JP6153929B2 - 改善された抗微生物性過酸組成物および無菌浄化における低下した温度での使用方法 - Google Patents
改善された抗微生物性過酸組成物および無菌浄化における低下した温度での使用方法 Download PDFInfo
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- JP6153929B2 JP6153929B2 JP2014520251A JP2014520251A JP6153929B2 JP 6153929 B2 JP6153929 B2 JP 6153929B2 JP 2014520251 A JP2014520251 A JP 2014520251A JP 2014520251 A JP2014520251 A JP 2014520251A JP 6153929 B2 JP6153929 B2 JP 6153929B2
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- peroxycarboxylic acid
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- BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 description 1
- WBGSMIRITKHZNA-UHFFFAOYSA-M trisodium;dioxido(oxidooxy)borane Chemical compound [Na+].[Na+].[Na+].[O-]OB([O-])[O-] WBGSMIRITKHZNA-UHFFFAOYSA-M 0.000 description 1
- HOOCZFRHVPMDTH-UHFFFAOYSA-M trisodium;dioxido(oxidooxy)borane;tetrahydrate Chemical compound O.O.O.O.[Na+].[Na+].[Na+].[O-]OB([O-])[O-] HOOCZFRHVPMDTH-UHFFFAOYSA-M 0.000 description 1
- 239000006150 trypticase soy agar Substances 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- ZNSZAXDZPSIPQV-UHFFFAOYSA-N undecaneperoxoic acid Chemical compound CCCCCCCCCCC(=O)OO ZNSZAXDZPSIPQV-UHFFFAOYSA-N 0.000 description 1
- OZHBUVQCJMARBN-UHFFFAOYSA-N undecylamine-n,n-dimethyl-n-oxide Chemical compound CCCCCCCCCCC[N+](C)(C)[O-] OZHBUVQCJMARBN-UHFFFAOYSA-N 0.000 description 1
- 241001515965 unidentified phage Species 0.000 description 1
- AQLJVWUFPCUVLO-UHFFFAOYSA-N urea hydrogen peroxide Chemical class OO.NC(N)=O AQLJVWUFPCUVLO-UHFFFAOYSA-N 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 239000012178 vegetable wax Substances 0.000 description 1
- 230000003253 viricidal effect Effects 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 229940105296 zinc peroxide Drugs 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group; Thio analogues thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
- A01N41/04—Sulfonic acids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Plant Pathology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
