JP5934228B2 - 多層カーボネートシート - Google Patents
多層カーボネートシート Download PDFInfo
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- JP5934228B2 JP5934228B2 JP2013535283A JP2013535283A JP5934228B2 JP 5934228 B2 JP5934228 B2 JP 5934228B2 JP 2013535283 A JP2013535283 A JP 2013535283A JP 2013535283 A JP2013535283 A JP 2013535283A JP 5934228 B2 JP5934228 B2 JP 5934228B2
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- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 title description 40
- 239000004417 polycarbonate Substances 0.000 claims description 51
- 229920000515 polycarbonate Polymers 0.000 claims description 51
- 238000001125 extrusion Methods 0.000 claims description 32
- 239000000155 melt Substances 0.000 claims description 19
- 238000000034 method Methods 0.000 claims description 19
- 238000004519 manufacturing process Methods 0.000 claims description 12
- 238000005227 gel permeation chromatography Methods 0.000 claims description 4
- 238000002844 melting Methods 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- 239000000203 mixture Substances 0.000 description 57
- 239000000975 dye Substances 0.000 description 51
- -1 PETG Polymers 0.000 description 46
- 239000000654 additive Substances 0.000 description 42
- 229920000642 polymer Polymers 0.000 description 32
- 125000003118 aryl group Chemical group 0.000 description 29
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- 239000002245 particle Substances 0.000 description 16
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 description 13
- 229920000728 polyester Polymers 0.000 description 13
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- 230000000996 additive effect Effects 0.000 description 11
- 239000002216 antistatic agent Substances 0.000 description 11
- 239000012760 heat stabilizer Substances 0.000 description 11
- 239000003963 antioxidant agent Substances 0.000 description 10
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 10
- 239000006085 branching agent Substances 0.000 description 9
- 239000004594 Masterbatch (MB) Substances 0.000 description 8
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 8
- 239000003795 chemical substances by application Substances 0.000 description 8
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- 229920001169 thermoplastic Polymers 0.000 description 8
- XBDQKXXYIPTUBI-UHFFFAOYSA-N Propionic acid Substances CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 7
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- 239000000126 substance Substances 0.000 description 7
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 6
- 239000002253 acid Substances 0.000 description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- 239000003063 flame retardant Substances 0.000 description 6
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- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 5
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- 125000001931 aliphatic group Chemical group 0.000 description 5
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- 229920005601 base polymer Polymers 0.000 description 5
- KKEYFWRCBNTPAC-UHFFFAOYSA-N benzene-dicarboxylic acid Natural products OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 5
- 238000009413 insulation Methods 0.000 description 5
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- 229920002545 silicone oil Polymers 0.000 description 5
- JLZIIHMTTRXXIN-UHFFFAOYSA-N 2-(2-hydroxy-4-methoxybenzoyl)benzoic acid Chemical compound OC1=CC(OC)=CC=C1C(=O)C1=CC=CC=C1C(O)=O JLZIIHMTTRXXIN-UHFFFAOYSA-N 0.000 description 4
- IYAZLDLPUNDVAG-UHFFFAOYSA-N 2-(benzotriazol-2-yl)-4-(2,4,4-trimethylpentan-2-yl)phenol Chemical compound CC(C)(C)CC(C)(C)C1=CC=C(O)C(N2N=C3C=CC=CC3=N2)=C1 IYAZLDLPUNDVAG-UHFFFAOYSA-N 0.000 description 4
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 4
- 230000003078 antioxidant effect Effects 0.000 description 4
- QQVIHTHCMHWDBS-UHFFFAOYSA-N isophthalic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=C1 QQVIHTHCMHWDBS-UHFFFAOYSA-N 0.000 description 4
- QUAMTGJKVDWJEQ-UHFFFAOYSA-N octabenzone Chemical compound OC1=CC(OCCCCCCCC)=CC=C1C(=O)C1=CC=CC=C1 QUAMTGJKVDWJEQ-UHFFFAOYSA-N 0.000 description 4
- 230000003287 optical effect Effects 0.000 description 4
- NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 description 4
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 4
