JP5756087B2 - 高効率触媒による特定のアルキレンオキサイド製造パラメーターを達成かつ維持する改良方法 - Google Patents

高効率触媒による特定のアルキレンオキサイド製造パラメーターを達成かつ維持する改良方法 Download PDF

Info

Publication number
JP5756087B2
JP5756087B2 JP2012507297A JP2012507297A JP5756087B2 JP 5756087 B2 JP5756087 B2 JP 5756087B2 JP 2012507297 A JP2012507297 A JP 2012507297A JP 2012507297 A JP2012507297 A JP 2012507297A JP 5756087 B2 JP5756087 B2 JP 5756087B2
Authority
JP
Japan
Prior art keywords
alkylene oxide
concentration
efficiency
catalyst
reaction temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2012507297A
Other languages
English (en)
Japanese (ja)
Other versions
JP2012524786A (ja
JP2012524786A5 (enExample
Inventor
チャン リッピン
チャン リッピン
リュー アルバート
リュー アルバート
ハベンシュス マイケル
ハベンシュス マイケル
Original Assignee
ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー
ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=42629694&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JP5756087(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー, ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー filed Critical ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー
Publication of JP2012524786A publication Critical patent/JP2012524786A/ja
Publication of JP2012524786A5 publication Critical patent/JP2012524786A5/ja
Application granted granted Critical
Publication of JP5756087B2 publication Critical patent/JP5756087B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/02Synthesis of the oxirane ring
    • C07D301/03Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
    • C07D301/08Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
    • C07D301/10Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/33Heterocyclic compounds
    • A61K31/395Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/495Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having six-membered rings with two or more nitrogen atoms as the only ring heteroatoms, e.g. piperazine or tetrazines
    • A61K31/498Pyrazines or piperazines ortho- and peri-condensed with carbocyclic ring systems, e.g. quinoxaline, phenazine
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02Impregnation, coating or precipitation
    • B01J37/0201Impregnation
    • B01J37/0205Impregnation in several steps
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D301/00Preparation of oxiranes
    • C07D301/02Synthesis of the oxirane ring
    • C07D301/03Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/04Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Veterinary Medicine (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2012507297A 2009-04-21 2010-04-20 高効率触媒による特定のアルキレンオキサイド製造パラメーターを達成かつ維持する改良方法 Active JP5756087B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US17128409P 2009-04-21 2009-04-21
US61/171,284 2009-04-21
PCT/US2010/031673 WO2010123844A1 (en) 2009-04-21 2010-04-20 Improved method of achieving and maintaining a specified alkylene oxide production parameter with a high efficiency catalyst

Publications (3)

Publication Number Publication Date
JP2012524786A JP2012524786A (ja) 2012-10-18
JP2012524786A5 JP2012524786A5 (enExample) 2013-05-30
JP5756087B2 true JP5756087B2 (ja) 2015-07-29

Family

ID=42629694

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012507297A Active JP5756087B2 (ja) 2009-04-21 2010-04-20 高効率触媒による特定のアルキレンオキサイド製造パラメーターを達成かつ維持する改良方法

Country Status (9)

Country Link
US (1) US8362284B2 (enExample)
EP (1) EP2421841B1 (enExample)
JP (1) JP5756087B2 (enExample)
KR (1) KR101730667B1 (enExample)
CN (1) CN102414188B (enExample)
CA (1) CA2759397C (enExample)
SG (1) SG175771A1 (enExample)
TW (1) TWI481599B (enExample)
WO (1) WO2010123844A1 (enExample)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PE20090146A1 (es) * 2007-04-20 2009-03-23 Glaxosmithkline Biolog Sa Composicion inmunogenica contra el virus influenza
JP5756088B2 (ja) * 2009-04-21 2015-07-29 ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー エポキシ化反応及びその運転条件
EP2649059B1 (en) 2010-12-10 2016-02-24 Dow Technology Investments LLC Method of reducing the value of an alkylene oxide production parameter in a process of making an alkylene oxide using a high efficiency catalyst
WO2012082389A1 (en) * 2010-12-15 2012-06-21 Dow Technology Investments Llc Method of starting-up a process of producing an alkylene oxide using a high-efficiency catalyst
EP2714670B2 (en) 2011-04-29 2022-03-02 Shell Internationale Research Maatschappij B.V. Process for improving the selectivity of an eo catalyst
CN108707125A (zh) * 2011-10-18 2018-10-26 哈桑·伊萨·阿拉哈迈迪 具有添加缓和剂的环氧化方法
SG11201403042SA (en) * 2011-12-09 2014-10-30 Dow Technology Investments Llc Method of maintaining the value of an alkylene oxide production parameter in a process of making an alkylene oxide using a high efficiency catalyst
EP2920159B1 (en) 2012-12-31 2020-02-12 Scientific Design Company Inc. Start-up process for high selectivity ethylene oxide catalysts
SG11201507353RA (en) 2013-03-15 2015-10-29 Dow Technology Investments Llc Method for the production of ethylene oxide
CA2972690C (en) * 2014-12-30 2023-08-22 Dow Technology Investments Llc Process for manufacturing ethylene oxide using scaled selectivity values
WO2019055773A1 (en) * 2017-09-15 2019-03-21 MultiPhase Solutions, Inc. GAS PHASE CHROMATOGRAPHY OF SELECTIVE HALOGEN DETECTION FOR ONLINE ANALYSIS AND CONTROL OF SELECTIVE OXIDATION CHEMICAL PRODUCTION PROCESSES
CN110673557B (zh) * 2019-09-27 2021-09-24 南京大学 基于工艺条件选择的智能化工系统
TW202239752A (zh) 2020-12-29 2022-10-16 荷蘭商蜆殼國際研究所 用於生產環氧乙烷之製程
WO2022214539A1 (en) 2021-04-08 2022-10-13 Shell Internationale Research Maatschappij B.V. Moderator and catalyst performance optimization for epoxidation of ethylene
CN118019732A (zh) * 2021-09-23 2024-05-10 陶氏环球技术有限责任公司 用于降低高选择性环氧乙烷催化剂的老化相关失活的方法