- Toxicology (AREA)
Description
機構の理解が本発明の実施に必須ではなく、本発明が任意の特定の作用機構に制限されない一方で、一部の実施形態において、エタノールといったアルコールを使用するペルオキシカルボン酸組成物が、従来の過酸に固有の短鎖の悪臭を除去および/またはマスクでき、また、得られるペルオキシカルボン酸組成物に対して可溶化および/または効果的な利益を提供するということが意図される。本発明のさらなる態様において、(アルコールを用いてエステル化反応を引き起こすこととは対照的に)ペルオキシカルボン酸組成物中でのエステルの使用は、同じ利益を提供し得る。
様々なペルオキシカルボン酸が、本発明に従う組成物に用いられ得る。本発明の一実施形態にしたがって、好適なペルオキシカルボン酸には、本明細書に記載のエステルペルオキシカルボン酸、アルキルエステルペルオキシカルボン酸、スルホペルオキシカルボン酸、および/またはいくつかの異なるペルオキシカルボン酸の組み合わせが挙げられる。本発明の追加の実施形態にしたがって、1つ以上のカルボン酸もまた、本明細書に開示の組成物に使用することができる。
ペルオキシカルボン酸を製造するための例示的方法および装置は、共に「Apparatus and Method for Making a Peroxycarboxylic Acid」と題される、米国特許第7,547,421号、および米国特許出願第12/430,523号に開示され、参照によりそれらの全体が本明細書に明示的に組み込まれる。本発明に従う特定のペルオキシカルボン酸および/またはスルホペルオキシカルボン酸を製造するためのこれらと他の既知の方法および装置は、本発明の範囲内に含まれる。
様々なエステルが、本発明に従うペルオキシカルボン酸組成物中で使用される。エステルは、好ましくはアルキルエステルである。さらなる態様において、エステルは、好ましくはエチルエステルである。さらなる態様において、エステルは、難溶性のエステルである。エステルの組み合わせはまた、ジメチルエステルといったものを用いてもよい。異なる濃度を有するエステルを、本発明に従って用いてもよい。
本発明に従うペルオキシカルボン酸組成物中で、様々なアルコールが使用されてもよい。アルコールは、エステル化を通して悪臭の、低分子量カルボン酸を除去することを含む種々の利益を提供する。加えて、アルコールは、可溶化の利益を提供することができる。アルコールは、好ましくはC2−C6またはC2−C4アルコールといったより低鎖アルコールである。好ましい態様において、アルコールは、tertブチル変性剤エタノールといったSDAエタノール(190プルーフ)である。
本発明の一部の態様において、ペルオキシカルボン酸組成物は、少なくとも1つの酸化剤を含む。ペルオキシカルボン酸組成物中に存在するとき、様々な酸化剤のいずれか、例えば、過酸化水素が、用いられてもよい。酸化剤は、カルボン酸またはスルホン化カルボン酸といった脂肪酸を、ペルオキシカルボン酸またはスルホン化ペルオキシカルボン酸に変換するのに有効な量で存在し得る。一部の実施形態において、酸化剤はまた、抗微生物活性を有する。他の実施形態において、酸化剤は、抗微生物活性を示すのに不十分な量で存在する。
本発明の一部の態様において、ペルオキシカルボン酸組成物は、少なくとも1つの界面活性剤を含む。界面活性剤は、好ましくは、ペルオキシカルボン酸の溶解度を高める、または組成物のpHを保持するために、ペルオキシカルボン酸組成物中に含まれる。本発明の一実施形態にしたがって、界面活性剤は、組成物の相が安定し、単一の高度に活性な水性形態を取りつづけることを保証するために使用できるヒドロトロープカプラーまたは溶解剤である。そのようなヒドロトロープ溶解剤またはカプラーは、相安定性を保持するが、欲しない組成相互作用をもたらさない濃度で使用され得る。
本発明の組成物との使用に適した、好適な非イオン界面活性剤には、アルコキシル化界面活性剤が挙げられる。好適なアルコキシル化界面活性剤には、EO/POコポリマー、キャッピングされたEO/POコポリマー、アルコールアルコキシレート、キャッピングされたアルコールアルコキシレート、それらの混合物等が挙げられる。溶媒としての使用に好適なアルコキシル化界面活性剤には、Pluronicおよび逆Pluronic界面活性剤といったEO/POブロックコポリマー、アルコールアルコキシレート、ならびにPlurafac LF221およびTegoten EC11といったキャッピングされたアルコールアルコキシレート、それらの混合物等が挙げられる。