- 229920000573 polyethylene Polymers 0.000 description 4
- 239000004926 polymethyl methacrylate Substances 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 150000005846 sugar alcohols Polymers 0.000 description 4
- 239000003017 thermal stabilizer Substances 0.000 description 4
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 4
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 3
- CVSXFBFIOUYODT-UHFFFAOYSA-N 178671-58-4 Chemical compound C=1C=CC=CC=1C(C=1C=CC=CC=1)=C(C#N)C(=O)OCC(COC(=O)C(C#N)=C(C=1C=CC=CC=1)C=1C=CC=CC=1)(COC(=O)C(C#N)=C(C=1C=CC=CC=1)C=1C=CC=CC=1)COC(=O)C(C#N)=C(C=1C=CC=CC=1)C1=CC=CC=C1 CVSXFBFIOUYODT-UHFFFAOYSA-N 0.000 description 3
- XKZQKPRCPNGNFR-UHFFFAOYSA-N 2-(3-hydroxyphenyl)phenol Chemical compound OC1=CC=CC(C=2C(=CC=CC=2)O)=C1 XKZQKPRCPNGNFR-UHFFFAOYSA-N 0.000 description 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 3
- 238000007792 addition Methods 0.000 description 3
- 150000008052 alkyl sulfonates Chemical class 0.000 description 3
- 239000001000 anthraquinone dye Substances 0.000 description 3
- 125000004432 carbon atom Chemical group C* 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- 238000009792 diffusion process Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 150000002430 hydrocarbons Chemical class 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 239000000314 lubricant Substances 0.000 description 3
- 125000001434 methanylylidene group Chemical group [H]C#[*] 0.000 description 3
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
- SSDSCDGVMJFTEQ-UHFFFAOYSA-N octadecyl 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 SSDSCDGVMJFTEQ-UHFFFAOYSA-N 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 239000012188 paraffin wax Substances 0.000 description 3
- DGBWPZSGHAXYGK-UHFFFAOYSA-N perinone Chemical compound C12=NC3=CC=CC=C3N2C(=O)C2=CC=C3C4=C2C1=CC=C4C(=O)N1C2=CC=CC=C2N=C13 DGBWPZSGHAXYGK-UHFFFAOYSA-N 0.000 description 3
- 150000002989 phenols Chemical class 0.000 description 3
- XYFCBTPGUUZFHI-UHFFFAOYSA-O phosphonium Chemical compound [PH4+] XYFCBTPGUUZFHI-UHFFFAOYSA-O 0.000 description 3
- 229920005644 polyethylene terephthalate glycol copolymer Polymers 0.000 description 3
- 235000013824 polyphenols Nutrition 0.000 description 3
- 229920001296 polysiloxane Polymers 0.000 description 3
- 235000019260 propionic acid Nutrition 0.000 description 3
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 3
- 230000005855 radiation Effects 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 229920001187 thermosetting polymer Polymers 0.000 description 3
- KPZGRMZPZLOPBS-UHFFFAOYSA-N 1,3-dichloro-2,2-bis(chloromethyl)propane Chemical compound ClCC(CCl)(CCl)CCl KPZGRMZPZLOPBS-UHFFFAOYSA-N 0.000 description 2
- IBABXJRXGSAJLQ-UHFFFAOYSA-N 1,4-bis(2,6-diethyl-4-methylanilino)anthracene-9,10-dione Chemical compound CCC1=CC(C)=CC(CC)=C1NC(C=1C(=O)C2=CC=CC=C2C(=O)C=11)=CC=C1NC1=C(CC)C=C(C)C=C1CC IBABXJRXGSAJLQ-UHFFFAOYSA-N 0.000 description 2
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 2
- QHZLMUACJMDIAE-UHFFFAOYSA-N 1-monopalmitoylglycerol Chemical compound CCCCCCCCCCCCCCCC(=O)OCC(O)CO QHZLMUACJMDIAE-UHFFFAOYSA-N 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 2
- BSWWXRFVMJHFBN-UHFFFAOYSA-N 2,4,6-tribromophenol Chemical compound OC1=C(Br)C=C(Br)C=C1Br BSWWXRFVMJHFBN-UHFFFAOYSA-N 0.000 description 2
- LEVFXWNQQSSNAC-UHFFFAOYSA-N 2-(4,6-diphenyl-1,3,5-triazin-2-yl)-5-hexoxyphenol Chemical compound OC1=CC(OCCCCCC)=CC=C1C1=NC(C=2C=CC=CC=2)=NC(C=2C=CC=CC=2)=N1 LEVFXWNQQSSNAC-UHFFFAOYSA-N 0.000 description 2
- BBITXNWQALLODC-UHFFFAOYSA-N 2-[4-(4-oxo-3,1-benzoxazin-2-yl)phenyl]-3,1-benzoxazin-4-one Chemical compound C1=CC=C2C(=O)OC(C3=CC=C(C=C3)C=3OC(C4=CC=CC=C4N=3)=O)=NC2=C1 BBITXNWQALLODC-UHFFFAOYSA-N 0.000 description 2
- VEORPZCZECFIRK-UHFFFAOYSA-N 3,3',5,5'-tetrabromobisphenol A Chemical compound C=1C(Br)=C(O)C(Br)=CC=1C(C)(C)C1=CC(Br)=C(O)C(Br)=C1 VEORPZCZECFIRK-UHFFFAOYSA-N 0.000 description 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 2
- 239000004429 Calibre Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- 239000006057 Non-nutritive feed additive Substances 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- YGYAWVDWMABLBF-UHFFFAOYSA-N Phosgene Chemical compound ClC(Cl)=O YGYAWVDWMABLBF-UHFFFAOYSA-N 0.000 description 2
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- 239000004743 Polypropylene Substances 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 239000007983 Tris buffer Substances 0.000 description 2
