JP6621760B2 - 気相ホスゲン化プラントの運転方法 - Google Patents
気相ホスゲン化プラントの運転方法 Download PDFInfo
- Publication number
- JP6621760B2 JP6621760B2 JP2016559280A JP2016559280A JP6621760B2 JP 6621760 B2 JP6621760 B2 JP 6621760B2 JP 2016559280 A JP2016559280 A JP 2016559280A JP 2016559280 A JP2016559280 A JP 2016559280A JP 6621760 B2 JP6621760 B2 JP 6621760B2
- Authority
- JP
- Japan
- Prior art keywords
- phosgene
- zone
- amine
- stream
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/10—Preparation of derivatives of isocyanic acid by reaction of amines with carbonyl halides, e.g. with phosgene
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
- B01J12/005—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor carried out at high temperatures, e.g. by pyrolysis
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/80—Phosgene
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
- C07C263/20—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C265/00—Derivatives of isocyanic acid
- C07C265/14—Derivatives of isocyanic acid containing at least two isocyanate groups bound to the same carbon skeleton
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14162004.7 | 2014-03-27 | ||
| EP14162004 | 2014-03-27 | ||
| PCT/EP2015/056214 WO2015144681A1 (de) | 2014-03-27 | 2015-03-24 | Verfahren zum betreiben einer gasphasenphosgenierungsanlage |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2017512798A JP2017512798A (ja) | 2017-05-25 |
| JP2017512798A5 JP2017512798A5 (enExample) | 2018-05-10 |
| JP6621760B2 true JP6621760B2 (ja) | 2019-12-18 |
Family
ID=50382340
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2016559280A Active JP6621760B2 (ja) | 2014-03-27 | 2015-03-24 | 気相ホスゲン化プラントの運転方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US9840461B2 (enExample) |
| EP (1) | EP3122719B1 (enExample) |
| JP (1) | JP6621760B2 (enExample) |
| KR (1) | KR20160138410A (enExample) |
| CN (1) | CN106458863B (enExample) |
| HU (1) | HUE039109T2 (enExample) |
| WO (1) | WO2015144681A1 (enExample) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3307708B1 (de) * | 2015-06-12 | 2021-12-01 | Covestro Intellectual Property GmbH & Co. KG | Verfahren zur herstellung von diisocyanaten in der gasphase |
| US10364214B1 (en) | 2016-09-01 | 2019-07-30 | Covestro Deutschland Ag | Method for producing isocyanates |
| EP3421426A1 (de) * | 2017-06-29 | 2019-01-02 | Covestro Deutschland AG | Energieeffizientes verfahren zur bereitstellung von phosgen-dampf |
| US11365172B2 (en) | 2017-07-03 | 2022-06-21 | Covestro Deutschland Ag | Production plant for producing a chemical product by reacting H-functional reactants with phosgene, and method for operating same with an interruption to production |
| KR102437607B1 (ko) * | 2018-06-18 | 2022-08-26 | 한화솔루션 주식회사 | 지방족 이소시아네이트의 제조방법 |
| US20230278000A1 (en) * | 2020-07-27 | 2023-09-07 | Basf Se | Phosgene production unit |
| WO2022023246A1 (en) * | 2020-07-27 | 2022-02-03 | Basf Se | Phosgene production unit |
| KR102839457B1 (ko) * | 2020-12-30 | 2025-07-25 | 한화솔루션 주식회사 | 이소시아네이트 화합물의 제조 방법 |
| CN117177940A (zh) * | 2021-04-21 | 2023-12-05 | 巴斯夫欧洲公司 | 光气的制备方法 |
| EP4296261A1 (de) | 2022-06-22 | 2023-12-27 | Covestro Deutschland AG | Verfahren und vorrichtung zur herstellung von isocyanaten |
| EP4296260A1 (de) * | 2022-06-22 | 2023-12-27 | Covestro Deutschland AG | Herstellung spezieller isocyanate durch co-phosgenierung |
| WO2023247522A1 (de) * | 2022-06-22 | 2023-12-28 | Covestro Deutschland Ag | Verfahren zur herstellung von isocyanaten durch phosgenierung eines gemischs (ar)aliphatischer diamine und cycloaliphatischer diamine |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS3510774B1 (enExample) * | 1954-12-01 | 1960-08-08 | ||
| DE3121036A1 (de) * | 1981-05-27 | 1982-12-16 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlicehn herstellung von organischen mono- oder polyisocyanaten |
| DE3714439A1 (de) | 1987-04-30 | 1988-11-10 | Bayer Ag | Verfahren zur herstellung von (cyclo)aliphatischen diisocyanaten |
