JP5995233B2 - 泡沫状エアゾール組成物 - Google Patents
泡沫状エアゾール組成物 Download PDFInfo
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- JP5995233B2 JP5995233B2 JP2012096955A JP2012096955A JP5995233B2 JP 5995233 B2 JP5995233 B2 JP 5995233B2 JP 2012096955 A JP2012096955 A JP 2012096955A JP 2012096955 A JP2012096955 A JP 2012096955A JP 5995233 B2 JP5995233 B2 JP 5995233B2
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- Prior art keywords
- acid
- poe
- foam
- oil
- fatty acid
- Prior art date
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- Cosmetics (AREA)
Description
、特許文献2に記載のエアゾール型皮膚化粧料では、水溶性高分子を配合することで、泡の安定性を改善しているが、起泡性が不十分であり、また皮膚の洗浄効果も弱いために使用後の感触が十分満足できるものに至っていない。特許文献3及び4に記載の泡沫状皮膚塗布剤では、炭酸ガスと炭化水素混合物を噴射剤として利用することで、ガスの破裂に伴う刺激を低減させてはいるが、拭き取った後や、洗い流した後につっぱり感が強いものであった。また特許文献5に記載のエアゾール型パック化粧料では、アシルアミノ酸型界面活性剤を用いて、シリコーン油を配合することにより、洗い流した後の肌のしっとり感に一定の改善はなされているものの、シリコーン油が起泡性や泡の安定性に影響を与え、洗浄時のマッサージ中に泡が消失してしまうなどの問題があった。
(A)N−アシルアミノ酸型界面活性剤
(B)25℃で液状のポリオキシエチレングリセリン脂肪酸エステル
(C)二酸化炭素
(D)25℃で0.1〜0.3MPaの蒸気圧を有する炭素数が3〜5の炭化水素
−アラニン、N−パーム核脂肪酸メチル−β−アラニン、N−ラウロイルメチル−β−アラニン等のN−アシルアラニンのナトリウム塩、カリウム塩及びトリエタノールアミン塩、N−ヤシ油脂肪酸サルコシン、N−パーム核脂肪酸サルコシン、N−ラウロイルサルコシン等のN−アシルサルコシンのナトリウム塩、カリウム塩及びトリエタノールアミン塩、N−ココイル−L−グルタミン酸、N−ラウロイル−L−グルタミン酸、N−ミリストイル−L−グルタミン酸等のN−アシルグルタミン酸のナトリウム塩、カリウム塩及びトリエタノールアミン塩、N−ヤシ油脂肪酸グリシン、N−パーム核脂肪酸グリシン、N−ラウロイルグリシン、N−ミリストイルグリシン等のN−アシルグリシンのナトリウム塩、カリウム塩及びトリエタノールアミン塩、N−ヤシ油脂肪酸アスパラギン酸、N−パーム核脂肪酸アスパラギン酸、N−ラウロイルアスパラギン酸等のN−アシルアスパラギン酸のナトリウム塩等が挙げられ、これらの中から一種単独又は二種以上を組み合わせて配合することができる。
モノステアレート、POE−グリセリンモノイソステアレート、POE−グリセリントリイソステアレート等のPOEグリセリン脂肪酸エステル類;POEモノオレエート、POEジステアレート、POEモノジオレエート、ジステアリン酸エチレングリコール等のPOE脂肪酸エステル類;POEラウリルエーテル、POEオレイルエーテル、POEステアリルエーテル、POEベヘニルエーテル、POE2−オクチルドデシルエーテル、POEコレスタノールエーテル等のPOEアルキルエーテル類;POEオクチルフェニルエーテル、POEノニルフェニルエーテル、POEジノニルフェニルエーテル等のPOEアルキルフェニルエーテル類;プルロニック(登録商標)等のプルアロニック型類;POE・ポリオキシプロピレン(以下、POPと略す。)セチルエーテル、POE・POP2−デシルテトラデシルエーテル、POE・POPモノブチルエーテル、POE・POP水添ラノリン、POE・POPグリセリンエーテル等のPOE・POPアルキルエーテル類;テトロニック(登録商標)等のテトラPOE・テトラPOPエチレンジアミン縮合物類;POEヒマシ油、POE硬化ヒマシ油、POE硬化ヒマシ油モノイソステアレート、POE硬化ヒマシ油トリイソステアレート、POE硬化ヒマシ油モノピログルタミン酸モノイソステアリン酸ジエステル、POE硬化ヒマシ油マレイン酸等のPOEヒマシ油硬化ヒマシ油誘導体;POEソルビットミツロウ等のPOEミツロウ・ラノリン誘導体;ヤシ油脂肪酸ジエタノールアミド、ラウリン酸モノエタノールアミド、脂肪酸イソプロパノールアミド等のアルカノールアミドのほか、POEプロピレングリコール脂肪酸エステル、POEアルキルアミン、POE脂肪酸アミド、ショ糖脂肪酸エステル、POEノニルフェニルホルムアルデヒド縮合物、アルキルエトキシジメチルアミンオキシド、トリオレイルリン酸などが挙げられる。これら非イオン性界面活性剤の配合量は、耐圧容器内の全組成物中に0.1〜10%、さらに0.5〜3%が特に好ましい。
