JP6867207B2 - ガラス板合紙用木材パルプ及びその使用、ガラス板用合紙、並びにガラス板合紙用木材パルプ又はガラス板用合紙の検査方法 - Google Patents
ガラス板合紙用木材パルプ及びその使用、ガラス板用合紙、並びにガラス板合紙用木材パルプ又はガラス板用合紙の検査方法 Download PDFInfo
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- JP6867207B2 JP6867207B2 JP2017063453A JP2017063453A JP6867207B2 JP 6867207 B2 JP6867207 B2 JP 6867207B2 JP 2017063453 A JP2017063453 A JP 2017063453A JP 2017063453 A JP2017063453 A JP 2017063453A JP 6867207 B2 JP6867207 B2 JP 6867207B2
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- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 description 1
- 229960002446 octanoic acid Drugs 0.000 description 1
- 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
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- XMLQWXUVTXCDDL-UHFFFAOYSA-N oleyl alcohol Natural products CCCCCCC=CCCCCCCCCCCO XMLQWXUVTXCDDL-UHFFFAOYSA-N 0.000 description 1
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- 125000004817 pentamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 1
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- 125000001147 pentyl group Chemical group C(CCCC)* 0.000 description 1
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- 235000021317 phosphate Nutrition 0.000 description 1
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- 238000000206 photolithography Methods 0.000 description 1
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- 229920000768 polyamine Polymers 0.000 description 1
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- 229920000515 polycarbonate Polymers 0.000 description 1
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- 229920000193 polymethacrylate Polymers 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
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- 229920002635 polyurethane Polymers 0.000 description 1
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- 229920000915 polyvinyl chloride Polymers 0.000 description 1
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- 229940096992 potassium oleate Drugs 0.000 description 1
- MLICVSDCCDDWMD-KVVVOXFISA-M potassium;(z)-octadec-9-enoate Chemical compound [K+].CCCCCCCC\C=C/CCCCCCCC([O-])=O MLICVSDCCDDWMD-KVVVOXFISA-M 0.000 description 1
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- 125000002572 propoxy group Chemical group [*]OC([H])([H])C(C([H])([H])[H])([H])[H] 0.000 description 1
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- 230000004043 responsiveness Effects 0.000 description 1
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- 125000005372 silanol group Chemical group 0.000 description 1
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- 229920002050 silicone resin Polymers 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- XCPXWEJIDZSUMF-UHFFFAOYSA-M sodium;dioctyl phosphate Chemical compound [Na+].CCCCCCCCOP([O-])(=O)OCCCCCCCC XCPXWEJIDZSUMF-UHFFFAOYSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 229940032094 squalane Drugs 0.000 description 1