| FR2723585B1 (fr) | 1994-08-12 | 1996-09-27 | Rhone Poulenc Chimie | Procede de preparation de composes du type polyisocyanates aromatiques en phase gazeuse. |
| DE19942299A1 (de) * | 1999-09-04 | 2001-03-08 | Basf Ag | Verbessertes Verfahren zur Herstellung von Mono- und Oligo-Isocyanaten |
| DE10158160A1 (de) | 2001-11-28 | 2003-06-12 | Basf Ag | Herstellung von Isocyanaten in der Gasphase |
| EP1371634A1 (en) | 2002-06-14 | 2003-12-17 | Bayer Ag | Process for the purification of mixtures of toluenediisocyanate |
| EP1371633A1 (en) | 2002-06-14 | 2003-12-17 | Bayer Ag | Process for the purification of mixtures of toluenediisocyanate incorporating a dividing-wall distillation column |
| DE60214195T2 (de) | 2002-10-22 | 2007-10-04 | Bayer Materialscience Ag | Verfahren zur Reinigung von Diisocyanatotoluol unter Verwendung einer Destillationskolonne mit Trennwand in der Endreinigung |
| DE10349504A1 (de) | 2003-10-23 | 2005-05-25 | Bayer Technology Services Gmbh | Verfahren zur Herstellung von Isocyanaten in der Gasphase |
| DE102005036870A1 (de) | 2005-08-02 | 2007-02-08 | Bayer Materialscience Ag | Verfahren zur Gasphasenphosgenierung |
| DE102005037328A1 (de) | 2005-08-04 | 2007-02-08 | Basf Ag | Verfahren zur Herstellung von Isocyanaten |
| DE102005042392A1 (de) | 2005-09-06 | 2007-03-08 | Basf Ag | Verfahren zur Herstellung von Isocyanaten |
| WO2008055898A1 (de) | 2006-11-07 | 2008-05-15 | Basf Se | Verfahren zur herstellung von isocyanaten |
| CN102850239B (zh) | 2007-01-17 | 2014-07-02 | 巴斯夫欧洲公司 | 制备异氰酸酯的方法 |
| DE102007056511A1 (de) | 2007-11-22 | 2009-05-28 | Bayer Materialscience Ag | Verfahren zur Herstellung aromatischer Diisocyanate in der Gasphase |
| EP2323973B1 (de) * | 2008-08-07 | 2012-03-21 | Basf Se | Verfahren zur herstellung von aromatischen isocyanaten |
| CN102245565B (zh) | 2008-10-15 | 2014-12-31 | 巴斯夫欧洲公司 | 制备异氰酸酯的方法 |
| JP2010153365A (ja) * | 2008-11-19 | 2010-07-08 | Semiconductor Energy Lab Co Ltd | 発光素子、発光装置、電子機器及び照明装置 |
| CN101429139B (zh) * | 2008-12-18 | 2012-11-14 | 宁波万华聚氨酯有限公司 | 二环己基甲烷二异氰酸酯及其中间体的制备方法 |
| JP5771535B2 (ja) * | 2009-03-06 | 2015-09-02 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | イソシアネートの製造方法および製造装置 |
| US9006481B2 (en) | 2009-03-20 | 2015-04-14 | Basf Se | Process and apparatus for preparing isocyanates |
| DE102009032413A1 (de) | 2009-07-09 | 2011-01-13 | Bayer Materialscience Ag | Verfahren zur Herstellung von Isocyanaten |
| WO2011104264A1 (de) * | 2010-02-26 | 2011-09-01 | Basf Se | Verfahren zur herstellung von isocyanaten in der gasphase |
| US8969615B2 (en) | 2011-03-31 | 2015-03-03 | Basf Se | Process for preparing isocyanates |
| US8816126B2 (en) * | 2011-09-02 | 2014-08-26 | Basf Se | Process for preparing isocyanates |
| BR112014004622A8 (pt) * | 2011-09-02 | 2017-06-20 | Basf Se | processo para a preparação de isocianatos |
| WO2013139703A1 (de) | 2012-03-19 | 2013-09-26 | Bayer Intellectual Property Gmbh | Verfahren zur herstellung von isocyanaten |
| HUE034207T2 (hu) | 2013-02-08 | 2018-01-29 | Covestro Deutschland Ag | Eljárás primer amin foszfogenálásával gázfázisban elõállított izocianát elválasztására a foszfogenálás gáz halmazállapotú nyerstermékétõl |
-
2015
- 2015-03-24 EP EP15711536.1A patent/EP3122719B1/de active Active
- 2015-03-24 WO PCT/EP2015/056214 patent/WO2015144681A1/de not_active Ceased
- 2015-03-24 KR KR1020167026160A patent/KR20160138410A/ko not_active Withdrawn
- 2015-03-24 JP JP2016559280A patent/JP6621760B2/ja active Active
- 2015-03-24 US US15/128,179 patent/US9840461B2/en active Active
- 2015-03-24 CN CN201580015894.4A patent/CN106458863B/zh active Active
- 2015-03-24 HU HUE15711536A patent/HUE039109T2/hu unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP3122719B1 (de) | 2018-05-16 |
| EP3122719A1 (de) | 2017-02-01 |
| CN106458863B (zh) | 2020-08-11 |
| WO2015144681A1 (de) | 2015-10-01 |
| JP2017512798A (ja) | 2017-05-25 |
| KR20160138410A (ko) | 2016-12-05 |
| CN106458863A (zh) | 2017-02-22 |
| US20170101367A1 (en) | 2017-04-13 |
| US9840461B2 (en) | 2017-12-12 |
| HUE039109T2 (hu) | 2018-12-28 |
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