半極性型の非イオン表面活性薬剤は、本発明の組成物に有用な別のクラスの非イオン界面活性剤である。半極性非イオン界面活性剤には、アミンオキシド、ホスフィンオキシド、スルホキシド、およびそれらのアルコキシル化誘導体が挙げられる。
本組成物での使用に適した陰イオン硫酸塩界面活性剤には、アルキルエーテル硫酸塩、アルキル硫酸塩、直鎖および分枝鎖第1級および第2級アルキル硫酸塩、アルキルエトキシ硫酸塩、脂肪族オレイルグリセロール硫酸塩、アルキルフェノール酸化エチレンエーテル硫酸塩、C5−C17アシル−N−−(C1−C4アルキル)、および−−N−−(C1−C2ヒドロキシアルキル)グルカミン硫酸塩、ならびにアルキルポリグルコシドの硫酸塩といったアルキルポリサッカライドの硫酸塩等が挙げられる。同様に含まれるものは、酸化エチレンおよびノニルフェノールの硫酸塩または縮合物(通常、1つの分子につき1〜6個のオキシエチレン基を有する)といったアルキル硫酸塩、アルキルポリ(エチレンオキシ)エーテル硫酸塩、ならびに芳香族ポリ(エチレンオキシ)硫酸塩である。
両性(amphotericまたはampholytic)界面活性剤は、塩基性親水基と酸性親水基の両方、および有機疎水基を含有する。これらのイオン性の実体は、他のタイプの界面活性剤について本明細書で説明される陰イオンまたは陽イオン基のいずれかであってもよい。塩基性窒素と酸性カルボキシレート基は、塩基性および酸性の親水基として用いられる典型的な官能基である。いくつかの界面活性剤において、スルホン酸塩、硫酸塩、ホスホン酸塩、またはリン酸塩は、負電荷を提供する。
(モノ)酢酸 (ジ)プロピオナート 両性スルホン酸塩
(式中、Rは、約8〜18個の炭素原子を含有する非環式疎水基であり、Mは、陰イオンの荷電を中和するための陽イオン、概して、ナトリウムである)を有する。本組成物に用いられ得る商用に有名なイミダゾリンに由来する両性物質には、例えば、ココアンホプロピオナート、ココアンホカルボキシプロピオナート、ココアンホグリシナート、ココアンホカルボキシグリシナート、ココアンホプロピルスルホン酸塩、およびココアンホカルボキシプロピオン酸が挙げられる。アンホカルボン酸は、脂肪族イミダゾリンから産生されてもよく、アンホジカルボン酸のジカルボン酸官能基はアセト酢酸および/またはジプロピオン酸である。
両性イオン界面活性剤は、両性界面活性剤の一部として考えることができ、そして陰イオン電荷を含んでもよい。両性イオン界面活性剤は、第2級および第3級アミンの誘導体、複素環式第2級および第3級アミンの誘導体、または第4級アンモニウム、第4級ホスホニウム、もしくは第3級スルホニウム化合物の誘導体と大まかに説明することができる。典型的に、両性イオン界面活性剤は、陽性荷電した第4級アンモニウム、または場合によりスルホニウムもしくはホスホニウムイオン、陰性荷電したカルボキシル基、およびアルキル基を含む。両性イオンは、概して、その分子の等電部位中でほぼ同程度までイオン化し、そして陽性−陰性電荷中心の間で強い「内部塩」吸引力を生み出すことができる陽イオン基および陰イオン基を含む。そのような両性イオン合成界面活性剤の例は、脂肪族第4級アンモニウム、ホスホニウム、およびスルホニウム化合物の誘導体を含み、脂肪族ラジカルは、直鎖または分枝であってよく、脂肪族置換基の1つが8〜18個の炭素原子を含有し、かつ、1つが陰イオン性水溶性基、例えば、カルボキシ、スルホン酸塩、硫酸塩、リン酸塩、もしくはホスホン酸塩を含む。ベタインおよびスルタイン(sultaine)界面活性剤は、本明細書中の使用のための例示的な両性イオン界面活性剤である。
一部の実施形態において、本発明の組成物は、他の追加の含有物を含むことができる。本発明の組成物との使用に適した追加の含有物には、酸味料(acidulant)、安定化剤、例えば、キレート剤、金属イオン封鎖剤および/または結晶化阻害剤、緩衝剤、洗浄剤、湿潤剤、消泡剤、増粘剤、発泡剤、過酸化水素還元剤(例えば、カタラーゼ酵素)、固化剤、美観向上剤(aesthetic enhancing agent)(すなわち、着色剤、付臭剤、または香料)、ならびに他の洗剤が挙げられるが、これらに限定されない。これらの追加の含有物は、本発明の組成物と事前に調合されてもよく、または本発明の組成物の添加の前、後、もしくは実質的に同時に系に添加されてもよい。加えて、組成物は、1つ以上の従来の洗剤、例えば、アルカリ性洗浄剤と併用されてもよい。