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 2
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 description 2
- LRTTZMZPZHBOPO-UHFFFAOYSA-N [B].[B].[Hf] Chemical compound [B].[B].[Hf] LRTTZMZPZHBOPO-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000009825 accumulation Methods 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- 229940045714 alkyl sulfonate alkylating agent Drugs 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 229910052787 antimony Inorganic materials 0.000 description 2
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- 235000010290 biphenyl Nutrition 0.000 description 2
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- FQUNFJULCYSSOP-UHFFFAOYSA-N bisoctrizole Chemical compound N1=C2C=CC=CC2=NN1C1=CC(C(C)(C)CC(C)(C)C)=CC(CC=2C(=C(C=C(C=2)C(C)(C)CC(C)(C)C)N2N=C3C=CC=CC3=N2)O)=C1O FQUNFJULCYSSOP-UHFFFAOYSA-N 0.000 description 2
- 239000001045 blue dye Substances 0.000 description 2
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- 230000015556 catabolic process Effects 0.000 description 2
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- 150000001805 chlorine compounds Chemical class 0.000 description 2
- WDECIBYCCFPHNR-UHFFFAOYSA-N chrysene Chemical compound C1=CC=CC2=CC=C3C4=CC=CC=C4C=CC3=C21 WDECIBYCCFPHNR-UHFFFAOYSA-N 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
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- VPUGDVKSAQVFFS-UHFFFAOYSA-N coronene Chemical compound C1=C(C2=C34)C=CC3=CC=C(C=C3)C4=C4C3=CC=C(C=C3)C4=C2C3=C1 VPUGDVKSAQVFFS-UHFFFAOYSA-N 0.000 description 2
- ZYGHJZDHTFUPRJ-UHFFFAOYSA-N coumarin Chemical compound C1=CC=C2OC(=O)C=CC2=C1 ZYGHJZDHTFUPRJ-UHFFFAOYSA-N 0.000 description 2
- MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 description 2
- GHVNFZFCNZKVNT-UHFFFAOYSA-N decanoic acid Chemical compound CCCCCCCCCC(O)=O GHVNFZFCNZKVNT-UHFFFAOYSA-N 0.000 description 2
- 238000006731 degradation reaction Methods 0.000 description 2
- 150000001991 dicarboxylic acids Chemical class 0.000 description 2
- 238000002845 discoloration Methods 0.000 description 2
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 description 2
- UKMSUNONTOPOIO-UHFFFAOYSA-N docosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCC(O)=O UKMSUNONTOPOIO-UHFFFAOYSA-N 0.000 description 2
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 238000004049 embossing Methods 0.000 description 2
- 239000000945 filler Substances 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 2
- 125000004464 hydroxyphenyl group Chemical group 0.000 description 2
- VKOBVWXKNCXXDE-UHFFFAOYSA-N icosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCC(O)=O VKOBVWXKNCXXDE-UHFFFAOYSA-N 0.000 description 2
- 229910052738 indium Inorganic materials 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
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- 239000006082 mold release agent Substances 0.000 description 2
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- 239000002105 nanoparticle Substances 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- BDJRBEYXGGNYIS-UHFFFAOYSA-N nonanedioic acid Chemical compound OC(=O)CCCCCCCC(O)=O BDJRBEYXGGNYIS-UHFFFAOYSA-N 0.000 description 2
- UTOPWMOLSKOLTQ-UHFFFAOYSA-N octacosanoic acid Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCC(O)=O UTOPWMOLSKOLTQ-UHFFFAOYSA-N 0.000 description 2
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 2
- 125000002080 perylenyl group Chemical group C1(=CC=C2C=CC=C3C4=CC=CC5=CC=CC(C1=C23)=C45)* 0.000 description 2
- CSHWQDPOILHKBI-UHFFFAOYSA-N peryrene Natural products C1=CC(C2=CC=CC=3C2=C2C=CC=3)=C3C2=CC=CC3=C1 CSHWQDPOILHKBI-UHFFFAOYSA-N 0.000 description 2
- ZQBAKBUEJOMQEX-UHFFFAOYSA-N phenyl salicylate Chemical compound OC1=CC=CC=C1C(=O)OC1=CC=CC=C1 ZQBAKBUEJOMQEX-UHFFFAOYSA-N 0.000 description 2
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
- AQSJGOWTSHOLKH-UHFFFAOYSA-N phosphite(3-) Chemical class [O-]P([O-])[O-] AQSJGOWTSHOLKH-UHFFFAOYSA-N 0.000 description 2
- IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 description 2
- QWYZFXLSWMXLDM-UHFFFAOYSA-M pinacyanol iodide Chemical compound [I-].C1=CC2=CC=CC=C2N(CC)C1=CC=CC1=CC=C(C=CC=C2)C2=[N+]1CC QWYZFXLSWMXLDM-UHFFFAOYSA-M 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 239000004431 polycarbonate resin Substances 0.000 description 2
