JP5078097B2 - セルロースエーテルを挽く方法 - Google Patents
セルロースエーテルを挽く方法 Download PDFInfo
- Publication number
- JP5078097B2 JP5078097B2 JP2008510569A JP2008510569A JP5078097B2 JP 5078097 B2 JP5078097 B2 JP 5078097B2 JP 2008510569 A JP2008510569 A JP 2008510569A JP 2008510569 A JP2008510569 A JP 2008510569A JP 5078097 B2 JP5078097 B2 JP 5078097B2
- Authority
- JP
- Japan
- Prior art keywords
- cellulose
- cellulose ether
- cationic surfactant
- grinding
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D101/00—Coating compositions based on cellulose, modified cellulose, or cellulose derivatives
- C09D101/08—Cellulose derivatives
- C09D101/26—Cellulose ethers
- C09D101/28—Alkyl ethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
- A61K47/36—Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
- A61K47/38—Cellulose; Derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/24—Macromolecular compounds
- C04B24/38—Polysaccharides or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
- C04B24/24—Macromolecular compounds
- C04B24/38—Polysaccharides or derivatives thereof
- C04B24/383—Cellulose or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/14—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing calcium sulfate cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B40/00—Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
- C04B40/0028—Aspects relating to the mixing step of the mortar preparation
- C04B40/0039—Premixtures of ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/193—Mixed ethers, i.e. ethers with two or more different etherifying groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B11/00—Preparation of cellulose ethers
- C08B11/20—Post-etherification treatments of chemical or physical type, e.g. mixed etherification in two steps, including purification
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/124—Treatment for improving the free-flowing characteristics
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L1/00—Compositions of cellulose, modified cellulose or cellulose derivatives
- C08L1/08—Cellulose derivatives
- C08L1/26—Cellulose ethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L1/00—Compositions of cellulose, modified cellulose or cellulose derivatives
- C08L1/08—Cellulose derivatives
- C08L1/26—Cellulose ethers
- C08L1/28—Alkyl ethers
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
- C04B2103/44—Thickening, gelling or viscosity increasing agents
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00482—Coating or impregnation materials
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2301/00—Characterised by the use of cellulose, modified cellulose or cellulose derivatives
- C08J2301/08—Cellulose derivatives
- C08J2301/26—Cellulose ethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2301/00—Characterised by the use of cellulose, modified cellulose or cellulose derivatives
- C08J2301/08—Cellulose derivatives
- C08J2301/26—Cellulose ethers
- C08J2301/28—Alkyl ethers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Ceramic Engineering (AREA)
- Medicinal Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Structural Engineering (AREA)
- Inorganic Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Pharmacology & Pharmacy (AREA)
- Wood Science & Technology (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Medicinal Preparation (AREA)
- Paints Or Removers (AREA)
Description
a)セルロースエーテルと水との合計重量に基づいて20〜90重量%の水を含むセルロースエーテルと、カチオン性界面活性剤とをミルにおいて挽くステップ;及び
b)挽く間に、挽くステップの前又は挽くステップに続いて、該混合物を乾燥させる任意的なステップ
を含む,セルロースエーテルを挽く方法により達成される。
エチルヒドロキシエチルセルロース(EHEC)の乾燥重量に基づいて計算されて50重量%の水を含むEHECの100重量部の3部が3つのプラスチック袋に入れられた。EHEC/水の塊は10〜20mmの直径を有する。1つの袋(袋A)において,0.01重量部のジデシルジメチルアンモニウムクロライドが添加された。第二の袋(袋B)において,0.01重量部のC14〜C16オレフィンのスルホネートが添加された。第三の袋(袋C)には界面活性剤は添加されなかった。袋A〜Cの中の成分は,各袋の外側への機械的力で激しく攪拌された。
