JP7086995B2 - 解析対象液体の処理装置 - Google Patents

解析対象液体の処理装置 Download PDF

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Publication number
JP7086995B2
JP7086995B2 JP2019563079A JP2019563079A JP7086995B2 JP 7086995 B2 JP7086995 B2 JP 7086995B2 JP 2019563079 A JP2019563079 A JP 2019563079A JP 2019563079 A JP2019563079 A JP 2019563079A JP 7086995 B2 JP7086995 B2 JP 7086995B2
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Japan
Prior art keywords
liquid
chamber
cylindrical chamber
processing apparatus
cryogenic
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JP2019563079A
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English (en)
Japanese (ja)
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JP2020521120A (ja
Inventor
パトリック・ルボー
フレデリック・クレイサック
ブノー・ダビディアン
マシュー・ルクレール
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
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Priority claimed from FR1754452A external-priority patent/FR3066596B1/fr
Priority claimed from FR1754453A external-priority patent/FR3066597B1/fr
Application filed by LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/40Concentrating samples
    • G01N1/4022Concentrating samples by thermal techniques; Phase changes
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C13/00Details of vessels or of the filling or discharging of vessels
    • F17C13/02Special adaptations of indicating, measuring, or monitoring equipment
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C13/00Details of vessels or of the filling or discharging of vessels
    • F17C13/08Mounting arrangements for vessels
    • F17C13/086Mounting arrangements for vessels for Dewar vessels or cryostats
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04406Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
    • F25J3/04412Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system in a classical double column flowsheet, i.e. with thermal coupling by a main reboiler-condenser in the bottom of low pressure respectively top of high pressure column
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04769Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04854Safety aspects of operation
    • F25J3/0486Safety aspects of operation of vaporisers for oxygen enriched liquids, e.g. purging of liquids
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/01Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the phase
    • F17C2223/0146Two-phase
    • F17C2223/0153Liquefied gas, e.g. LPG, GPL
    • F17C2223/0161Liquefied gas, e.g. LPG, GPL cryogenic, e.g. LNG, GNL, PLNG
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2250/00Accessories; Control means; Indicating, measuring or monitoring of parameters
    • F17C2250/04Indicating or measuring of parameters as input values
    • F17C2250/0404Parameters indicated or measured
    • F17C2250/0447Composition; Humidity
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2280/00Control of the process or apparatus
    • F25J2280/02Control in general, load changes, different modes ("runs"), measurements
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2202Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
    • G01N1/2214Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling by sorption
    • G01N2001/2217Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling by sorption using a liquid
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/40Concentrating samples
    • G01N1/4022Concentrating samples by thermal techniques; Phase changes
    • G01N2001/4027Concentrating samples by thermal techniques; Phase changes evaporation leaving a concentrated sample

Landscapes

  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Chemical & Material Sciences (AREA)
  • Immunology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Thermal Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
JP2019563079A 2017-05-19 2018-05-18 解析対象液体の処理装置 Active JP7086995B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
FR1754452 2017-05-19
FR1754452A FR3066596B1 (fr) 2017-05-19 2017-05-19 Procede d'analyse des traces de contaminants d'un liquide cryogenique
FR1754453 2017-05-19
FR1754453A FR3066597B1 (fr) 2017-05-19 2017-05-19 Appareil d'analyse des traces de contaminants d'un liquide cryogenique
PCT/FR2018/051207 WO2018211230A1 (fr) 2017-05-19 2018-05-18 Appareil de traitement de liquide a analyser

Publications (2)

Publication Number Publication Date
JP2020521120A JP2020521120A (ja) 2020-07-16
JP7086995B2 true JP7086995B2 (ja) 2022-06-20

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JP2019563079A Active JP7086995B2 (ja) 2017-05-19 2018-05-18 解析対象液体の処理装置
JP2019563134A Active JP7019726B2 (ja) 2017-05-19 2018-05-18 極低温液体の極微量汚染物質の解析方法

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JP2019563134A Active JP7019726B2 (ja) 2017-05-19 2018-05-18 極低温液体の極微量汚染物質の解析方法

Country Status (7)

Country Link
US (2) US11585738B2 (zh)
EP (2) EP3625536B1 (zh)
JP (2) JP7086995B2 (zh)
KR (1) KR20200009041A (zh)
CN (2) CN110621973A (zh)
RU (2) RU2757775C2 (zh)
WO (2) WO2018211229A1 (zh)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114041034B (zh) * 2019-07-10 2023-07-21 大阳日酸株式会社 空气分离装置及空气分离方法
FR3116324B1 (fr) * 2020-11-19 2023-05-05 Air Liquide Procédé et appareil de vaporisation d’un liquide
FR3116586B1 (fr) * 2020-11-26 2023-05-12 Air Liquide Procédé et appareil de vaporisation de liquide de purge d’un vaporiseur de liquide cryogénique

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004069676A (ja) 2002-04-25 2004-03-04 L'air Liquide Sa Pour L'etude & L'exploitation Des Procedes Georges Claude 低温液体を試料採取するための方法およびシステムならびに少なくとも1つのそのようなシステムを備える空気分離ユニット

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US3123982A (en) * 1964-03-10 Cryogenic gas sampler
DE2408845C2 (de) * 1974-02-23 1985-01-10 Linde Ag, 6200 Wiesbaden Probenahmegerät für verflüssigte Gase
CA1320849C (en) * 1988-06-02 1993-08-03 Jose M. Dieguez Cryogenic liquid sampling
JP3061471B2 (ja) * 1991-02-18 2000-07-10 大阪酸素工業株式会社 液サンプリング装置
US5282927A (en) * 1991-05-09 1994-02-01 Mark Weidner Concentrating evaporator
US5567887A (en) * 1994-03-10 1996-10-22 Texas Instruments Incorporated Anhydrous ammonia gas sampler and concentration system
FR2730172B1 (fr) * 1995-02-07 1997-03-21 Air Liquide Methode et appareil de surveillance de fonctionnement d'une installation de separation d'air
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Publication number Priority date Publication date Assignee Title
JP2004069676A (ja) 2002-04-25 2004-03-04 L'air Liquide Sa Pour L'etude & L'exploitation Des Procedes Georges Claude 低温液体を試料採取するための方法およびシステムならびに少なくとも1つのそのようなシステムを備える空気分離ユニット

Also Published As

Publication number Publication date
WO2018211229A1 (fr) 2018-11-22
RU2019139654A (ru) 2021-06-07
CN110621973A (zh) 2019-12-27
EP3625535A1 (fr) 2020-03-25
CN110869731B (zh) 2023-07-28
US20200209113A1 (en) 2020-07-02
US11585738B2 (en) 2023-02-21
RU2019141098A (ru) 2021-06-15
JP2020521120A (ja) 2020-07-16
JP7019726B2 (ja) 2022-02-15
US20200191689A1 (en) 2020-06-18
RU2019139654A3 (zh) 2021-06-07
KR20200009041A (ko) 2020-01-29
RU2755284C2 (ru) 2021-09-14
JP2020521121A (ja) 2020-07-16
RU2757775C2 (ru) 2021-10-21
RU2019141098A3 (zh) 2021-06-15
EP3625536A1 (fr) 2020-03-25
EP3625536B1 (fr) 2022-11-16
WO2018211230A1 (fr) 2018-11-22
CN110869731A (zh) 2020-03-06

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