- 229920005668 polycarbonate resin Polymers 0.000 description 2
- 239000002952 polymeric resin Substances 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 150000008442 polyphenolic compounds Chemical class 0.000 description 2
- 229920001155 polypropylene Polymers 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- BBEAQIROQSPTKN-UHFFFAOYSA-N pyrene Chemical compound C1=CC=C2C=CC3=CC=CC4=CC=C1C2=C43 BBEAQIROQSPTKN-UHFFFAOYSA-N 0.000 description 2
- CYIDZMCFTVVTJO-UHFFFAOYSA-N pyromellitic acid Chemical compound OC(=O)C1=CC(C(O)=O)=C(C(O)=O)C=C1C(O)=O CYIDZMCFTVVTJO-UHFFFAOYSA-N 0.000 description 2
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- QCLVFLIIJODTJU-UHFFFAOYSA-N triethyl(octyl)phosphanium Chemical compound CCCCCCCC[P+](CC)(CC)CC QCLVFLIIJODTJU-UHFFFAOYSA-N 0.000 description 1
- ITMCEJHCFYSIIV-UHFFFAOYSA-N triflic acid Chemical compound OS(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-N 0.000 description 1
- NVQBNLRCSAEYHZ-UHFFFAOYSA-N trimethyl(octyl)phosphanium Chemical compound CCCCCCCC[P+](C)(C)C NVQBNLRCSAEYHZ-UHFFFAOYSA-N 0.000 description 1
- BZVJOYBTLHNRDW-UHFFFAOYSA-N triphenylmethanamine Chemical compound C=1C=CC=CC=1C(C=1C=CC=CC=1)(N)C1=CC=CC=C1 BZVJOYBTLHNRDW-UHFFFAOYSA-N 0.000 description 1
- WGKLOLBTFWFKOD-UHFFFAOYSA-N tris(2-nonylphenyl) phosphite Chemical compound CCCCCCCCCC1=CC=CC=C1OP(OC=1C(=CC=CC=1)CCCCCCCCC)OC1=CC=CC=C1CCCCCCCCC WGKLOLBTFWFKOD-UHFFFAOYSA-N 0.000 description 1
- 239000001018 xanthene dye Substances 0.000 description 1
- NAWDYIZEMPQZHO-UHFFFAOYSA-N ytterbium Chemical compound [Yb] NAWDYIZEMPQZHO-UHFFFAOYSA-N 0.000 description 1
- 229910052727 yttrium Inorganic materials 0.000 description 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- 229910052726 zirconium Inorganic materials 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
Images
Classifications
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04C—STRUCTURAL ELEMENTS; BUILDING MATERIALS
- E04C2/00—Building elements of relatively thin form for the construction of parts of buildings, e.g. sheet materials, slabs, or panels
- E04C2/02—Building elements of relatively thin form for the construction of parts of buildings, e.g. sheet materials, slabs, or panels characterised by specified materials
- E04C2/10—Building elements of relatively thin form for the construction of parts of buildings, e.g. sheet materials, slabs, or panels characterised by specified materials of wood, fibres, chips, vegetable stems, or the like; of plastics; of foamed products
- E04C2/20—Building elements of relatively thin form for the construction of parts of buildings, e.g. sheet materials, slabs, or panels characterised by specified materials of wood, fibres, chips, vegetable stems, or the like; of plastics; of foamed products of plastics
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29D—PRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE
- B29D24/00—Producing articles with hollow walls
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/02—Aliphatic polycarbonates
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04B—GENERAL BUILDING CONSTRUCTIONS; WALLS, e.g. PARTITIONS; ROOFS; FLOORS; CEILINGS; INSULATION OR OTHER PROTECTION OF BUILDINGS
- E04B1/00—Constructions in general; Structures which are not restricted either to walls, e.g. partitions, or floors or ceilings or roofs
- E04B1/62—Insulation or other protection; Elements or use of specified material therefor
- E04B1/74—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls
- E04B1/76—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to heat only
- E04B1/7608—Heat, sound or noise insulation, absorption, or reflection; Other building methods affording favourable thermal or acoustical conditions, e.g. accumulating of heat within walls specifically with respect to heat only comprising a prefabricated insulating layer, disposed between two other layers or panels
-
- E—FIXED CONSTRUCTIONS
- E04—BUILDING
- E04C—STRUCTURAL ELEMENTS; BUILDING MATERIALS
- E04C2/00—Building elements of relatively thin form for the construction of parts of buildings, e.g. sheet materials, slabs, or panels
- E04C2/54—Slab-like translucent elements
- E04C2/543—Hollow multi-walled panels with integrated webs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/24—Structurally defined web or sheet [e.g., overall dimension, etc.]