Family Cites Families (49)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE752859R (fr) 1969-07-10 1971-01-04 Halcon International Inc Oxydation controlee de l'oxyde
US5387751A (en) 1978-02-10 1995-02-07 Imperial Chemical Industries Plc Production of olefine oxides
JPS6110570A (ja) 1984-06-25 1986-01-18 Mitsui Toatsu Chem Inc エチレンオキシドの製造方法
CA1286687C (en) 1985-08-13 1991-07-23 Michael Paul Habenschuss Process for manufacture of alkene oxide
US4766105A (en) 1986-10-31 1988-08-23 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
US4808738A (en) 1986-10-31 1989-02-28 Shell Oil Company Ethylene oxide process
IL84232A (en) 1986-10-31 1992-06-21 Shell Int Research Catalyst and process for the catalytic production of ethylene oxide
US4820675A (en) 1986-10-31 1989-04-11 Shell Oil Company Ethylene oxide catalyst & process for preparing the catalyst
US4761394A (en) 1986-10-31 1988-08-02 Shell Oil Company Ethylene oxide catalyst and process for preparing the catalyst
GB8626687D0 (en) * 1986-11-07 1986-12-10 Shell Int Research Preparing silver catalyst
US4908343A (en) 1987-02-20 1990-03-13 Union Carbide Chemicals And Plastics Company Inc. Catalyst composition for oxidation of ethylene to ethylene oxide
US4769047A (en) 1987-06-29 1988-09-06 Shell Oil Company Process for the production of ethylene oxide
GB8716653D0 (en) 1987-07-15 1987-08-19 Shell Int Research Silver-containing catalyst
US4759313A (en) 1987-10-30 1988-07-26 Shell Oil Company Ethylene oxide process improvement
CA1339317C (en) 1988-07-25 1997-08-19 Ann Marie Lauritzen Process for producing ethylene oxide
US4874879A (en) 1988-07-25 1989-10-17 Shell Oil Company Process for starting-up an ethylene oxide reactor
EP0357293B1 (en) 1988-08-30 1996-02-28 Union Carbide Corporation Catalysts for the production of ethylene oxide and their preparation processes
CA1337722C (en) 1989-04-18 1995-12-12 Madan Mohan Bhasin Alkylene oxide catalysts having enhanced activity and/or stability
GB9005964D0 (en) 1990-03-16 1990-05-09 Shell Int Research Catalyst preparation process
US5102848A (en) 1990-09-28 1992-04-07 Union Carbide Chemicals & Plastics Technology Corporation Catalyst composition for oxidation of ethylene to ethylene oxide
JPH04298241A (ja) 1990-10-12 1992-10-22 Union Carbide Chem & Plast Co Inc 向上した安定性を有する超高性能アルキレンオキシド触媒
CA2053411C (en) 1990-10-12 1997-06-03 Albert Cheng-Yu Liu Alkylene oxide catalysts having enhanced activity and/or stability
US5145824A (en) 1991-01-22 1992-09-08 Shell Oil Company Ethylene oxide catalyst
US5228484A (en) 1991-06-20 1993-07-20 Catalyst Technology, Inc. Air lance reel for catalyst unloading of tubular reactors
US5155242A (en) 1991-12-05 1992-10-13 Shell Oil Company Process for starting-up an ethylene oxide reactor
US5262551A (en) 1992-04-20 1993-11-16 Texaco Chemical Company Process for ethylene expoxidation
US5447897A (en) 1993-05-17 1995-09-05 Shell Oil Company Ethylene oxide catalyst and process
US5380697A (en) 1993-09-08 1995-01-10 Shell Oil Company Ethylene oxide catalyst and process
US5364826A (en) 1993-09-13 1994-11-15 Shell Oil Company Process for preparing ethylene oxide catalysts
TW314512B (enExample) 1993-09-20 1997-09-01 Shell Int Research
US5418202A (en) 1993-12-30 1995-05-23 Shell Oil Company Ethylene oxide catalyst and process
US5545603A (en) 1994-11-01 1996-08-13 Shell Oil Company Ethylene oxide catalyst and process
BR9608185A (pt) 1995-04-18 1999-05-04 Shell Int Research Processo para a oxidação catalítica de etileno em fase de vapor
US5739075A (en) 1995-10-06 1998-04-14 Shell Oil Company Process for preparing ethylene oxide catalysts
KR100447357B1 (ko) 1995-11-23 2004-12-03 셀 인터나쵸나아레 레사아치 마아츠샤피 비이부이 알킬렌글리콜의제조방법
US5801259A (en) 1996-04-30 1998-09-01 Shell Oil Company Ethylene oxide catalyst and process
US5840932A (en) 1996-05-21 1998-11-24 Shell Oil Company Process for ethylene oxide production
WO1997046317A1 (en) 1996-06-05 1997-12-11 Shell Internationale Research Maatschappij B.V. Epoxidation catalyst and process
US5770746A (en) * 1997-06-23 1998-06-23 Arco Chemical Technology, L.P. Epoxidation process using supported silver catalysts pretreated with organic chloride
US7193094B2 (en) 2001-11-20 2007-03-20 Shell Oil Company Process and systems for the epoxidation of an olefin
KR100977098B1 (ko) * 2001-11-20 2010-08-23 셀 인터나쵸나아레 레사아치 마아츠샤피 비이부이 올레핀의 에폭시화 방법 및 시스템
BR0312011B1 (pt) 2002-06-28 2014-08-05 Shell Int Research Processo para a partida de um processo de epoxidação, um catalisador e um processo para a epoxidação de uma olefina
RU2005102097A (ru) 2002-06-28 2005-08-27 Шелл Интернэшнл Рисерч Маатсхаппий Б.В. (NL) Способ введения в действие способа эпоксидирования и способ эпоксидирования олефина
RU2328491C2 (ru) 2003-04-01 2008-07-10 Шелл Интернэшнл Рисерч Маатсхаппий Б.В. Способ эпоксидирования олефинов и катализатор для применения в способе
US7615655B2 (en) * 2003-09-29 2009-11-10 Dow Global Technologies, Inc. Process for the production of alkylene oxide using a gas-phase promoter system
CN100572370C (zh) 2004-06-18 2009-12-23 国际壳牌研究有限公司 生产烯烃氧化物、1,2-二醇、1,2-二醇醚或链烷醇胺的方法
US7803957B2 (en) * 2007-09-11 2010-09-28 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Ethylene oxide production using fixed moderator concentration
US7553980B2 (en) 2007-09-26 2009-06-30 Sd Lizenzverwertungsgesellschaft Mbh & Co. Kg Process for initiating a highly selective ethylene oxide catalyst
JP2012524785A (ja) * 2009-04-21 2012-10-18 ダウ テクノロジー インベストメンツ リミティド ライアビリティー カンパニー 高効率触媒を用いたアルキレンオキシド簡易製造方法