一部の実施形態において、本発明の組成物は、酸味料を含む。酸味料は、カルボン酸のペルオキシカルボン酸への変換、またはエステル形成のための触媒として作用することができる。酸味料は、約1以下のpHを有する濃縮組成物の形成に有効であり得る。酸味料は、約5、約5以下、約4、約4以下、約3、約3以下、約2、約2以下等のpHを有する使用組成物の形成に有効であり得る。一部の実施形態において、酸味料は、アルカリ性浄化液のpHを約10、約10以下、約9、約9以下、約8、約8以下、約7、約7以下、約6、または約6以下のpHに下げるために使用され得る。一実施形態において、酸味料は、無機酸を含む。好適な無機酸には、硫酸、硫酸水素ナトリウム、リン酸、硝酸、塩酸が挙げられるが、これらに限定されない。一部の実施形態において、酸味料は、有機酸を含む。好適な有機酸には、メタンスルホン酸、エタンスルホン酸、プロパンスルホン酸、ブタンスルホン酸、キシレンスルホン酸、ベンゼンスルホン酸、ギ酸、酢酸、モノ、ジ、もしくはトリハロカルボン酸、ピコリン酸、ジピコリン酸、およびそれらの混合物が挙げられるが、これらに限定されない。一部の実施形態において、本発明の組成物は亜リン酸系の酸を含まないか、あるいは実質的に含まない。
一部の実施形態において、本発明の組成物は、1つ以上の安定化剤を含む。例えば、過酸および過酸化水素を安定させるために、ならびに本発明の組成物中のこの構成要素の早すぎる酸化を防ぐために、安定化剤を使用してもよい。一部の実施形態において、酸性の安定化剤が使用されてもよい。このため、一部の実施形態において、本発明の組成物は、実質的に追加の酸味料を含まなくてもよい。好適な安定化剤には、例えば、キレート剤または金属イオン封鎖剤が挙げられる。好適な金属イオン封鎖剤には、溶液中の金属イオン、特に遷移金属イオンを封鎖する有機キレート化合物が挙げられるが、これらに限定されない。そのような金属イオン封鎖剤には、(酸または可溶性塩の形態のいずれかで)有機アミノまたはヒドロキシポリホスホン酸錯化剤、カルボン酸(例えば、高分子ポリカルボキシレート)、ヒドロキシカルボン酸、アミノカルボン酸、複素環式カルボン酸、例えば、ピリジン−2,6−ジカルボン酸(ジピコリン酸)が挙げられる。
本発明の組成物において同様に有用なものは、湿潤または消泡剤である。湿潤剤は、本発明の抗微生物性組成物の表面接触または浸透作用を増大するように機能する。本発明の組成物に使用され得る湿潤剤は、本発明の組成物の界面活性を高める当分野内で既知のそれら構成要素のうちのいずれかを含む。
本発明の組成物は、種々の既知の増粘剤のいずれかを含んでもよい。好適な増粘剤には、キサンタンゴム、グアールガム、または植物粘液由来の他のゴムといった天然のゴム、アルギナート、デンプン、およびセルロースポリマー(例えば、カルボキシメチルセルロース)といった多糖類ベースの増粘剤、ポリアクリラート増粘剤、およびペクチンといったハイドロコロイド増粘剤が挙げられる。一実施形態において、増粘剤は、物体の表面上に汚染残留物を残さない。例えば、増粘剤またはゲル化剤は、食物または接触面内の他の傷つきやすい製品に適合し得る。概して、本組成物または方法に用いられる増粘剤の濃度は、最終組成物内の所望の粘度によって決定される。しかし、一般的な指針として、本組成物中の増粘剤の粘度は、約0.1重量%〜約5重量%、約0.1重量%〜約1.0重量%、または約0.1重量%〜約0.5重量%の範囲にわたる。これらの値および範囲内のすべての値および範囲が、本発明によって包含されることを理解されたい。
本組成物は、組成物を固体の形態に保持することに関与し得る固化剤を含んでもよい。一部の実施形態において、固化剤は、組成物を固体に形成および/または保持することができる。他の実施形態において、固化剤は、最終的なスルホン化ペルオキシカルボン酸の解放を許容し難く損ずることなく組成物を固化することができる。固化剤は、例えば、中性の不活性特徴を有するか、あるいは本組成物の機能化、安定化もしくは洗浄化に寄与する有機または無機固体化合物を含み得る。好適な固化剤には、固形のポリエチレングリコール(PEG)、固定のポリプロピレングリコール、固形のEO/POブロックコポリマー、アミド、尿素(カルバミドとしても既知である)、非イオン界面活性剤(カプラーと共に用いられ得る)、陰イオン界面活性剤、水溶性にされたデンプン(例えば、酸またはアルカリ処理プロセスを介して)、水溶性にされたセルロース、無機剤、ポリ(無水マレイン酸/メチルビニルエーテル)、ポリメタクリル酸、高い融点をもつ他の一般に機能的であるかまたは不活性な物質、それらの混合物等が挙げられる。