- Y10T428/24479—Structurally defined web or sheet [e.g., overall dimension, etc.] including variation in thickness
- Y10T428/2457—Parallel ribs and/or grooves
Landscapes
- Engineering & Computer Science (AREA)
- Architecture (AREA)
- Structural Engineering (AREA)
- Civil Engineering (AREA)
- Physics & Mathematics (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Mechanical Engineering (AREA)
- Electromagnetism (AREA)
- Acoustics & Sound (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Laminated Bodies (AREA)
- Extrusion Moulding Of Plastics Or The Like (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Description
xは、各場合において、互いに独立して0、1または2を示し、
pは、0または1を示し、
RCおよびRdは、それぞれ互いに独立しており、各X1に対して個別に選択可能であり、水素またはC1〜C6−アルキルであり、適切には水素、メチルまたはエチルであり、
X1は、炭素を表し、および
mは4〜7の整数、場合によっては4または5であり、ただし、RCおよびRdが少なくとも1つのX1原子のアルキルを同時に表すことを条件とする。
本発明の多層製品の遮熱特性を改善するために適切なIR吸収剤は、金属ホウ化物、セシウムタングステン酸化物、アンチモンをドープした酸化錫粒子、In、Ga、Al、ならびにSbから選択された少なくとも1種の元素を含む酸化亜鉛粒子、スズをドープしたインジウム酸化物粒子、本発明のカーボネート組成物に混ぜ合わせることができるフタロシアニン系組成物、ナフタロシアニン系組成物、硫化銅、もしくは銅イオン化合物等の他の有機または無機IR吸収剤である。
組成物は、1種または複数のUV吸収添加剤をさらに備えることができる。適切なUV吸収添加剤は、シアノアクリル酸化合物、トリアジン化合物、ベンゾフェノン化合物、例えば、2,4−ジヒドロキシベンゾフェノン、2−ヒドロキシ−4−メトキシベンゾフェノン、2−ヒドロキシ−4−n−オクトキシベンゾフェノン、4−ドデシルオキシ−2−ヒドロキシベンゾフェノン、2−ヒドロキシ−4−オクタデシルオキシベンゾフェノン、2,2’−ジヒドロキシ−4−メトキシベンゾフェノン、2,2’,4,4’−テトラヒドロキシベンゾフェノン、2−ヒドロキシ−4−メトキシ−5−スルホベンゾフェノン、2−ヒドロキシ−4−メトキシ−2’−カルボキシベンゾフェノン、2,2’−ジヒドロキシ−4,4’−ジメトキシ−5−スルホベンゾフェノン、2−ヒドロキシ−4−(2−ヒドロキシ−3−メチルアリールオキシ)プロポキシベンゾフェノン、2−ヒドロキシ−4−クロロベンゾフェノン等;ベンゾトリアゾール化合物、例えば、2−(2−ヒドロキシ−5−tert−オクチルフェニル)ベンゾトリアゾール、2−ヒドロキシ−4−n−オクトキシベンゾフェノン2−(2−ヒドロキシ−5−メチルフェニル)ベンゾトリアゾール、2−(2−ヒドロキシ−3’,5’−ジ−tert−ブチルフェニル)ベンゾトリアゾール、および2−(2−ヒドロキシ−X−tert,ブチル−5’−メチルフェニル)ベンゾトリアゾール等;サリチル酸塩化合物、例えば、サリチル酸フェニル、サリチル酸カルボキシフェニル、サリチル酸p−オクチルフェニル、サリチル酸ストロンチウム、サリチル酸p−tert−ブチルフェニル、サリチル酸メチル、サリチル酸ドデシル等;ならびにレソルシノールモノベンゾエート、2−エチルヘキシル−2−シアノ、3−フェニルシンナマート、2−エチルヘキシル−2−シアノ−3,3−ジフェニルアクリレート、エチル−2−シアノ−3,3−ジフェニルアクリレート、2−2’−チオビス(4−t−オクチルフェノラート)−1−n−ブチルアミン等の他の紫外線吸収剤、または上記UV吸収添加剤の少なくとも1種を含む組合せである。