Also Published As

Publication number Publication date
JP2012524786A (ja) 2012-10-18
US8362284B2 (en) 2013-01-29
WO2010123844A1 (en) 2010-10-28
TWI481599B (zh) 2015-04-21
EP2421841A1 (en) 2012-02-29
KR101730667B1 (ko) 2017-04-26
CA2759397C (en) 2019-01-29
CA2759397A1 (en) 2010-10-28
CN102414188A (zh) 2012-04-11
KR20120014160A (ko) 2012-02-16
US20100267972A1 (en) 2010-10-21
CN102414188B (zh) 2015-05-27
TW201105641A (en) 2011-02-16
SG175771A1 (en) 2011-12-29
EP2421841B1 (en) 2018-12-26

Similar Documents

Publication Publication Date Title
JP5756087B2 (ja) 高効率触媒による特定のアルキレンオキサイド製造パラメーターを達成かつ維持する改良方法
JP6034436B2 (ja) エポキシ化反応及びその運転条件
CN102414187B (zh) 采用催化剂随其老化而制备环氧烷的方法
TWI510476B (zh) 以高效能催化劑起始一製造環氧烷烴製程的方法
US8884037B2 (en) Method of reducing the value of an alkylene oxide production parameter in a process of making an alkylene oxide using a high efficiency catalyst

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20130409

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20130409

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20140805

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20141031

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20141209

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20150407

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20150414

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20150512

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20150528

R150 Certificate of patent or registration of utility model

Ref document number: 5756087

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250