エチルヒドロキシエチルセルロース(EHEC)の乾燥重量に基づいて計算されて50重量%の水を含む100重量部のEHECが,0.01重量部のジデシルジメチルアンモニウムクロライド(カチオン性界面活性剤)と攪拌された。EHECは、混合物中でよく分散された。塊は観察されなかった。次に,混合物はインパクトミルに導入され,そこで乾燥されて,200μm未満の粒子サイズを有する粉末を形成した。ミルの壁にEHECはなかった。
Claims (12)
- a)セルロースエーテルと水との合計重量に基づいて20〜90重量%の水を含むセルロースエーテルと、カチオン性界面活性剤とをミルにおいて挽くステップ;及び
b)挽く間に、又は挽くステップに続いて、該混合物を乾燥させる任意的なステップを含み、該カチオン性界面活性剤が4級アンモニウム塩である、セルロースエーテルを挽く方法。 - カチオン性界面活性剤が、8〜22の炭素原子を含む少なくとも1の炭化水素基を含む4級アンモニウム塩である、請求項1に記載の方法。
- カチオン性界面活性剤が混合物の合計重量に基づいて0.001〜 2重量%の量で存在する、請求項1〜2のいずれか1項に記載の方法。
- カチオン性界面活性剤が混合物の合計重量に基づいて0.01〜0.5 重量%の量で存在する、請求項3に記載の方法。
- セルロースエーテルが、メチルセルロース,ヒドロキシエチルセルロース,メチルヒドロキシエチルセルロース,エチルヒドロキシエチルセルロース,メチルエチルヒドロキシエチルセルロース,ヒドロキシプロピルヒドロキシエチルセルロース,メチルヒドロキシプロピルヒドロキシエチルセルロース,ヒドロキシプロピルセルロース,メチルヒドロキシプロピルセルロース,及びエチルヒドロキシプロピルセルロースからなる群から選択されたノニオン性セルロースエーテルである、請求項1〜4のいずれか1項に記載の方法。
- 請求項1〜5のいずれか1項に記載の方法により得られるセルロースエーテル。
- 請求項6に記載のセルロースエーテルを含むセメント組成物。
- 請求項6に記載のセルロースエーテルを含む石膏。
- 請求項6に記載のセルロースエーテルを含むコーティング組成物。
- 請求項6に記載のセルロースエーテルを含む増粘剤。
- 請求項6に記載のセルロースエーテルを含むバインダー。
- 請求項6に記載のセルロースエーテルを含む医薬品。
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP05103978 | 2005-05-12 | ||
EP05103978.2 | 2005-05-12 | ||
US69365705P | 2005-06-24 | 2005-06-24 | |
US60/693,657 | 2005-06-24 | ||
PCT/EP2006/062159 WO2006120194A1 (en) | 2005-05-12 | 2006-05-09 | Process for grinding cellulose ether |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2008540759A JP2008540759A (ja) | 2008-11-20 |
JP5078097B2 true JP5078097B2 (ja) | 2012-11-21 |
Family
ID=34939809
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2008510569A Expired - Fee Related JP5078097B2 (ja) | 2005-05-12 | 2006-05-09 | セルロースエーテルを挽く方法 |
Country Status (11)
Country | Link |
---|---|
US (1) | US9523014B2 (ja) |
EP (1) | EP1879943B1 (ja) |
JP (1) | JP5078097B2 (ja) |
KR (2) | KR20130064143A (ja) |
CN (1) | CN101175793B (ja) |
AT (1) | ATE518902T1 (ja) |
BR (1) | BRPI0608962A2 (ja) |
ES (1) | ES2369038T3 (ja) |
MX (1) | MX2007014091A (ja) |
RU (1) | RU2415882C2 (ja) |
WO (1) | WO2006120194A1 (ja) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102007016726A1 (de) * | 2007-04-07 | 2008-10-09 | Dow Wolff Cellulosics Gmbh | Methylhydroxyethylhydroxypropylcellulose (MHEHPC) in mineralisch gebundenen Baustoffsystemen |
EP2177561B1 (de) | 2008-10-16 | 2017-11-22 | Dow Global Technologies LLC | Verweilen und Verteilen eines Aufgabegutes |
JP6034365B2 (ja) * | 2011-04-06 | 2016-11-30 | ダウ グローバル テクノロジーズ エルエルシー | 高い嵩密度、良好な流動性及び改善された冷水分散性を有するセルロース誘導体の製造方法。 |
EP2900753B1 (en) | 2012-09-25 | 2018-07-04 | Dow Global Technologies LLC | Process for producing cellulose derivatives of high bulk density, good flowability and/or dispersibility in cold water as well as low solution color |
KR102109750B1 (ko) * | 2013-06-21 | 2020-05-12 | 롯데정밀화학 주식회사 | 분산성이 향상된 석고 플라스터용 첨가제 조성물 및 그 제조방법 |
US10577432B2 (en) * | 2015-06-05 | 2020-03-03 | Dow Global Technologies Llc | Cellulose ether powders |
Family Cites Families (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1068685B (de) | 1959-11-12 | Henkel ß. Cie. G.m.b.H., Dussel· dorf-Holthausen | Verfahren zur Hersteilung leicht wasserlöslicher Cdllulöseäther | |
US2720464A (en) | 1952-10-24 | 1955-10-11 | Dow Chemical Co | Method of preparing cold-water-soluble powdered cellulose ethers |
GB1224390A (en) * | 1968-01-02 | 1971-03-10 | Wolff & Co Ag | Readily-soluble aluminium-carboxymethylcellulose, its manufacture, and its use for preparing distempers and emulsion paints |
ZA757758B (en) * | 1974-12-13 | 1976-11-24 | Hoechst Ag | Grinding method for cellulose |
US4076935A (en) | 1974-12-13 | 1978-02-28 | Hoechst Aktiengesellschaft | Grinding method for cellulose |
JPS5450025A (en) * | 1977-09-28 | 1979-04-19 | Mitsubishi Chem Ind | Method of making light weight gypsum formed product |