商業的に入手可能なUV吸収添加剤は、CibaSpecialtyChemicalsから商業的に入手可能なTINUVINTM(商標)234、TINUVIN329、TINUVIN350およびTINUVIN360;CytecIndustriesから入手可能なCYASORB(商標)UV吸収添加剤、例えば、2−(2H−ベンゾトリアゾール−2−イル)−4−(1,1,3,3−テトラメチルブチル)−フェノール(CYASORB5411);2−ヒドロキシ−4−n−オクチルオキシベンゾフェノン(CYASORB531);2−[4,6−ビス(2,4−ジメチルフェニル)−1,3,5−トリアジン−2−イル]−5−(オクチルオキシ)−フェノール(CYASORB1164);2,2’−(1,4−フェニレン)ビス(4H−3,1−ベンゾオキサジン−4−オン)(CYASORB UV−3638);1,3−ビス[(2−シアノ−3,3−ジフェニルアクリロイル)オキシ]−2,2−ビス[[(2−シアノ−3,3−ジフェニル−アクリロイル)オキシ]メチル]プロパン(UVINUL(商標)3030);2,2’−(1,4−フェニレン)ビス(4H−3,1−ベンゾオキサジン−4−オン);1,3−ビス[(2−シアノ−3,3−ジフェニルアクリロイル)オキシ]−2,2−ビス[[(2−シアノ−3,3−ジフェニル−アクリロイル)オキシ]メチル]プロパン;2,2’−メチレン−ビス−(6−{2H−ベンゾトリアゾール−2−イル}−4−{1,1,3,3−テトラメチルブチル}フェノール)(AdekaArgus製LA−31);または2−(4,6−ジフェニル−1,3,5−トリアジン−2−イル)−5−ヘキシルオキシフェノール(CibaGeigy製Tinuvin1577)。押出によって成形される製品のためには、BASFから商業的に入手可能なUVINUL3030が、その低い揮発性のために、特に有用である。
組成物は、IR光と無機赤外線遮蔽添加剤との相互作用によってもたらされた温度上昇を補償するために1種または複数の熱安定剤を含むことができる。さらに、熱安定剤の添加は溶融混合等の加工作業中に材料を保護する。通常は、無機赤外線遮蔽添加剤を含む熱可塑性ポリマーを備える製品は、光に曝されたときに約20℃までの温度上昇を経験する可能性がある。組成物への熱安定剤の添加は、長期老化特性を改善し、製品の寿命を延ばす。
本発明において使用することができる酸化防止剤の例には、ヒンダードフェノール系酸化防止剤が含まれる。ヒンダードフェノール系酸化防止剤の具体例には、テトラキス[3−(3,5−ジ−t−ブチル−4−ヒドロキシフェニル)プロピオン酸]ペンタエリトリチル、3−(3,5−ジ−t−ブチル−4−ヒドロキシフェニル)プロピオン酸オクタデシル、チオ−ジエチレンビス[3−(3,5−ジ−t−ブチル−4−ヒドロキシフェニル)プロピオナート]、N,N’−ヘキサン−1,6−ジ−イル−ビス[3−(3,5−ジ−t−ブチル−4−ヒドロキシフェニルプロピオンアミド)、2,4−ジメチル−6−(1−メチルペンタデシル)フェノール、ジエチル[[3,5−ビス(1,1−ジメチルエチル)−4−ヒドロキシフェニル]メチル]ホスファート、3,3’,3”,5,5’,5”−ヘキサ−t−ブチル−a,a’,a”−(メシチレン−2,4,6−トリ−イル)トリ−p−クレゾール、4,6−ビス(オクチルチオメチル)−o−クレゾール、エチレン−ビス(オキシエチレン)ビス[3−(5−t−ブチル−4−ヒドロキシ−m−トリル)プロピオナート]、ヘキサメチレン−ビス[3−(3,5−ジ−t−ブチル−4−ヒドロキシフェニル)プロピオナート]、1,3,5−トリス(3,5−ジ−t−ブチル−4−ヒドロキシベンジル)−1,3,5−トリアジン−2,4,6(1H,3H,5H)−トリ−オン、2,6−ジ−t−ブチル−4−(4,6−ビス(オクチルチオ)−1,3,5−トリアジン−2−イル−アミノ)フェノール等が含まれる。これらのなかでも、テトラキス[3−(3,5−ジ−t−ブチル−4−ヒドロキシフェニル)プロピオン酸]ペンタエリトリチルおよび3−(3,5−ジ−t−ブチル−4−ヒドロキシフェニル)プロピオン酸オクタデシルが特に好ましい。これらの2種のフェノール系酸化防止剤は、それぞれ、CibaSpecialityChemicalsCorp.によって生産され、「IRGANOX1010」および「IRGANOX1076」の商品名で入手可能である。
用語「帯電防止剤」とは、伝導性および総合的な物理的性能を改善するために、ポリマー樹脂の中に加工することができる、および/または材料または製品上に噴霧することができる、単量体の、オリゴマーの、またはポリマーの物質をいう。単量体の帯電防止剤の例には、グリセロールモノステアラート、グリセロールジステアラート、グリセロールトリステアラート、エトキシ化アミン、第一級、第二級および第三級アミン、エトキシ化アルコール、硫酸アルキル、アルキルアリールスルファート、アルキルホスファート、アルキルアミンスルファート、スルホン酸ステアリル・ナトリウムやベンゼンスルホン酸ドデシル・ナトリウム等のアルキルスルホナート塩、第四級アンモニウム塩、第四級アンモニウム樹脂、イミダゾリン誘導体、ソルビタンエステル、エタノールアミド、ベタイン等、または上記の単量体の帯電防止剤の少なくとも1種を含む組合せが含まれる。
本発明において有用な離型剤の例には、脂肪族カルボン酸、脂肪族カルボン酸と脂肪族アルコールのエステル、200〜15000の数平均分子量を有する脂肪族炭化水素化合物、およびポリシロキサン系シリコーンオイルから選択される少なくとも1種が含まれる。
光学用途のポリカーボネート組成物は典型的には色補正される、すなわちそれらはポリカーボネートのいかなるわずかな色合いをも、典型的には黄色を補償するために色を調節する染料を含む。
他の添加剤
Claims (10)
