JP7281751B2 - 封止用樹脂組成物、積層シート、硬化物、半導体装置及び半導体装置の製造方法 - Google Patents
封止用樹脂組成物、積層シート、硬化物、半導体装置及び半導体装置の製造方法 Download PDFInfo
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Description
封止用樹脂組成物である実施例1~4、参考例1、及び比較例1~4を、次のように調製した。
・変性ポリブタジエン:マレイン酸変性ポリブタジエン、クレイバレー社製、品名Ricobond1756。
・アクリル化合物1:エトキシ化ビスフェノールAジメタクリレート、新中村化学工業社製、品番BPE-100。
・アクリル化合物2:ビスフェノールA型エポキシアクリレート、昭和高分子社製、品番VR-77。
・アクリル化合物3:トリシクロデカンジメタノールジアクリレート、新中村化学工業社製、品番A-DCP。
・アクリル化合物4:トリメチロールプロパントリアクリレート、新中村化学工業社製、品番A-TMPT。
・ポリフェニレンエーテル樹脂:上記式(3)に示す構造を有し、式(3)中のXが上記式(1)に示す構造を有する基(Rはメチル基)である、変性ポリフェニレンエーテル樹脂、SABIC社製、品番SA9000。
・熱ラジカル重合開始剤:ジクミルパーオキサイド、日油株式会社製、品名パークミルD。
・熱可塑性樹脂:メチルメタクリレート,n-ブチルメタクリレート共重合体、エボニック社製、品名DYNACOLL AC2740。
・無機充填材1(フィラー):シリカ粉、株式会社トクヤマ製、品番NMH-24D、平均粒径0.24μm。
・無機充填材2(フィラー):株式会社アドマテックス製、品番SO-C2、平均粒径0.5μm。
・ニトロキシド化合物:2,2,6,6-テトラメチル-1-ピペリジンオキシフリーラジカル、東京化成工業株式会社製。
・シランカップリング剤:3-グリシドキシプロピルトリメトキシシラン、信越化学工業株式会社製、品番KBM-403。
・フラックス:セバシン酸。
封止用樹脂組成物に対し、次の評価試験を行った。これらの評価試験の結果は、表1に示す。
各実施例、参考例、及び比較例の封止用樹脂組成物を、TAインスツルメンツ株式会社製のレオメータ(型番 AR2000ex)を用いて、温度範囲100~300℃、昇温速度60℃/min、角速度0.209rad/sの条件で、溶融粘度の温度依存性を測定した。これにより、各封止用樹脂組成物の温度と溶融粘度との関係を示す溶融粘度曲線を得た。この溶融粘度曲線から、最低溶融粘度を読み取るとともに、最低溶融粘度から50Pa・s上昇した溶融粘度における温度を読み取ることで、封止用樹脂組成物の反応開始温度を得た。また、この反応開始温度を基準として、反応開始温度での溶融粘度、反応開始温度より40℃低い温度以上反応開始温度以下の温度での最も高い溶融粘度、及び反応開始温度より50℃低い温度での溶融粘度を読み取り、所定の温度での溶融粘度をそれぞれ表1の所定の欄に示した。
支持シートとしてポリエチレンテレフタレート製フィルムを用意した。この支持シートに封止用樹脂組成物を、バーコーターを用いて湿潤膜厚100μmになるように成膜し、80℃、30分間の条件で加熱した。これにより、支持シート上に厚み50μmのシート材を作製した。複数枚のシート材を積層し、真空ラミネーターで圧縮成形し、オーブンで150℃、2時間の条件で加熱することで硬化させ、続いてカットすることで、平面視4mm×40mm、厚み800mmの寸法のサンプルを作製した。
封止用樹脂組成物を用い、次のようにして半導体装置を作製した。
封止用樹脂組成物を用い、上記(3)ボイド評価の場合と同じ方法で試験用の半導体装置を作製した。この半導体装置の接続性を、次のように評価した。半導体装置を切断し、それにより生じた断面を研磨した。この断面に現れる、はんだバンプを介した、半導体チップにおけるCuピラーと基材の導体配線との間の寸法を測定した。その結果、この寸法が5μm未満であれば「A」、5μm以上10μm未満であれば「B」、10μm以上であれば「C」と評価した。
封止用樹脂組成物を用い、上記(3)ボイド評価の場合と同じ方法で試験用の半導体装置を作製した。半導体装置における硬化物と半導体チップ及び基材との界面の剥離の有無を、超音波探傷装置(SAT)を用いて調査した。その結果、剥離が認められない場合を「A」、剥離が認められる場合を「C」と、評価した。
2 基材
21 導体配線
3 半導体チップ
31 バンプ電極
40 シート材
41 封止材
6 積層シート
Claims (9)
- 基材と前記基材に実装されている半導体チップとの間の隙間を封止するための封止用樹脂組成物であり、
前記封止用樹脂組成物の反応開始温度は、160℃以下であり、
前記封止用樹脂組成物の溶融粘度は、
前記反応開始温度において200Pa・s以下、
前記反応開始温度より40℃低い温度以上前記反応開始温度以下のいかなる温度においても400Pa・s以下、かつ
前記反応開始温度より50℃低い温度において、1000Pa・s以下である、
封止用樹脂組成物。 - アクリル化合物(A)と、
ラジカル重合性を有する置換基(b1)を有するポリフェニレンエーテル樹脂(B)と、
熱ラジカル重合開始剤(C)と、
を含有する、
請求項1に記載の封止用樹脂組成物。 - 無機充填材(D)を更に含有する、
請求項1又は2に記載の封止用樹脂組成物。 - シート状の形状を有する、
請求項1から3のいずれか一項に記載の封止用樹脂組成物。 - 請求項4に記載の封止用樹脂組成物と、
前記封止用樹脂組成物を支持する支持シートを備える、
積層シート。 - 請求項1から4のいずれか一項に記載の封止用樹脂組成物を、熱硬化させて得られる、
硬化物。 - ガラス転移温度は、100℃以上である、
請求項6に記載の硬化物。 - 基材と、
前記基材にフェイスダウンで実装されている半導体チップと、
前記基材と前記半導体チップとの間の隙間を封止する封止材とを備え、
前記封止材が請求項6又は7に記載の硬化物からなる、
半導体装置。 - 導体配線を備える基材の前記導体配線がある面に、請求項1から4のいずれか一項に記載の封止用樹脂組成物を介在させて、バンプ電極を備える半導体チップを前記導体配線と前記バンプ電極が対向するように配置し、
前記封止用樹脂組成物を加熱しながら、超音波振動を与えることで、前記封止用樹脂組成物を硬化させるとともに、前記導体配線と前記バンプ電極とを電気的に接続することを含む、
半導体装置の製造方法。
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US20150348861A1 (en) | 2014-05-28 | 2015-12-03 | Stats Chippac, Ltd. | Semiconductor device and method of forming adhesive layer over insulating layer for bonding carrier to mixed surfaces of semiconductor die and encapsulant |
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