JP5139071B2 - ガラスマイクロバブルおよび生製品の製造方法 - Google Patents
ガラスマイクロバブルおよび生製品の製造方法 Download PDFInfo
- Publication number
- JP5139071B2 JP5139071B2 JP2007544338A JP2007544338A JP5139071B2 JP 5139071 B2 JP5139071 B2 JP 5139071B2 JP 2007544338 A JP2007544338 A JP 2007544338A JP 2007544338 A JP2007544338 A JP 2007544338A JP 5139071 B2 JP5139071 B2 JP 5139071B2
- Authority
- JP
- Japan
- Prior art keywords
- glass microbubbles
- feed
- glass
- frit
- fsc
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 239000011521 glass Substances 0.000 title claims description 69
- 238000004519 manufacturing process Methods 0.000 title description 3
- 238000009826 distribution Methods 0.000 claims description 23
- 238000000034 method Methods 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 11
- 239000002861 polymer material Substances 0.000 claims 1
- 239000002245 particle Substances 0.000 description 32
- 238000000227 grinding Methods 0.000 description 11
- 239000011324 bead Substances 0.000 description 10
- 239000000203 mixture Substances 0.000 description 9
- 238000012545 processing Methods 0.000 description 9
- 239000011734 sodium Substances 0.000 description 9
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 8
- 239000000463 material Substances 0.000 description 8
- 239000011593 sulfur Substances 0.000 description 7
- 229910052717 sulfur Inorganic materials 0.000 description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- 229910004298 SiO 2 Inorganic materials 0.000 description 5
- 239000012530 fluid Substances 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 239000004604 Blowing Agent Substances 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 229910044991 metal oxide Inorganic materials 0.000 description 4
- 150000004706 metal oxides Chemical class 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 3
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- 239000004005 microsphere Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000010298 pulverizing process Methods 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- 241000203482 Polyscias Species 0.000 description 2
- 241001625808 Trona Species 0.000 description 2
- 229910021538 borax Inorganic materials 0.000 description 2
- 229910052796 boron Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000002706 hydrostatic effect Effects 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 239000005368 silicate glass Substances 0.000 description 2
- 239000004328 sodium tetraborate Substances 0.000 description 2
- 235000010339 sodium tetraborate Nutrition 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 229910000287 alkaline earth metal oxide Inorganic materials 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003623 enhancer Substances 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000005188 flotation Methods 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
- 229910052731 fluorine Inorganic materials 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 1
- 229910052808 lithium carbonate Inorganic materials 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- 239000006060 molten glass Substances 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000005549 size reduction Methods 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 235000017550 sodium carbonate Nutrition 0.000 description 1
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003464 sulfur compounds Chemical class 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 235000019818 tetrasodium diphosphate Nutrition 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C11/00—Multi-cellular glass ; Porous or hollow glass or glass particles
- C03C11/002—Hollow glass particles
