially adapted therefor
    • G01N30/72—Mass spectrometers
    • G01N30/7206—Mass spectrometers interfaced to gas chromatograph
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/60—Use in several different columns
    • B01J2220/603—Use in several different columns serially disposed columns
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/04—Preparation or injection of sample to be analysed
    • G01N2030/042—Standards
    • G01N2030/045—Standards internal
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
    • G01N2030/884—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds
    • G01N2030/8854—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds involving hydrocarbons

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  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
JP2019089135A 2019-05-09 2019-05-09 短鎖塩素化パラフィンの同族体の検出方法 Active JP7379862B2 (ja)

Priority Applications (2)

Application Number Priority Date Filing Date Title
JP2019089135A JP7379862B2 (ja) 2019-05-09 2019-05-09 短鎖塩素化パラフィンの同族体の検出方法
US16/851,555 US20200355651A1 (en) 2019-05-09 2020-04-17 Detection method for congeners of short-chain chlorinated paraffins

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JP2019089135A JP7379862B2 (ja) 2019-05-09 2019-05-09 短鎖塩素化パラフィンの同族体の検出方法

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JP2020183924A5 JP2020183924A5 (enExample) 2021-10-14
JP7379862B2 true JP7379862B2 (ja) 2023-11-15

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CN112526010B (zh) * 2020-11-17 2022-09-27 浙江省海洋水产研究所 一种海产品中短链氯化石蜡的检测方法
CN112730684A (zh) * 2020-12-27 2021-04-30 宁波市华测检测技术有限公司 一种检测海水沉积物生物体短链氯化石蜡的测试方法
CN113484452B (zh) * 2021-04-12 2024-01-02 黎明职业大学 鞋服制品塑料件中链氯化石蜡的检测方法
CN113533556B (zh) * 2021-06-18 2022-04-29 广东省农业科学院农业质量标准与监测技术研究所 一种肝微粒体离体代谢氯化石蜡的方法
CN116068097B (zh) * 2021-11-01 2025-11-14 中国石油化工股份有限公司 一种航煤中的抗氧剂的分离方法及含量测定的方法
JP7596328B2 (ja) * 2022-03-23 2024-12-09 株式会社東芝 有機ハロゲン化合物の分析方法
CN114924010B (zh) * 2022-06-17 2024-11-26 广州海关技术中心 一种测定氯化石蜡原料中的短链和中链氯化石蜡含量的方法
CN116609154B (zh) * 2023-06-05 2025-11-25 中轻检验认证有限公司 用于检测皮革中短链氯化石蜡的标准样品及其制备方法

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JP2004061485A (ja) 2002-06-03 2004-02-26 Chubu Electric Power Co Inc Ｐｃｂの分析法
JP2006284371A (ja) 2005-03-31 2006-10-19 Shimadzu Corp 質量分析方法
US20070137481A1 (en) 2005-12-20 2007-06-21 Jan Blomberg Method to measure olefins in a complex hydrocarbon mixture
US20090139934A1 (en) 2007-12-03 2009-06-04 Schlumberger Technology Corporation Differential acceleration chromatography
JP2014521928A (ja) 2011-06-10 2014-08-28 テクノロジアン テュトキムスケスクス ヴェーテーテー アルツハイマー病のリスクの増加を診断するための方法
US20180095060A1 (en) 2016-10-04 2018-04-05 The Regents Of The University Of Michigan Multi-channel multi-dimensional comprehensive gas chromatography

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US5135549A (en) * 1991-01-30 1992-08-04 The Board Of Trustees Of Southern Illinois University Chromatographic technique and apparatus
US5498279A (en) * 1994-05-13 1996-03-12 Chromatofast High speed gas chromatography system for analysis of polar organic compounds
US8145438B2 (en) * 2006-10-31 2012-03-27 Shimadzu Corporation Method for quantitating substance to be measured

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004061485A (ja) 2002-06-03 2004-02-26 Chubu Electric Power Co Inc Ｐｃｂの分析法
JP2006284371A (ja) 2005-03-31 2006-10-19 Shimadzu Corp 質量分析方法
US20070137481A1 (en) 2005-12-20 2007-06-21 Jan Blomberg Method to measure olefins in a complex hydrocarbon mixture
US20090139934A1 (en) 2007-12-03 2009-06-04 Schlumberger Technology Corporation Differential acceleration chromatography
JP2014521928A (ja) 2011-06-10 2014-08-28 テクノロジアン テュトキムスケスクス ヴェーテーテー アルツハイマー病のリスクの増加を診断するための方法
US20180095060A1 (en) 2016-10-04 2018-04-05 The Regents Of The University Of Michigan Multi-channel multi-dimensional comprehensive gas chromatography

Non-Patent Citations (3)

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Title
Dan Xia et al,，A Novel Method for Profiling and Quantifying Short-and Medium-Chain Chlorinated Paraffins in Environmental Samples Using Comprehensive Two-Dimensional Gas Chromatography-Electron Capture Negative Ionization High- Resolution Time-of-Flight Mass Spectrometry，Environmental Science and Technology，2016年05月16日，50，P7601-7609
Gregg T. Tomy，Analysis of Chlorinated Paraffins in Environmental Matrics: The Ultimate Challenge for the Analytical Chemist，Analysis of Chlorinated Paraffins in Environmental Matrics，Vol.10，2010年01月12日，P83-106
落合伸夫，包括的2次元ガスクロマトグラフィー（ＧＣ×ＧＣ）の原理と環境分析への応用，環境技術，Vol.34 No.11，2005年，P801-805

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