、ステアリン酸イソセチル、イソステアリン酸イソセチル、12−ヒドロキシステアリル酸コレステリル、ジ−2−エチルヘキシル酸エチレングリコール、ジペンタエリスリトール脂肪酸エステル、モノイソステアリン酸N−アルキルグリコール、ジカプリン酸ネオペンチルグリコール、リンゴ酸ジイソステアリル、ジ−2−ヘプチルウンデカン酸グリセリン、トリ−2−エチルヘキシル酸トリメチロールプロパン、トリイソステアリン酸トリメチロールプロパン、テトラ−2−エチルヘキシル酸ペンタンエリスリトール、トリー2−エチルヘキシル酸グリセリン、トリイソステアリン酸トリメチロールプロパン、セチル2−エチルヘキサノエート、2−エチルヘキシルパルミテート、トリミリスチン酸グリセリン、トリ−2−ヘプチルウンデカン酸グリセライド、ヒマシ油脂肪酸メチルエステル、オレイン酸オイル、アセトグリセライド、パルミチン酸2−ヘプチルウンデシル、アジピン酸ジイソブチル、N−ラウロイル−L−グルタミン酸−2−クチルドデシルエステル、アジピン酸ジ−2−ヘプチルウンデシル、エチルラウレート、セバチン酸ジ−2−エチルヘキシル、ミリスチン酸2−ヘキシルデシル、パルミチン酸2−ヘキシルデシル、アジピン酸2−ヘキシルデシル、セバチン酸ジイソプロピル、コハク酸2−エチルヘキシル、酢酸エチル、酢酸ブチル、酢酸アミル、クエン酸トリエチル、クロタミトン(C13H17NO)などが例示される。シリコーンとしては、ジメチルポリシロキサン、メチルフェニルポリシロキサン、メチルハイドロジェンポリシロキサン等の鎖状ポリシロキサン;デカメチルポリシロキサン、ドデカメチルポリシロキサン、テトラメチルテトラハイドロジェンポリシロキサン等の環状ポリシロキサン;3次元網目構造を形成しているシリコ−ン樹脂、シリコーンゴムなどが例示される。
このとき、必要に応じて、他の噴射ガスを充填することも可能である。
常法により調整した実施例及び比較例の泡沫状エアゾール組成物を、25℃で1週間保存後に、50mLのガラス製容器内に噴射し、50mLの泡の質量を測り、単位体積(1cm3)あたりの密度を算出し、以下の基準で判定した。尚、密度が小さいほど、起泡性が高いことを示す。
◎:密度が0.15g/mL未満
〇:密度が0.15g/mL以上、0.2g/mL未満
△:密度が0.2g/mL以上、0.3g/mL未満
×:密度が0.3g/mL以上
常法により調整した実施例及び比較例の泡沫状エアゾール組成物を、25℃で1週間保存後に、100mLのメスシリンダー内に噴射し、2分間放置後の体積を測り、泡の安定性を以下の基準で判定した。
◎:泡の体積が90mL以上
〇:泡の体積が80mL以上、90mL未満
△:泡の体積が70mL以上、80mL未満
×:泡の体積が70mL未満
10名の専門パネルを用いて、常法により調製した実施例及び比較例の泡沫状エアゾール組成物を頬の部位に塗布した。塗布後3分間マッサージを行い、ぬるま湯にて洗い流した。その後10分放置して乾燥させた。その後、被験者本人が1点から5点の5段階にて、マッサージのしやすさ、洗浄効果、洗い上がりのつっぱりのなさ、しっとり感について官能評価を行い、平均評価点を算出した。評価基準は以下の通りである。
◎:平均点が4.0以上
〇:平均点が3.0以上、4.0未満
△:平均点が2.0以上、3.0未満
×:平均点が2.0未満
表1〜3に示した泡沫状エアゾール組成物を調整し、前記各試験を実施した。その結果を
表1〜3に併せて示す。
Claims (3)
- 次の成分(A)〜(D)を含有し、成分(A)の含有量が耐圧容器内の全組成物中に2〜7質量%、かつ成分(B)の含有量が耐圧容器内の全組成物中に0.5〜10質量%であることを特徴とする泡沫状エアゾール組成物。
(A)N−アシルアミノ酸型界面活性剤
(B)25℃で液状のポリオキシエチレングリセリン脂肪酸エステル
(C)二酸化炭素及び
(D)25℃で0.1〜0.3MPaの蒸気圧を有する炭素数が3〜5の炭化水素 - さらに成分(E)多価アルコールを含有する請求項1記載の泡沫状エアゾール組成物。
- 成分(C)及び(D)の質量比(C):(D)が1:9〜1:4である請求項1又は2記載の泡沫状エアゾール組成物。
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