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
- C03B19/107—Forming hollow beads
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C12/00—Powdered glass; Bead compositions
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/004,385 | 2004-12-03 | ||
| US11/004,385 US20060122049A1 (en) | 2004-12-03 | 2004-12-03 | Method of making glass microbubbles and raw product |
| PCT/US2005/032887 WO2006062566A1 (en) | 2004-12-03 | 2005-09-15 | Method of making glass microbubbles and raw product |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2008521750A JP2008521750A (ja) | 2008-06-26 |
| JP2008521750A5 JP2008521750A5 (https=) | 2008-10-16 |
| JP5139071B2 true JP5139071B2 (ja) | 2013-02-06 |
Family
ID=36575076
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2007544338A Expired - Fee Related JP5139071B2 (ja) | 2004-12-03 | 2005-09-15 | ガラスマイクロバブルおよび生製品の製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20060122049A1 (https=) |
| EP (1) | EP1833767B1 (https=) |
| JP (1) | JP5139071B2 (https=) |
| KR (1) | KR20070085613A (https=) |
| CN (1) | CN101068753B (https=) |
| BR (1) | BRPI0518722A2 (https=) |
| MX (1) | MX2007006391A (https=) |
| WO (1) | WO2006062566A1 (https=) |
Families Citing this family (39)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060243363A1 (en) * | 2005-04-29 | 2006-11-02 | 3M Innovative Properties Company | Glass microbubble-containing syntactic foams, explosives, and method of making |
| US8701441B2 (en) | 2006-08-21 | 2014-04-22 | 3M Innovative Properties Company | Method of making inorganic, metal oxide spheres using microstructured molds |
| WO2008067267A2 (en) * | 2006-11-29 | 2008-06-05 | 3M Innovative Properties Company | Microsphere-containing insulation |
| US20080166558A1 (en) * | 2006-12-22 | 2008-07-10 | 3M Innovative Properties Company | Compositions of particles |
| US20080152913A1 (en) * | 2006-12-22 | 2008-06-26 | 3M Innovative Properties Company | Method of making compositions including particles |
| US20080153963A1 (en) * | 2006-12-22 | 2008-06-26 | 3M Innovative Properties Company | Method for making a dispersion |
| US8362114B2 (en) * | 2007-02-28 | 2013-01-29 | Solvay Advanced Polymers, L.L.C. | Thermoplastic compositions containing microspheres |
| US7900474B2 (en) * | 2008-08-14 | 2011-03-08 | Beck Warren R | Hollow glass microspheres comprising selenium oxide and method of making thereof |
| US20100330309A1 (en) * | 2009-06-30 | 2010-12-30 | Guardian Industries Corp. | Frit or solder glass compound including beads, and assemblies incorporating the same |
| US8261577B2 (en) | 2009-12-21 | 2012-09-11 | 3M Innovative Properties Company | Method for making hollow microspheres |
| EP2598600A1 (en) | 2010-07-29 | 2013-06-05 | 3M Innovative Properties Company | Elastomer-modified crosslinked epoxy vinyl ester particles and methods for making and using the same |
| BR112013005527B1 (pt) * | 2010-09-08 | 2020-10-13 | 3M Innovative Properties Company | classificação de microesferas ocas de vidro, compósito compreendendo a mesma, e seu método para produção. |
| EP2655273A2 (en) * | 2010-12-20 | 2013-10-30 | 3M Innovative Properties Company | Hollow microspheres and method of making hollow microspheres |
| JP6425541B2 (ja) | 2011-07-07 | 2018-11-21 | スリーエム イノベイティブ プロパティズ カンパニー | 多成分繊維及び中空のセラミック微小球を含む物品、並びにその製造方法及び使用方法 |
| PT106237B (pt) * | 2012-03-30 | 2015-03-19 | Hovione Farmaci Ncia S A | Produção de partículas substancialmente monodispersas utilizando moagem e separação por membranas |
| WO2013184307A2 (en) | 2012-06-06 | 2013-12-12 | 3M Innovative Properties Company | Low density glass particles with low boron content |
