JP5852125B2 - ナフテン酸カルシウムを含む原油からカルシウムを除去するための添加剤及び方法 - Google Patents
ナフテン酸カルシウムを含む原油からカルシウムを除去するための添加剤及び方法 Download PDFInfo
- Publication number
- JP5852125B2 JP5852125B2 JP2013538334A JP2013538334A JP5852125B2 JP 5852125 B2 JP5852125 B2 JP 5852125B2 JP 2013538334 A JP2013538334 A JP 2013538334A JP 2013538334 A JP2013538334 A JP 2013538334A JP 5852125 B2 JP5852125 B2 JP 5852125B2
- Authority
- JP
- Japan
- Prior art keywords
- crude oil
- calcium
- additive
- wash water
- blend
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000010779 crude oil Substances 0.000 title claims description 92
- 239000011575 calcium Substances 0.000 title claims description 66
- 239000000654 additive Substances 0.000 title claims description 65
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims description 58
- 229910052791 calcium Inorganic materials 0.000 title claims description 58
- NKFIBMOQAPEKNZ-UHFFFAOYSA-N 5-amino-1h-indole-2-carboxylic acid Chemical compound NC1=CC=C2NC(C(O)=O)=CC2=C1 NKFIBMOQAPEKNZ-UHFFFAOYSA-N 0.000 title claims description 41
- 238000000034 method Methods 0.000 title claims description 27
- HHLFWLYXYJOTON-UHFFFAOYSA-N glyoxylic acid Chemical compound OC(=O)C=O HHLFWLYXYJOTON-UHFFFAOYSA-N 0.000 claims description 79
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 57
- 239000000203 mixture Substances 0.000 claims description 54
- 230000000996 additive effect Effects 0.000 claims description 42
- 150000001875 compounds Chemical class 0.000 claims description 21
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 16
- 229910052717 sulfur Inorganic materials 0.000 claims description 16
- 239000011593 sulfur Substances 0.000 claims description 16
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 15
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 14
- 229910017464 nitrogen compound Inorganic materials 0.000 claims description 13
- 150000002830 nitrogen compounds Chemical class 0.000 claims description 13
- 239000002253 acid Substances 0.000 claims description 12
- 150000007514 bases Chemical class 0.000 claims description 12
- 239000000908 ammonium hydroxide Substances 0.000 claims description 11
- 229910021529 ammonia Inorganic materials 0.000 claims description 7
- 238000011033 desalting Methods 0.000 claims description 7
- 238000010612 desalination reaction Methods 0.000 claims description 6
- 238000005406 washing Methods 0.000 claims description 2
- 150000007513 acids Chemical class 0.000 claims 2
- 150000003934 aromatic aldehydes Chemical class 0.000 claims 2
- 125000004432 carbon atom Chemical group C* 0.000 claims 2
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Chemical compound OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 description 32
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 21
- 239000010410 layer Substances 0.000 description 21
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 20
- 238000002474 experimental method Methods 0.000 description 20
- 239000001630 malic acid Substances 0.000 description 20
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 description 19
- 235000011090 malic acid Nutrition 0.000 description 19
- 238000010979 pH adjustment Methods 0.000 description 11
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 8
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- RGHNJXZEOKUKBD-SQOUGZDYSA-N D-gluconic acid Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O RGHNJXZEOKUKBD-SQOUGZDYSA-N 0.000 description 6
- RGHNJXZEOKUKBD-UHFFFAOYSA-N D-gluconic acid Natural products OCC(O)C(O)C(O)C(O)C(O)=O RGHNJXZEOKUKBD-UHFFFAOYSA-N 0.000 description 6
- 229950006191 gluconic acid Drugs 0.000 description 6
- 235000012208 gluconic acid Nutrition 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 238000007670 refining Methods 0.000 description 4
- 230000001105 regulatory effect Effects 0.000 description 4
- 238000007792 addition Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 238000009616 inductively coupled plasma Methods 0.000 description 3
- 239000012044 organic layer Substances 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- 239000008186 active pharmaceutical agent Substances 0.000 description 2