一部の実施形態において、本発明の組成物は、担体を含む。担体は、組成物の他の成分を溶解する、懸濁する、または担持する媒体を提供する。例えば、担体は、スルホン化ペルオキシカルボン酸の可溶化、懸濁化、または産生のための、および平衡混合物を形成するための媒体を提供し得る。担体はまた、物体上で本発明の組成物を供給し、湿らせるように機能し得る。このために、担体は、これらの機能を促進することができる任意の成分(単数または複数)を含有することができる。
本発明のペルオキシカルボン酸組成物は、濃縮組成物および使用組成物の両方を含む。例えば、濃縮組成物は、例えば、水で希釈されて、使用組成物を形成することができる。一実施形態において、濃縮組成物は、物体への適用前に使用溶液に希釈されてもよい。主に経済的な理由から濃縮物が販売されている場合がり、エンドユーザは濃縮物を水または水性の希釈剤で使用溶液に希釈してもよい。
本発明は、改善された抗微生物性過酸組成物を用いる方法を含む。本発明の1つの実施形態にしたがって、方法は、過酸の組成物の抗微生物性または漂白作用を用いる。本発明の組成物を、様々な基質および表面、例えば、織物および硬い表面に対する抗微生物性組成物または漂白組成物として使用することができる。本発明の組成物をまた、抗微生物性消毒剤組成物および/または抗微生物性清浄剤組成物として使用してもよい。本発明の組成物をまた、例えば、エポキシドを含むポリマーの産生に対して使用することができる。本発明の組成物をさらに、製造方法に対して改善した臭気を有するパルプおよび紙の漂白方法において使用してもよい。
本発明の方法および組成物は、低下した温度、例えば、約0℃以上〜約80℃以下、好ましくは約40℃以上〜約60℃以下で、より好ましくは約60℃以下、または約50℃以下の温度で使用することができる。本発明の組成物は、これらの温度で使用される従来の単一過酸組成物と比較して、向上した浄化作用、および特に消毒作用を提供する。
混合ペルオキシカルボン酸組成物の調合物を、ミクロ効果を判定するために分析した。ミクロ効果を犠牲にすることなくコストを改善するためのヒドロトロープを含む従来のカップリング剤を減少させる、または除去すると同時に、抗微生物効果の改善が得られ得るかどうかを判定するために、過スルホン化オレイン酸(PSOA)、オクタン酸、および酢酸を含有する混合ペルオキシカルボン酸組成物を分析した。オクタン酸を可溶化する酢酸およびエタノールを含む他の薬剤の能力を分析した。
組成物A(2000ppmの過酢酸を含有し、業界標準に対する比較に使用される市販のベンチマーク)、試験された他の調合物すべてを、組成物Aと比較して費用効果のよい調合法(例えば、費用効果のよい希釈物)に基づいて希釈した。
組成物B(エステルを含まない(すなわち、アルコールを含まない)調合物)
組成物C(本発明に従うエステル過酸調合物)
組成物D(実験用のエステルを含まない(すなわち、アルコールを含まない)調合物)
組成物E(実験用のエステルを含まない(すなわち、アルコールを含まない)調合物)
1.10mLの栄養ブイヨンを植付け、35℃で24時間培養する。
2.この培養を使用して、6プレートの補正された寒天培地を植え付ける。
500uLで植え付け、プレートの表面に広げる。
3.35℃で12日間、反転して培養する。
4.10mLの冷たい滅菌水で漱ぎ、各プレートを採取する。
5.管を遠心分離機にかけ、冷たい滅菌水中でペレットを再懸濁する。4回繰り返す。
6.プレート毎に、最終量10mLの滅菌水で再懸濁する。
7.使用準備ができるまで、2〜8℃で保存する。
8.使用直前に培養を1:50で希釈する。
追加のミクロ効果データを、例2の手法を使用して評価した。本発明の平衡後組成物を使用して抗微生物効果の改善が得られたかどうかを判定するために、エステル化のためのアルコール、過スルホン化オレイン酸(PSOA)、オクタン酸、および酢酸を含有する混合ペルオキシカルボン酸組成物を、酢酸を含有する市販の対照製品に対して分析した。
無菌ボトル漱ぎに使用される業界標準の単一過酸化学物質と比較して、本発明に従って混合エステル過酸組成物を用いる例3の過酸組成物を使用するミクロ効果試験を実施した。対照は、同じ市販の過酢酸組成物(すなわち、単一過酸種)であった。ミクロ効果を、当業界で死滅が困難な微生物を象徴する内生胞子形成性病原細菌である、アトロフィーウス菌上で実施した。無菌浄化は、微生物の個体群の5ログの減少を達成する効果的な殺胞子剤を必要とする。