| EP2864413B1 (en) | 2012-06-25 | 2017-01-25 | 3M Innovative Properties Company | Masterbatch composition, method of using, and rubber composition |
| AU2013286932B2 (en) | 2012-07-03 | 2016-04-28 | 3M Innovative Properties Company | Siloxane-based pipe coatings |
| CN102910828B (zh) * | 2012-11-21 | 2015-07-15 | 贵州威顿晶磷电子材料股份有限公司 | 用于硅太阳能电池正面银浆无铅低熔点玻璃粉及制备方法 |
| EP2935444B1 (en) | 2012-12-20 | 2019-09-18 | 3M Innovative Properties Company | Composite particles including a fluoropolymer, methods of making, and articles including the same |
| WO2015009461A2 (en) | 2013-07-18 | 2015-01-22 | 3M Innovative Properties Company | Glass microbubbles, raw product, and methods of making the same |
| WO2015103099A1 (en) | 2013-12-30 | 2015-07-09 | 3M Innovative Properties Company | Polyolefin composition including hollow glass microspheres and method of using the same |
| EP3090022B1 (en) | 2013-12-30 | 2018-09-05 | 3M Innovative Properties Company | Poly(methylpentene) composition including hollow glass microspheres and method of using the same |
| GB201415005D0 (en) * | 2014-08-22 | 2014-10-08 | Univ Nottingham | Porous and non-pourous bodies |
| US10494525B2 (en) | 2015-02-27 | 2019-12-03 | 3M Innovative Properties Company | Polyamide composition including hollow glass microspheres and articles and methods relating to the same |
| EP3130636A1 (en) | 2015-08-13 | 2017-02-15 | 3M Innovative Properties Company | Polyolefin composition comprising hollow glass microspheres |
| WO2017040900A1 (en) * | 2015-09-04 | 2017-03-09 | 3M Innovative Properties Company | Method of making hollow glass microspheres |
| NO3184494T3 (https=) * | 2015-12-21 | 2018-07-07 | ||
| BR112018017027A2 (pt) | 2016-02-26 | 2018-12-26 | 3M Innovative Properties Co | artigo de esfregamento e método para produção de um artigo de esfregamento |
| US20190344496A1 (en) | 2016-12-20 | 2019-11-14 | 3M Innovative Properties Company | Composition including fluoropolymer and inorganic filler and method of making a three-dimensional article |
| KR102864246B1 (ko) * | 2018-07-26 | 2025-09-24 | 옴야 인터내셔널 아게 | 중공 구형 유리 입자 |
| MX2022009077A (es) | 2020-01-24 | 2022-08-15 | Basf Se | Proceso de fabricacion de particulas de vidrio esfericas huecas. |
| JP2024517373A (ja) * | 2021-03-19 | 2024-04-22 | ネオゲン フード セイフティ ユーエス ホルドコ コーポレイション | 分析物を検出する組成物及び方法 |
| EP4370474A1 (en) | 2021-07-16 | 2024-05-22 | 3M Innovative Properties Company | Glass bubbles and articles therefrom |
| EP4197980A1 (en) | 2021-12-16 | 2023-06-21 | 3M Innovative Properties Company | Coated glass microspheres comprising a coating comprising hexagonal boron nitride particles |
| WO2024134299A1 (en) | 2022-12-21 | 2024-06-27 | 3M Innovative Properties Company | Coated glass bubbles and methods of making coated glass bubbles by mechanical exfoliation |
| EP4705391A1 (en) | 2023-07-21 | 2026-03-11 | 3M Innovative Properties Company | Castable composition comprising liquid silicone rubber and hollow glass microspheres |
| WO2025099515A1 (en) | 2023-11-09 | 2025-05-15 | 3M Innovative Properties Company | Composites containing graphene coated hollow particles useful in high frequency applications |
| WO2026078538A1 (en) | 2024-10-10 | 2026-04-16 | 3M Innovative Properties Company | Curable compositions including a polymerizable composition and a block copolymer, methods, cured compositions, and multilayer articles |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2797201A (en) * | 1953-05-11 | 1957-06-25 | Standard Oil Co | Process of producing hollow particles and resulting product |
| US2676892A (en) * | 1953-11-13 | 1954-04-27 | Kanium Corp | Method for making unicellular spherulized clay particles and articles and composition thereof |
| NL232500A (https=) * | 1957-10-22 | |||