- IFQUWYZCAGRUJN-UHFFFAOYSA-N ethylenediaminediacetic acid Chemical compound OC(=O)CNCCNCC(O)=O IFQUWYZCAGRUJN-UHFFFAOYSA-N 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 150000001261 hydroxy acids Chemical class 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 1
- -1 amine compounds Chemical class 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- QDCSTXADKDXERF-JJKGCWMISA-N calcium;(2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanoic acid Chemical compound [Ca].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O QDCSTXADKDXERF-JJKGCWMISA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000004255 ion exchange chromatography Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 150000003464 sulfur compounds Chemical class 0.000 description 1
- 229910021642 ultra pure water Inorganic materials 0.000 description 1
- 239000012498 ultrapure water Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G17/00—Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge
- C10G17/02—Refining of hydrocarbon oils in the absence of hydrogen, with acids, acid-forming compounds or acid-containing liquids, e.g. acid sludge with acids or acid-containing liquids, e.g. acid sludge
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G19/00—Refining hydrocarbon oils in the absence of hydrogen, by alkaline treatment
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G29/00—Refining of hydrocarbon oils, in the absence of hydrogen, with other chemicals
- C10G29/20—Organic compounds not containing metal atoms
- C10G29/22—Organic compounds not containing metal atoms containing oxygen as the only hetero atom
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G31/00—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for
- C10G31/08—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for by treating with water
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/20—Characteristics of the feedstock or the products
- C10G2300/201—Impurities
- C10G2300/202—Heteroatoms content, i.e. S, N, O, P
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/80—Additives
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IN3111/MUM/2010 | 2010-11-15 | ||
| IN3111MU2010 | 2010-11-15 | ||
| PCT/IN2011/000786 WO2012066566A1 (en) | 2010-11-15 | 2011-11-14 | Additive and method for removal of calcium from crude oils containing calcium naphthenate. |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013542306A JP2013542306A (ja) | 2013-11-21 |
| JP2013542306A5 JP2013542306A5 (enExample) | 2015-08-20 |
| JP5852125B2 true JP5852125B2 (ja) | 2016-02-03 |
Family
ID=45607323
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013538334A Expired - Fee Related JP5852125B2 (ja) | 2010-11-15 | 2011-11-14 | ナフテン酸カルシウムを含む原油からカルシウムを除去するための添加剤及び方法 |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US9434889B2 (enExample) |
| EP (1) | EP2640809B1 (enExample) |
| JP (1) | JP5852125B2 (enExample) |
| KR (1) | KR101748417B1 (enExample) |
| CN (1) | CN103210064B (enExample) |
| AU (1) | AU2011330718B2 (enExample) |
| BR (1) | BR112013012007B1 (enExample) |
| CA (1) | CA2817040C (enExample) |
| CL (1) | CL2013001337A1 (enExample) |
| CO (1) | CO6721015A2 (enExample) |
| ES (1) | ES2882131T3 (enExample) |
| HR (1) | HRP20211301T1 (enExample) |
| MX (1) | MX342558B (enExample) |
| MY (1) | MY163743A (enExample) |
| PE (1) | PE20140394A1 (enExample) |
| PH (1) | PH12013500887A1 (enExample) |
| PL (1) | PL2640809T3 (enExample) |
| RS (1) | RS62223B1 (enExample) |
| SG (1) | SG190706A1 (enExample) |
| WO (1) | WO2012066566A1 (enExample) |
| ZA (1) | ZA201304365B (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2761942T3 (es) * | 2009-04-15 | 2020-05-21 | Dorf Ketal Chemicals I Private Ltd | Procedimiento de uso de un aditivo no polimérico y antiincrustante efectivo para inhibir la corrosión por ácido nafténico a alta temperatura |
| ES2882131T3 (es) | 2010-11-15 | 2021-12-01 | Dorf Ketal Chemicals India Private Ltd | Eliminación del calcio del petróleo crudo que contiene naftenato de calcio |
| EP3316982B1 (en) * | 2015-07-01 | 2020-02-19 | Dorf Ketal Chemicals (India) Private Limited | Additive composition for demulsification of water-in-oil emulsion, and method of use thereof, and method of demulsification |