[1]
低下した濃度および温度で使用するための改善されたペルオキシカルボン酸組成物であって、
少なくとも1つのC 1 −C 22 カルボン酸と、
少なくとも1つのC 1 −C 22 過カルボン酸と、
過酸化水素と、
界面活性剤またはスルホン化カルボン酸および対応するスルホン化過カルボン酸と、
アルコールと、を含み、前記ペルオキシカルボン酸の濃度が、約2000ppm未満であり、約50℃以下の温度でバチルス種に対して有効である、組成物。
[2]
エステルがアルキルエステルである、項目1に記載の組成物。
[3]
前記過カルボン酸が、アルキルペルオキシカルボン酸、C 2 −C 4 ペルオキシカルボン酸、C 8 −C 12 ペルオキシカルボン酸、エステルペルオキシカルボン酸、アルキルエステルペルオキシカルボン酸、およびそれらの組み合わせから成る群から選択され、前記スルホン化過カルボン酸が、過スルホン化オレイン酸である、項目1に記載の組成物。
[4]
前記組成物が、約0.01重量%〜約50重量%の過カルボン酸、約0.1重量%〜約40重量%のカルボン酸、および約0.1重量%〜約80重量%の過酸化水素を含む、項目1に記載の組成物。
[5]
前記アルコールが、約0.01重量%〜約20重量%の前記組成物を含むエステルにエステル化される、項目4に記載の組成物。
[6]
前記組成物が、前記ペルオキシカルボン酸組成物に関係する悪臭の検出をもたらさない、項目1に記載の組成物。
[7]
前記組成物が、悪臭の発生を伴わずに少なくとも1年間室温で安定している、項目1に記載の組成物。
[8]
前記組成物が、界面活性剤および/または安定化剤をさらに含む、項目1に記載の組成物。
[9]
前記組成物が、冷却安定性である、項目1に記載の組成物。
[10]
低下した濃度および温度で使用するための改善されたペルオキシカルボン酸組成物であって、
酢酸、オクタン酸、スルホン化オレイン酸、およびそれらの組み合わせから成る群から選択される少なくとも1つのC1−C22カルボン酸と、
過酢酸、過オクタン酸、過スルホン化オレイン酸、およびそれらの組み合わせから成る群から選択される少なくとも1つのC1−C22過カルボン酸と、
過酸化水素と、
アルコールと、を含み、
前記組成物が、使用溶液において若干水不溶性であり、
前記組成物が、約2000ppm未満の濃度の前記C1−C22過カルボン酸を提供し、
前記組成物が、約50℃以下の温度でバチルス種に対して有効であり、
前記アルコールが、前記過カルボン酸およびカルボン酸に関係する前記悪臭をマスキングおよび/または誘導体化する快い香りを提供するエステル種を生成する、組成物。
[11]
前記アルコールが、アルキルエステルを生成するために提供された短鎖アルコールである、項目10に記載の組成物。
[12]
前記アルコールが、メタノール、エタノール、プロパノール、ブタノール、ノナノール、ベンジルアルコール、およびそれらの組み合わせから成る群から選択される、項目11に記載の組成物。
[13]
前記アルコールが、エタノールであり、前記過カルボン酸濃度が、約1750ppm未満である、項目11に記載の組成物。
[14]
前記組成物が、ヒドロトロープ界面活性剤を含まない、項目11に記載の組成物。
[15]
低下した温度および濃度で物体上の微生物の個体群を減少させる方法であって、
項目1に記載の混合過カルボン酸組成物を提供することと、
前記混合過カルボン酸組成物に関係する悪臭を検出することなく、約50℃以下の温度で物体を前記混合過カルボン酸組成物と接触させることと、を含む、方法。
[16]
前記物体が、食品加工もしくは製造に関する表面、食物組織、食品包装、医療管理に関する表面、医療もしくは手術機器、織物、水域もしくは水流、気体域もしくは気体の流れ、接客部門に関する表面、工業部門に関する表面、農業に関する表面、獣医学に関する表面、建築に関する表面、食卓用食器、硬い表面包装、またはそれらの組み合わせを含む、項目15に記載の方法。
[17]
前記混合過カルボン酸組成物が、微生物の優れた減少を提供し、約60℃を超える温度で少なくとも2000ppmを超える活性濃度を有する単一の過カルボン酸組成物と比べて低減された蒸気圧を有する、項目15に記載の方法。
[18]
前記エステルが、過カルボン酸組成物に関係する短鎖の悪臭を除去および/またはマスキングすることができるアルキルエステルである、項目15に記載の方法。
[19]