- 229940031439 squalene Drugs 0.000 description 1
- TUHBEKDERLKLEC-UHFFFAOYSA-N squalene Natural products CC(=CCCC(=CCCC(=CCCC=C(/C)CCC=C(/C)CC=C(C)C)C)C)C TUHBEKDERLKLEC-UHFFFAOYSA-N 0.000 description 1
- 239000011550 stock solution Substances 0.000 description 1
- 239000010902 straw Substances 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- 229940099373 sudan iii Drugs 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
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- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
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- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 1
- LADGBHLMCUINGV-UHFFFAOYSA-N tricaprin Chemical compound CCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCC)COC(=O)CCCCCCCCC LADGBHLMCUINGV-UHFFFAOYSA-N 0.000 description 1
- 229940117985 trimethyl pentaphenyl trisiloxane Drugs 0.000 description 1
- SCRSFLUHMDMRFP-UHFFFAOYSA-N trimethyl-(methyl-octyl-trimethylsilyloxysilyl)oxysilane Chemical compound CCCCCCCC[Si](C)(O[Si](C)(C)C)O[Si](C)(C)C SCRSFLUHMDMRFP-UHFFFAOYSA-N 0.000 description 1
- LINXHFKHZLOLEI-UHFFFAOYSA-N trimethyl-[phenyl-bis(trimethylsilyloxy)silyl]oxysilane Chemical compound C[Si](C)(C)O[Si](O[Si](C)(C)C)(O[Si](C)(C)C)C1=CC=CC=C1 LINXHFKHZLOLEI-UHFFFAOYSA-N 0.000 description 1
- SVTUWEUXLNHYPF-UHFFFAOYSA-N trimethyl-[propyl-bis(trimethylsilyloxy)silyl]oxysilane Chemical compound CCC[Si](O[Si](C)(C)C)(O[Si](C)(C)C)O[Si](C)(C)C SVTUWEUXLNHYPF-UHFFFAOYSA-N 0.000 description 1
- 125000003258 trimethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])[*:1] 0.000 description 1
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Description
JIS P 8120による普通紙試験片の離解方法に従って前記木材パルプを分散させてスラリーを調製し、
前記スラリーに着色剤又は発色剤を加えた後の着色スラリー又は発色スラリーをフローサイトメーターで測定したときの0.1μm〜50μmのサイズの着色異物又は発色異物の個数が30000個/μg以下であるガラス板合紙用木材パルプである。
JIS P 8120による普通紙試験片の離解方法に従って前記合紙を分散させてスラリーを調製し、
前記スラリーに着色剤又は発色剤を加えた後の着色スラリー又は発色スラリーをフローサイトメーターで測定したときの0.1μm〜50μmのサイズの着色異物又は発色異物の個数が15000個/μg以下であるガラス板用合紙である。
ガラス板合紙用木材パルプ又はガラス板用合紙をJIS P 8120による普通紙試験片の離解方法に従って分散させてスラリーを調製する工程、
前記スラリーに着色剤又は発色剤を加えて着色スラリー又は発色スラリーを得る工程、
前記着色又は発色スラリーをフローサイトメーターで測定して0.1μm〜50μmのサイズの着色異物又は発色異物の個数を測定する工程、
前記異物の数が30000個/μg以下のガラス板合紙用木材パルプ又は前記異物の数が15000個/μg以下のガラス板用合紙を選別する工程
を含む、ガラス板合紙用木材パルプ又はガラス板用合紙の検査方法に関する。
JIS P 8120による普通紙試験片の離解方法に従って前記木材パルプを分散させてスラリーを調製し、
前記スラリーに着色剤又は発色剤を加えた後の着色スラリー又は発色スラリーをフローサイトメーターで測定したときの0.1μm〜50μmのサイズの着色異物又は発色異物の個数が30000個/μg以下、好ましくは25000個/μg以下、より好ましくは20000個/μg以下であるガラス板合紙用木材パルプである。
JIS P 8120による普通紙試験片の離解方法に従って前記合紙を分散させてスラリーを調製し、
前記スラリーに着色剤又は発色剤を加えた後の着色スラリー又は発色スラリーをフローサイトメーターで測定したときの0.1μm〜50μmのサイズの着色異物又は発色異物の個数が15000個/μg以下、好ましくは10000個/μg以下、より好ましくは7000個/μg以下であるガラス板用合紙である。
R1 3SiO−(R1 2SiO)a−SiR1 3 (1)
(式中、
R1は、それぞれ独立して、水素原子、水酸基、或いは、置換若しくは非置換の一価炭化水素基、アルコキシ基で示される基から選択される基であり、
aは、0〜1000の整数であり、
bは3〜100の整数であり、