| CN109790472B (zh) * | 2016-09-22 | 2021-06-01 | Bp北美公司 | 从原油除去污染物 |
| US20200239785A1 (en) * | 2019-01-24 | 2020-07-30 | Exxonmobil Research And Engineering Company | Organic acid removal from liquid hydrocarbon product streams |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4476930A (en) * | 1982-08-23 | 1984-10-16 | Union Oil Company Of California | Inhibition of scale deposition from steam generation fluids |
| JPS6361087A (ja) * | 1986-08-28 | 1988-03-17 | シエブロン リサ−チ カンパニ− | 炭化水素供給原料の脱金属方法 |
| US5284635A (en) * | 1989-09-05 | 1994-02-08 | Societe Francaise Hoechst | Process for the elimination of hydrogen sulfide by using water-in-oil emulsions |
| FR2651500A1 (fr) * | 1989-09-05 | 1991-03-08 | Hoechst France | Nouvelles emulsions eau dans huile et leur application a l'elimination du sulfure d'hydrogene. |
| JPH03277691A (ja) * | 1990-03-27 | 1991-12-09 | Chevron Res Co | 炭化水素原料からの金属除去方法 |
| US6068056A (en) * | 1999-10-13 | 2000-05-30 | Schlumberger Technology Corporation | Well treatment fluids comprising mixed aldehydes |
| MY160536A (en) * | 2008-01-24 | 2017-03-15 | Dorf Ketal Chemicals (I) Private Ltd | Method of removing metals from hydrocarbon feedstock using esters of carboxylic acids |
| US8778172B2 (en) * | 2009-05-05 | 2014-07-15 | Dorf Ketal Chemicals (I) Private Limited | Method of scavenging hydrogen sulfide from hydrocarbon stream |
| ES2882131T3 (es) | 2010-11-15 | 2021-12-01 | Dorf Ketal Chemicals India Private Ltd | Eliminación del calcio del petróleo crudo que contiene naftenato de calcio |
-
2011
- 2011-11-14 ES ES11817538T patent/ES2882131T3/es active Active
- 2011-11-14 JP JP2013538334A patent/JP5852125B2/ja not_active Expired - Fee Related
- 2011-11-14 RS RS20211017A patent/RS62223B1/sr unknown
- 2011-11-14 PL PL11817538T patent/PL2640809T3/pl unknown
- 2011-11-14 US US13/885,216 patent/US9434889B2/en active Active
- 2011-11-14 AU AU2011330718A patent/AU2011330718B2/en not_active Ceased
- 2011-11-14 BR BR112013012007-0A patent/BR112013012007B1/pt not_active IP Right Cessation
- 2011-11-14 HR HRP20211301TT patent/HRP20211301T1/hr unknown
- 2011-11-14 EP EP11817538.9A patent/EP2640809B1/en active Active
- 2011-11-14 PE PE2013001081A patent/PE20140394A1/es active IP Right Grant
- 2011-11-14 PH PH1/2013/500887A patent/PH12013500887A1/en unknown
- 2011-11-14 CN CN201180055049.1A patent/CN103210064B/zh not_active Expired - Fee Related
- 2011-11-14 WO PCT/IN2011/000786 patent/WO2012066566A1/en not_active Ceased
- 2011-11-14 MX MX2013005404A patent/MX342558B/es active IP Right Grant
- 2011-11-14 SG SG2013037429A patent/SG190706A1/en unknown
- 2011-11-14 MY MYPI2013700797A patent/MY163743A/en unknown
- 2011-11-14 CA CA2817040A patent/CA2817040C/en active Active
- 2011-11-14 KR KR1020137015222A patent/KR101748417B1/ko active Active
-
2013
- 2013-05-14 CL CL2013001337A patent/CL2013001337A1/es unknown
- 2013-06-13 ZA ZA2013/04365A patent/ZA201304365B/en unknown
- 2013-06-14 CO CO13142402A patent/CO6721015A2/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP2640809B1 (en) | 2021-05-19 |
| ES2882131T3 (es) | 2021-12-01 |
| JP2013542306A (ja) | 2013-11-21 |
| KR20130106863A (ko) | 2013-09-30 |
| SG190706A1 (en) | 2013-07-31 |
| WO2012066566A1 (en) | 2012-05-24 |
| KR101748417B1 (ko) | 2017-06-16 |
| CL2013001337A1 (es) | 2013-08-09 |
| US9434889B2 (en) | 2016-09-06 |
| BR112013012007B1 (pt) | 2018-12-26 |
| CN103210064A (zh) | 2013-07-17 |
| PE20140394A1 (es) | 2014-04-03 |
| PL2640809T3 (pl) | 2021-11-22 |
| US20130233770A1 (en) | 2013-09-12 |
| MY163743A (en) | 2017-10-31 |
| CO6721015A2 (es) | 2013-07-31 |
| HRP20211301T1 (hr) | 2021-11-12 |
| CA2817040A1 (en) | 2012-05-24 |
| MX2013005404A (es) | 2013-08-01 |
| AU2011330718A1 (en) | 2013-06-06 |
| ZA201304365B (en) | 2014-09-25 |
| CA2817040C (en) | 2016-07-12 |
| BR112013012007A2 (pt) | 2016-09-06 |
| RS62223B1 (sr) | 2021-09-30 |
| CN103210064B (zh) | 2016-03-16 |
| PH12013500887A1 (en) | 2022-10-24 |
| AU2011330718B2 (en) | 2016-02-25 |
| EP2640809A1 (en) | 2013-09-25 |
| MX342558B (es) | 2016-10-05 |
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