| US3230034A (en) * | 1960-09-29 | 1966-01-18 | Du Pont | Method of treating exhaust gases of internal combustion engines |
| US3365315A (en) * | 1963-08-23 | 1968-01-23 | Minnesota Mining & Mfg | Glass bubbles prepared by reheating solid glass partiles |
| US4017290A (en) * | 1974-04-15 | 1977-04-12 | Kms Fusion, Inc. | Method and apparatus for making uniform pellets for fusion reactors |
| US3961978A (en) * | 1974-09-20 | 1976-06-08 | General Refractories Company | Process for producing perlite microspheres |
| US4391646A (en) * | 1982-02-25 | 1983-07-05 | Minnesota Mining And Manufacturing Company | Glass bubbles of increased collapse strength |
| US4736527A (en) * | 1982-12-13 | 1988-04-12 | Konishiroku Photo Industry Co., Ltd. | Apparatus for the heat treatment of powdery material |
| FR2566384B1 (fr) * | 1984-06-21 | 1986-09-05 | Saint Gobain Vitrage | Perfectionnements aux techniques de production de microspheres en verre |
| US4767726A (en) * | 1987-01-12 | 1988-08-30 | Minnesota Mining And Manufacturing Company | Glass microbubbles |
| US5217928A (en) * | 1988-08-24 | 1993-06-08 | Potters Industries, Inc. | Hollow glass spheres |
| US4983550A (en) * | 1988-08-24 | 1991-01-08 | Potters Industries, Inc. | Hollow glass spheres |
| US4940497A (en) * | 1988-12-14 | 1990-07-10 | Atlas Powder Company | Emulsion explosive composition containing expanded perlite |
| DE69020623T3 (de) * | 1989-04-18 | 2000-03-02 | Tokai Kogyo Co. Ltd., Tokio/Tokyo | Glasfrit, verwendbar zur Herstellung von Glashohlkugeln, und daraus hergestellte Glashohlkugeln. |
| FR2671072B1 (fr) * | 1990-11-14 | 1993-12-03 | Saint Gobain Vitrage Internal | Verre silico-sodo-calcique, microspheres obtenues a partir de ce verre et procede pour leur fabrication. |
| US5500287A (en) * | 1992-10-30 | 1996-03-19 | Innovation Associates, Inc. | Thermal insulating material and method of manufacturing same |
| EP1172341A4 (en) * | 1999-06-30 | 2003-06-04 | Asahi Glass Co Ltd | FINE, HOLLOW AND SPHERICAL GLASS PARTICLES AND METHOD FOR THEIR PRODUCTION |
| US6951589B2 (en) * | 2000-01-25 | 2005-10-04 | The Lubrizol Corporation | Water in oil explosive emulsions |
| US6464770B1 (en) * | 2000-08-08 | 2002-10-15 | Advanced Minerals Corporation | Perlite products with controlled particle size distribution |
| US6906009B2 (en) * | 2002-08-14 | 2005-06-14 | 3M Innovative Properties Company | Drilling fluid containing microspheres and use thereof |
| US20060243363A1 (en) * | 2005-04-29 | 2006-11-02 | 3M Innovative Properties Company | Glass microbubble-containing syntactic foams, explosives, and method of making |
-
2004
- 2004-12-03 US US11/004,385 patent/US20060122049A1/en not_active Abandoned
-
2005
- 2005-09-15 MX MX2007006391A patent/MX2007006391A/es unknown
- 2005-09-15 WO PCT/US2005/032887 patent/WO2006062566A1/en not_active Ceased
- 2005-09-15 BR BRPI0518722-2A patent/BRPI0518722A2/pt not_active Application Discontinuation
- 2005-09-15 EP EP05797410.7A patent/EP1833767B1/en not_active Expired - Lifetime
- 2005-09-15 KR KR1020077012385A patent/KR20070085613A/ko not_active Withdrawn
- 2005-09-15 CN CN2005800412180A patent/CN101068753B/zh not_active Expired - Fee Related
- 2005-09-15 JP JP2007544338A patent/JP5139071B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP1833767A1 (en) | 2007-09-19 |
| US20060122049A1 (en) | 2006-06-08 |
| KR20070085613A (ko) | 2007-08-27 |
| BRPI0518722A2 (pt) | 2008-12-02 |
| CN101068753A (zh) | 2007-11-07 |
| CN101068753B (zh) | 2012-02-29 |
| MX2007006391A (es) | 2007-07-11 |
| JP2008521750A (ja) | 2008-06-26 |
| EP1833767B1 (en) | 2019-08-14 |
| WO2006062566A1 (en) | 2006-06-15 |
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