前記過カルボン酸組成物が、微生物の個体群の少なくとも5対数桁の減少に有効な量で存在し、前記微生物は、胞子、細菌、かび、酵母、ウイルス、およびそれらの混合物から成る群から選択され、および前記微生物は、セレウス菌、枯草菌、アトロフィーウス菌(B.atrophaeus)、クロストリジウムディフィシル、クロストリジウムスポロゲネス、黄色ブドウ球菌、メチシリン耐性黄色ブドウ球菌、緑膿菌、大腸菌、およびそれらの混合物から成る群から選択される、項目15に記載の方法。
[20]
微生物の少なくとも5ログの減少を得ることをさらに含む、項目15に記載の方法。
Claims (6)
- 低下した濃度および温度で使用するための改善されたペルオキシカルボン酸組成物であって、
少なくとも1つのC1−C22カルボン酸と、
少なくとも1つのC1−C22ペルオキシカルボン酸と、
過酸化水素と、
スルホン化カルボン酸および対応するスルホン化ペルオキシカルボン酸と、
0.1〜20質量%のアルコールと、を含み、前記ペルオキシカルボン酸の濃度が、2000ppm未満であり、50℃以下の温度でバチルス種に対して有効である、組成物。 - 前記ペルオキシカルボン酸が、アルキルペルオキシカルボン酸、C2−C4ペルオキシカルボン酸、C8−C12ペルオキシカルボン酸、エステルペルオキシカルボン酸、アルキルエステルペルオキシカルボン酸、およびそれらの組み合わせから成る群から選択され、前記スルホン化ペルオキシカルボン酸が、過スルホン化オレイン酸である、請求項1に記載の組成物。
- 前記組成物が、界面活性剤および/または安定化剤をさらに含む、請求項1に記載の組成物。
- 低下した温度および濃度で物体上の微生物の個体群を減少させる方法であって、前記物体は、人間を含まず、
請求項1に記載のペルオキシカルボン酸組成物を提供することと、
前記ペルオキシカルボン酸組成物に関係する悪臭を検出することなく、50℃以下の温度で物体を前記ペルオキシカルボン酸組成物と接触させることと、を含む、方法。 - 前記物体が、食品加工もしくは製造に関する表面、食物組織、食品包装、医療管理に関する表面、医療もしくは手術機器、織物、水域もしくは水流、気体域もしくは気体の流れ、接客部門に関する表面、工業部門に関する表面、農業に関する表面、獣医学に関する表面、建築に関する表面、食卓用食器、硬い表面包装、またはそれらの組み合わせを含む、請求項4に記載の方法。
- 前記ペルオキシカルボン酸組成物が、微生物の個体群の少なくとも5対数桁の減少に有効な量で存在し、前記微生物は、胞子、細菌、かび、酵母、ウイルス、およびそれらの混合物から成る群から選択され、前記微生物は、セレウス菌、枯草菌、アトロフィーウス菌(Bacillus atrophaeus)、クロストリジウムディフィシル、クロストリジウムスポロゲネス、黄色ブドウ球菌、メチシリン耐性黄色ブドウ球菌、緑膿菌、大腸菌、およびそれらの混合物から成る群から選択される、請求項4に記載の方法。
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CN107079924A (zh) | 2017-08-22 |
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JP6092860B2 (ja) | 2017-03-08 |
JP2017075195A (ja) | 2017-04-20 |
EP2731431A4 (en) | 2014-12-31 |
CN103826453A (zh) | 2014-05-28 |
EP2731432A4 (en) | 2014-12-17 |
WO2013009754A2 (en) | 2013-01-17 |
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EP2731432A2 (en) | 2014-05-21 |
JP6431102B2 (ja) | 2018-11-28 |
JP6603259B2 (ja) | 2019-11-06 |
JP2019189636A (ja) | 2019-10-31 |
JP2014522857A (ja) | 2014-09-08 |
CN103826453B (zh) | 2017-04-26 |
US20130018097A1 (en) | 2013-01-17 |
JP6871219B2 (ja) | 2021-05-12 |
EP2731431A2 (en) | 2014-05-21 |
EP2731431B1 (en) | 2019-08-21 |
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