JP6752587B2 - シート化粧料 - Google Patents
シート化粧料 Download PDFInfo
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- JP6752587B2 JP6752587B2 JP2016033881A JP2016033881A JP6752587B2 JP 6752587 B2 JP6752587 B2 JP 6752587B2 JP 2016033881 A JP2016033881 A JP 2016033881A JP 2016033881 A JP2016033881 A JP 2016033881A JP 6752587 B2 JP6752587 B2 JP 6752587B2
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- 239000002537 cosmetic Substances 0.000 title claims description 53
- 239000007788 liquid Substances 0.000 claims description 43
- 239000000203 mixture Substances 0.000 claims description 43
- -1 polyoxyethylene Polymers 0.000 claims description 33
- 239000004745 nonwoven fabric Substances 0.000 claims description 28
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 27
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 24
- 239000000835 fiber Substances 0.000 claims description 23
- 239000000463 material Substances 0.000 claims description 17
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 12
- 239000000194 fatty acid Substances 0.000 claims description 9
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 8
- 229930195729 fatty acid Natural products 0.000 claims description 8
- 239000012209 synthetic fiber Substances 0.000 claims description 8
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- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 5
- 229940087068 glyceryl caprylate Drugs 0.000 claims description 4
- GHBFNMLVSPCDGN-UHFFFAOYSA-N rac-1-monooctanoylglycerol Chemical compound CCCCCCCC(=O)OCC(O)CO GHBFNMLVSPCDGN-UHFFFAOYSA-N 0.000 claims description 4
- 229940031723 1,2-octanediol Drugs 0.000 claims description 3
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 claims description 3
- 230000002421 anti-septic effect Effects 0.000 description 46
- 125000003976 glyceryl group Chemical group [H]C([*])([H])C(O[H])([H])C(O[H])([H])[H] 0.000 description 14
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- 238000012360 testing method Methods 0.000 description 9
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- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 8
- 241000589517 Pseudomonas aeruginosa Species 0.000 description 7
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- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 description 6
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- OQQOAWVKVDAJOI-UHFFFAOYSA-N (2-dodecanoyloxy-3-hydroxypropyl) dodecanoate Chemical compound CCCCCCCCCCCC(=O)OCC(CO)OC(=O)CCCCCCCCCCC OQQOAWVKVDAJOI-UHFFFAOYSA-N 0.000 description 2
- XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 description 2
- JNAYPSWVMNJOPQ-UHFFFAOYSA-N 2,3-bis(16-methylheptadecanoyloxy)propyl 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCC(C)C)COC(=O)CCCCCCCCCCCCCCC(C)C JNAYPSWVMNJOPQ-UHFFFAOYSA-N 0.000 description 2
- 229920001817 Agar Polymers 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
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- PHYFQTYBJUILEZ-UHFFFAOYSA-N Trioleoylglycerol Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCCCCCCCC)COC(=O)CCCCCCCC=CCCCCCCCC PHYFQTYBJUILEZ-UHFFFAOYSA-N 0.000 description 2