cは1〜4の整数、好ましくは2〜4の整数である)
で表されるオルガノポリシロキサンが挙げられる。
R2 3SiO−(R1 2SiO)d−(R1ASiO)e−SiR2 3 (4)
(式中、
R1は、それぞれ独立して、上記と同様であり、
R2は、それぞれ独立して、R1又はAであり、
Aは、それぞれ独立して、R3Gで表される基であり、R3は、置換若しくは非置換の二価炭化水素基であり、Gはエチレンオキサイド、プロピレンオキサイド等の炭素数2〜5のアルキレンオキサイドを少なくとも1種含有してなるポリオキシアルキレン基を表し、
dは1〜500の整数を表し、
eは1〜50の整数を表す)。
xは20〜160であり、yは1〜25であり、x/yの値は50〜2であり、
Aは、例えば−(CH2)3O−(CH2CH2O)m−(CH2CH2CH2O)n−R4であり、mは7〜40、nは0〜40、m+nの値は少なくとも1であり、グラフト重合されたものでもランダム重合されたものでもよく、R4は水素原子又は上記置換若しくは非置換の一価炭化水素基を表す。好適には、mは7〜30、nは0〜30である)
ガラス板合紙用木材パルプ又はガラス板用合紙をJIS P 8120による普通紙試験片の離解方法に従って分散させてスラリーを調製する工程、
前記スラリーに着色剤又は発色剤を加えて着色スラリー又は発色スラリーを得る工程、
前記着色又は発色スラリーをフローサイトメーターで測定して0.1μm〜50μmのサイズの着色異物又は発色異物の個数を測定する工程、
前記異物の数が30000個/μg以下のガラス板合紙用木材パルプ又は前記異物の数が15000個/μg以下のガラス板用合紙を選別する工程
を含む。
蒸解工程と、洗浄工程と、酸素脱リグニン反応工程と、二酸化塩素及び過酸化水素による多段晒漂白工程とからなる針葉樹晒クラフトパルプの製造装置において、蒸解工程後にノットを除去した直後のドラムウォッシャーの洗浄液に使用される消泡剤として非シリコーン系の消泡剤である鉱物油系消泡剤「プロナールA5044」(東邦化学社製)の原液を適量連続添加した。また、プレス洗浄の工程でウォッシュプレスに添加される消泡剤として同じく「プロナールA5044」を適量加えた。なお、洗浄工程ではトルエンとメタノールを混合した溶剤で洗浄し、ろ過する溶剤洗浄を5回繰り返した。以上のように、製造工程中で非シリコーン系消泡剤を使用した針葉樹晒クラフトパルプAを得た。この針葉樹晒クラフトパルプAの形態を、定法に従って、厚さ1.2mm、坪量700g/m2のシート状パルプとした。
この針葉樹晒クラフトパルプAをJIS P 8120による普通紙試験片の離解方法に従って分散させて1g/100mlの濃度のスラリーを調製し、前記スラリーに「ナイルレッド」(和光純薬工業(株))を20ppm添加した後の着色スラリーをフローサイトメーター(シスメックス社製CyFlow Cube 6)で測定したときの0.1μm〜50μmのサイズの発色異物の個数は26000個/μgであった。
前記溶剤洗浄を行わない以外は実施例1と同様にして針葉樹晒クラフトパルプBを得た。この針葉樹晒クラフトパルプBの形態を、定法に従って、厚さ1.2mm、坪量700g/m2のシート状パルプとした。
この針葉樹晒クラフトパルプAをJIS P 8120による普通紙試験片の離解方法に従って分散させて1g/100mlの濃度のスラリーを調製し、前記スラリーに「ナイルレッド」(和光純薬工業(株))を20ppm添加した後の着色スラリーをフローサイトメーター(シスメックス社製CyFlow Cube 6)で測定したときの0.1μm〜50μmのサイズの発色異物の個数は38000個/μgであった。
木材パルプとして実施例1の針葉樹晒クラフトパルプAを100質量部用意し、これを離解して叩解度を520mlc.s.f.に調製したスラリーに紙力増強剤としてポリアクリルアミド(商品名:ポリストロン1250、荒川化学工業社製)を全パルプ質量に対して0.5質量部添加し、0.4%濃度のパルプスラリーを調製した。これから、長網抄紙機を使用して、坪量50g/m2、厚さ0.093mmのガラス板合紙を得た。
このガラス板合紙をJIS P 8120による普通紙試験片の離解方法に従って分散させて1g/100mlの濃度のスラリーを調製し、前記スラリーに「ナイルレッド」(和光純薬工業(株))を20ppm添加した後の着色スラリーをフローサイトメーター(シスメックス社製CyFlow Cube 6)で測定したときの0.1μm〜50μmのサイズの発色異物の個数は12000個/μgであった。
木材パルプとして比較例1の針葉樹晒クラフトパルプB100質量部を使用した以外は実施例2と同様の手法で、坪量50g/m2のガラス板合紙を得た。
このガラス板合紙をJIS P 8120による普通紙試験片の離解方法に従って分散させて1g/100mlの濃度のスラリーを調製し、前記スラリーに「ナイルレッド」(和光純薬工業(株))を20ppm添加した後の着色スラリーをフローサイトメーター(シスメックス社製CyFlow Cube 6)で測定したときの0.1μm〜50μmのサイズの発色異物の個数は19000個/μgであった。
Claims (6)
- TFT液晶ディスプレイ用若しくは有機ELディスプレイ用であるガラス板の合紙用木材パルプ又はTFT液晶ディスプレイ用若しくは有機ELディスプレイ用であるガラス板用合紙をJIS P 8120による普通紙試験片の離解方法に従って分散させてスラリーを調製する工程、
前記スラリーに着色剤又は発色剤を加えて着色スラリー又は発色スラリーを得る工程、
前記着色又は発色スラリーをフローサイトメーターで測定して0.1〜50μmのサイズの着色異物又は発色異物の個数を測定する工程、
前記異物の数が30000個/μg以下の木材パルプ又は前記異物の数が15000個/μg以下の合紙を選別する工程
を含む、TFT液晶ディスプレイ用若しくは有機ELディスプレイ用であるガラス板の合紙用木材パルプ又はTFT液晶ディスプレイ用若しくは有機ELディスプレイ用であるガラス板用合紙の検査方法。 - 前記着色剤又は発色剤が疎水性である、請求項1に記載の検査方法。
- 前記発色剤が蛍光発色剤である、請求項1又は2に記載の検査方法。
- 前記蛍光発色剤がナイルブルー又はナイルレッドである、請求項3に記載の検査方法。
- 前記異物が疎水性物質を含む、請求項1から4のいずれか一項に記載の検査方法。
- 前記疎水性物質がシリコーン、ピッチ、樹脂、ゴム、油及び疎水性異物を吸着したタルクからなる群から選択される、請求項5に記載の検査方法。
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