- 押出成形されたポリカーボネート多壁シート構造体であって、
a.少なくとも7つの概ね平行な間隔のあいた壁と、
b.押出方向に前記シートの長さを伸ばし、隣接壁を分ける複数のリブとを備え、
前記シートは、40mm以上の総厚を有し、前記ポリカーボネートは、260℃で測定された4.5超の溶融粘度比を有し、前記溶融粘度比は、せん断速度0.1s-1での粘度と、せん断速度100s-1での粘度との比である、構造体。 - 前記ポリカーボネートが、せん断速度0.1s-1で、および260℃で10,000Pas超の溶融粘度を有する、
請求項1に記載の構造体。 - 前記ポリカーボネートが、ゲル浸透クロマトグラフィーを使用して測定した際に35,000から40,000の間の重量平均分子量を有する、
請求項1に記載の構造体。 - 少なくとも9つの壁を備える、
請求項1に記載の構造体。 - 少なくとも10の壁を備える、
請求項1に記載の構造体。 - 多壁構造体を製造する方法であって、
a.260℃で測定された4.5超の溶融粘度比を有するポリカーボネートを製造し、前記溶融粘度比は、せん断速度0.1s-1での粘度と、せん断速度100s-1での粘度との比であり、
b.260℃の溶融温度および0.5m/min以上のライン速度で前記ポリカーボネートを押出成形し、押出方向に前記シートの長さを伸ばすリブによって互いから分けられた少なくとも7つの概ね平行な間隔のあいた壁を有するシートを形成することを備える、方法。 - 前記ポリカーボネートが、せん断速度0.1s-1で、および260℃で10,000Pas超の粘度を有する、
請求項6に記載の方法。 - 前記ポリカーボネートが、ゲル浸透クロマトグラフィーを使用して測定した際に35,000から40,000の間の重量平均分子量を有する、
請求項6に記載の方法。 - 前記シートが、10以上の壁を有する、
請求項6に記載の方法。 - 前記シートが、40mm以上の総厚を有する、
請求項8に記載の方法。
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WO2021095607A1 (ja) * | 2019-11-11 | 2021-05-20 | マクセルホールディングス株式会社 | 樹脂発泡板 |
TWI727675B (zh) | 2020-02-26 | 2021-05-11 | 南亞塑膠工業股份有限公司 | 紅外線遮蔽膜及其製造方法 |
KR102238977B1 (ko) * | 2020-07-27 | 2021-04-13 | 주식회사 스타폴리캠 | 복합 적층 구조를 이루는 건축용 외장패널 구조체 |
WO2023094970A1 (en) * | 2021-11-23 | 2023-06-01 | King Abdullah University Of Science And Technology | Transparent photo-to-thermal energy conversion module and method |
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US4260731A (en) | 1978-09-11 | 1981-04-07 | Mitsubishi Chemical Industries, Ltd. | Aromatic polyester-polycarbonate |
DE3048695A1 (de) * | 1980-12-23 | 1982-07-08 | Bayer Ag, 5090 Leverkusen | Stegdoppelplatten |
US4529791A (en) | 1981-01-28 | 1985-07-16 | The Dow Chemical Company | Interfacial polycarbonate preparation by adding additional solvent |
US4677162A (en) | 1983-04-15 | 1987-06-30 | Mobay Corporation | Polycarbonate blends having low gloss |
US5856012A (en) * | 1993-10-18 | 1999-01-05 | Bayer Ag | Process for the production of multilayer plastic sheets |
JP3885834B2 (ja) * | 1994-11-08 | 2007-02-28 | 三菱瓦斯化学株式会社 | 透明ポリカーボネート樹脂成形材料の製法 |
KR20010023843A (ko) | 1997-09-10 | 2001-03-26 | 에프. 아. 프라저 | 착색제로서 유용한 이속신디고 및 이의 제조방법 |
US5972475A (en) * | 1997-10-24 | 1999-10-26 | The Dow Chemical Company | Structural sheet design for reduced weight and increased rigidity |