- CMPDPBDUZTUXAD-UHFFFAOYSA-N [3-hydroxy-2-(16-methylheptadecanoyloxy)propyl] 16-methylheptadecanoate Chemical compound CC(C)CCCCCCCCCCCCCCC(=O)OCC(CO)OC(=O)CCCCCCCCCCCCCCC(C)C CMPDPBDUZTUXAD-UHFFFAOYSA-N 0.000 description 2
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- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 229960002446 octanoic acid Drugs 0.000 description 2
- 239000002504 physiological saline solution Substances 0.000 description 2
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 2
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- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- ZORQXIQZAOLNGE-UHFFFAOYSA-N 1,1-difluorocyclohexane Chemical compound FC1(F)CCCCC1 ZORQXIQZAOLNGE-UHFFFAOYSA-N 0.000 description 1
- 229940015975 1,2-hexanediol Drugs 0.000 description 1
- RZRNAYUHWVFMIP-KTKRTIGZSA-N 1-oleoylglycerol Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(O)CO RZRNAYUHWVFMIP-KTKRTIGZSA-N 0.000 description 1
- OBXRIJKJJWWQLE-UHFFFAOYSA-N 2-(2,3-dihydroxypropyl)octanoic acid Chemical compound CCCCCCC(C(O)=O)CC(O)CO OBXRIJKJJWWQLE-UHFFFAOYSA-N 0.000 description 1
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- ODHCTXKNWHHXJC-VKHMYHEASA-M 5-oxo-L-prolinate Chemical compound [O-]C(=O)[C@@H]1CCC(=O)N1 ODHCTXKNWHHXJC-VKHMYHEASA-M 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- 241001331781 Aspergillus brasiliensis Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 description 1
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 229930195714 L-glutamate Natural products 0.000 description 1
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 1
- 239000005639 Lauric acid Substances 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
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- 235000021355 Stearic acid Nutrition 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 239000000159 acid neutralizing agent Substances 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 1
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- 239000005018 casein Substances 0.000 description 1
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
- 235000021240 caseins Nutrition 0.000 description 1
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- 239000002738 chelating agent Substances 0.000 description 1
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- 239000003086 colorant Substances 0.000 description 1
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- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- YSRSBDQINUMTIF-UHFFFAOYSA-N decane-1,2-diol Chemical compound CCCCCCCCC(O)CO YSRSBDQINUMTIF-UHFFFAOYSA-N 0.000 description 1
- ZITKDVFRMRXIJQ-UHFFFAOYSA-N dodecane-1,2-diol Chemical compound CCCCCCCCCCC(O)CO ZITKDVFRMRXIJQ-UHFFFAOYSA-N 0.000 description 1
- 239000002552 dosage form Substances 0.000 description 1
- 231100000507 endocrine disrupting Toxicity 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 210000000245 forearm Anatomy 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 229940074049 glyceryl dilaurate Drugs 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- FHKSXSQHXQEMOK-UHFFFAOYSA-N hexane-1,2-diol Chemical compound CCCCC(O)CO FHKSXSQHXQEMOK-UHFFFAOYSA-N 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 239000012784 inorganic fiber Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 229960004488 linolenic acid Drugs 0.000 description 1
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- WCVRQHFDJLLWFE-UHFFFAOYSA-N pentane-1,2-diol Chemical compound CCCC(O)CO WCVRQHFDJLLWFE-UHFFFAOYSA-N 0.000 description 1
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- 239000000419 plant extract Substances 0.000 description 1
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- 239000002994 raw material Substances 0.000 description 1
- 239000001593 sorbitan monooleate Substances 0.000 description 1
- 235000011069 sorbitan monooleate Nutrition 0.000 description 1
- 229940035049 sorbitan monooleate Drugs 0.000 description 1
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- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
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Landscapes
- Cosmetics (AREA)
Description
〔1〕実質的にエタノールを含有しない液体組成物をシート基材に含浸してなるシート化粧料であって、
前記液体組成物が、下記成分A、成分Bおよび成分Cを含有し、
前記シート基材100質量部に対して、前記液体組成物を400〜1000質量部含浸させることを特徴とするシート化粧料、
成分A:炭素数5〜12の1,2−アルカンジオールの群から選ばれる少なくとも1種
成分B:カプリル酸グリセリル
成分C:1,3−ブチレングリコール
〔2〕前記液体組成物100質量%中の前記成分Aの含有量が0.05〜0.5質量%、前記成分Bの含有量が0.05〜0.5質量%、前記成分Cの含有量が5〜15質量%である前記〔1〕に記載のシート化粧料、
〔3〕前記液体組成物が、成分D:ポリオキシエチレンモノ脂肪酸グリセリル、ポリオキシエチレンジ脂肪酸グリセリルおよびポリオキシエチレントリ脂肪酸グリセリルの群から選ばれる少なくとも1種をさらに含有することを特徴とする前記〔1〕又は〔2〕に記載のシート化粧料、
〔4〕前記シート基材が、再生繊維と合成繊維とから構成されてなる不織布であることを特徴とする前記〔1〕〜〔3〕の何れか一項に記載のシート化粧料
に関する。
表1に記した組成に従い、サンプル番号(1)〜(6)の液状組成物を常法により調製した。尚、配合量は特記しない限り「質量%」を表す。また、配合成分は全て純分に換算した。
レーヨンが70%、ポリエステルが30%の清潔な不織布(坪量(目付):40.0g/m2、シートサイズ:19cm×15cm、Dalian Ruiguang Nonwoven Group製)を四つ折りにしたものを用いた。
表2に記した構成に従い、上記シート基材(不織布)1枚あたりにサンプル1〜6の液体組成物を所定量含浸させて、実施例1〜5および比較例1〜3のシート化粧料を作製した(実施例4、5は参考例1,2とする)。次いで、各シート化粧料を10枚積層してアルミピロー袋内に入れて密封した。試験には、アルミピロー袋からシート化粧料を1枚ずつ取り出して用いた。
供試菌として、Pseudomonas aeruginosa NBRC 13275(緑膿菌)、並びにAspergillus brasiliensis NBRC 9455(クロコウジカビ)を用いた。
緑膿菌については、寒天培地を用いて35℃で培養後、更にブイヨン培地に移植して35℃で培養したものを接種用菌液とした。
クロコウジカビについては、寒天培地を用いて25℃で培養後に2%Tween80(ポリオキシエチレン(20E.O.)ソルビタンモノオレエート)添加の生理食塩水に胞子を懸濁させたものを接種用菌液とした。
各実施例および各比較例のシート化粧料1枚を、容積が100mLの滅菌処理を行ったバイアルに投入した。細菌(緑膿菌)は107CFU/mL、カビ(クロコウジカビ)は105CFU/mLになるように調製した接種用菌液を、上記シート化粧料1枚に含浸量に対して1/10量になるよう均一に接種して密閉し、試験試料とした。細菌を接種した試料については35℃の恒温槽内に該バイアルを保存した。一方、カビを接種した試料については25℃の恒温槽内に該バイアルを保存した。なお、菌数はコロニーカウント法により確認した。
○(良好):10CFU/mL未満の菌数
△(やや不良):10〜1×103CFU/mLの菌数
×(不良):1×103CFU/mLを超える菌数
各実施例および各比較例のシート化粧料をアルミピロー袋から1枚ずつ取り出してもらい、該シート化粧料を前腕内側部に押し当てた後、5往復させて実際に拭き取り操作を行った。拭き取り後の皮膚の刺激感について下記評価基準に従い官能評価した。結果を表4に示す。尚、評価は、官能評価パネル10名で行い、最も人数の多く得られた評価結果を各試料の成績とした。
○(良好):皮膚刺激はないと回答
△(やや不良):僅かに皮膚刺激があると回答
×(不良):明らかな皮膚刺激があると回答
Claims (3)
- 実質的にエタノールを含有しない液体組成物をシート基材に含浸してなるシート化粧料であって、
前記液体組成物が、下記成分A、成分Bおよび成分Cを含有し、
前記液体組成物100質量%中の下記成分Aの含有量が0.1〜0.3質量%、前記成分Bの含有量が0.1〜0.3質量%、前記成分Cの含有量が5〜10質量%であり、
前記シート基材100質量部に対して、前記液体組成物を400〜1000質量部含浸させることを特徴とするシート化粧料。
成分A:1,2−オクタンジオール
成分B:カプリル酸グリセリル
成分C:1,3−ブチレングリコール - 前記液体組成物が、成分D:ポリオキシエチレンモノ脂肪酸グリセリル、ポリオキシエチレンジ脂肪酸グリセリルおよびポリオキシエチレントリ脂肪酸グリセリルの群から選ばれる少なくとも1種をさらに含有すること特徴とする請求項1に記載のシート化粧料。
- 前記シート基材が、再生繊維と合成繊維とから構成されてなる不織布であることを特徴とする請求項1又は2に記載のシート化粧料。
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