DE19747395A1 (de) | 1997-10-27 | 1999-04-29 | Clariant Int Ltd | Heterocyclische Verbindungen als polymerlösliche Farbstoffe |
JP2000007905A (ja) * | 1998-06-23 | 2000-01-11 | Daicel Chem Ind Ltd | 押出成形用ポリカーボネート系樹脂組成物、及び押出成形シート又はフィルム |
IT1307930B1 (it) * | 1999-01-26 | 2001-11-29 | Sinco Ricerche Spa | Articoli trasparenti in resina poliestere (mg32). |
US6210030B1 (en) * | 1999-06-15 | 2001-04-03 | Jean-Pierre Ibar | Method and apparatus to control viscosity of molten plastics prior to a molding operation |
DE19943642A1 (de) * | 1999-09-13 | 2001-03-15 | Bayer Ag | Behälter |
US20030214070A1 (en) * | 2002-05-08 | 2003-11-20 | General Electric Company | Multiwall polycarbonate sheet and method for its production |
JP2004123792A (ja) * | 2002-09-30 | 2004-04-22 | Mitsubishi Engineering Plastics Corp | 異形押出成形体 |
DE10318739A1 (de) * | 2003-04-25 | 2004-11-11 | Bayer Materialscience Ag | Polycarbonat-Formteile |
DE102004022673A1 (de) * | 2004-05-07 | 2005-11-24 | Bayer Materialscience Ag | Copolycarbonate mit verbesserter Fließfähigkeit |
EP2083999B1 (en) * | 2006-10-16 | 2010-05-26 | Valspar Sourcing, Inc. | Multilayer thermoplastic film |
US8568860B2 (en) * | 2007-11-12 | 2013-10-29 | Sabic Innovative Plastics Ip B.V. | Multiwall polymer sheet comprising branched polycarbonate |
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2010
- 2010-10-26 KR KR1020137010322A patent/KR101909297B1/ko active IP Right Grant
- 2010-10-26 CN CN2010800698189A patent/CN103189199A/zh active Pending
- 2010-10-26 JP JP2013535283A patent/JP5934228B2/ja active Active
- 2010-10-26 EP EP10770822.4A patent/EP2632707B1/en active Active
- 2010-10-26 WO PCT/EP2010/066171 patent/WO2012055429A1/en active Application Filing
- 2010-10-26 US US13/881,214 patent/US20130251954A1/en not_active Abandoned
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KR101909297B1 (ko) | 2018-10-17 |
EP2632707B1 (en) | 2019-04-10 |
CN103189199A (zh) | 2013-07-03 |
JP2013540623A (ja) | 2013-11-07 |
KR20130140687A (ko) | 2013-12-24 |
EP2632707A1 (en) | 2013-09-04 |
RU2558591C2 (ru) | 2015-08-10 |
WO2012055429A1 (en) | 2012-05-03 |
US20130251954A1 (en) | 2013-09-26 |
RU2013123989A (ru) | 2014-12-10 |
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