DE3038001A1 (de) * | 1980-10-08 | 1982-05-06 | Henkel KGaA, 4000 Düsseldorf | Verfahren zur herstellung von mikropulvern aus celluloseether oder cellulose |
US4329451A (en) * | 1980-11-03 | 1982-05-11 | The Dow Chemical Company | Preparing an aqueous dispersion of colloidal size particles of a water-insoluble polysaccharide derivative |
JPS596293A (ja) * | 1982-07-05 | 1984-01-13 | ライオン株式会社 | 粒状洗剤用添加剤 |
US4707189A (en) * | 1984-11-07 | 1987-11-17 | Hercules Incorporated | Biostable compositions and the aqueous solutions thereof as thickeners for aqueous-based systems |
DE3543370A1 (de) | 1985-12-07 | 1987-06-11 | Jackering Altenburger Masch | Muehle mit mehreren mahlstufen |
DE3811910C2 (de) | 1988-04-09 | 1997-04-10 | Mahltechnik Goergens Gmbh | Mühle und Verfahren zum gleichzeitigen Mahlen und Trocknen eines feuchten Produkts |
GB2262527A (en) * | 1992-07-02 | 1993-06-23 | Dow Deutschland Inc | Process for grinding cellulose compounds |
DE69618431T2 (de) | 1995-11-24 | 2002-08-29 | Altenburger Maschinen Jaeckering Gmbh | Mechanischer Zerkleinerungsapparat |
DE19641781A1 (de) * | 1996-10-10 | 1998-04-16 | Clariant Gmbh | Verfahren und Vorrichtung zum gleichzeitigen Mahlen und Trocknen eines feuchten Celluloseether enthaltenden Mahlgutes |
TR199903067T2 (xx) | 1997-06-13 | 2000-03-21 | Akzo Nobel N.V. | Hidrofobik olarak de�i�tirilmi� aniyonik sel�loz eterler. |
SE514347C2 (sv) | 1998-08-06 | 2001-02-12 | Akzo Nobel Nv | Nonjonisk cellulosaeter och dess användning som förtjockningsmedel i färgkompositioner |
US7635662B2 (en) * | 1998-09-04 | 2009-12-22 | Chemipro Kasei Kaisha, Ltd. | Compound for color-producing composition, and recording material |
US6197100B1 (en) * | 1998-12-04 | 2001-03-06 | Hercules Incorporated | Dispersible water soluble polymers |
US6165965A (en) * | 1999-04-16 | 2000-12-26 | Spartan Chemical Company, Inc. | Aqueous disinfectant and hard surface cleaning composition and method of use |
DE10009409A1 (de) * | 2000-02-28 | 2001-08-30 | Wolff Walsrode Ag | Verfahren zur Herstellung von pulverförmigen wasserlöslichen Cellulosederivaten |
JP4488458B2 (ja) * | 2000-05-15 | 2010-06-23 | 株式会社Adeka | 液体洗浄剤組成物 |
DE10201344A1 (de) * | 2002-01-16 | 2003-09-18 | Polygal Ag & Co Nachf | Neue Polyurethan- Polysaccharid-Verdicker und ihre Verwendung in wässrigen Lacken und Farben |
-
2006
- 2006-05-09 JP JP2008510569A patent/JP5078097B2/ja not_active Expired - Fee Related
- 2006-05-09 MX MX2007014091A patent/MX2007014091A/es active IP Right Grant
- 2006-05-09 KR KR1020137013120A patent/KR20130064143A/ko not_active Application Discontinuation
- 2006-05-09 RU RU2007146143/05A patent/RU2415882C2/ru active
- 2006-05-09 US US11/913,891 patent/US9523014B2/en active Active
- 2006-05-09 CN CN2006800161416A patent/CN101175793B/zh not_active Expired - Fee Related
- 2006-05-09 KR KR1020077025967A patent/KR101311319B1/ko active IP Right Grant
- 2006-05-09 BR BRPI0608962-3A patent/BRPI0608962A2/pt not_active IP Right Cessation
- 2006-05-09 AT AT06755100T patent/ATE518902T1/de not_active IP Right Cessation
- 2006-05-09 EP EP06755100A patent/EP1879943B1/en active Active
- 2006-05-09 ES ES06755100T patent/ES2369038T3/es active Active
- 2006-05-09 WO PCT/EP2006/062159 patent/WO2006120194A1/en active Application Filing
Also Published As
Publication number | Publication date |
---|---|
CN101175793B (zh) | 2012-10-17 |
ATE518902T1 (de) | 2011-08-15 |
JP2008540759A (ja) | 2008-11-20 |
CN101175793A (zh) | 2008-05-07 |
RU2007146143A (ru) | 2009-06-20 |
KR20130064143A (ko) | 2013-06-17 |
RU2415882C2 (ru) | 2011-04-10 |
EP1879943B1 (en) | 2011-08-03 |
WO2006120194A1 (en) | 2006-11-16 |
KR101311319B1 (ko) | 2013-09-25 |
EP1879943A1 (en) | 2008-01-23 |
US9523014B2 (en) | 2016-12-20 |
MX2007014091A (es) | 2008-02-07 |
BRPI0608962A2 (pt) | 2010-02-17 |
US20080207893A1 (en) | 2008-08-28 |
ES2369038T3 (es) | 2011-11-24 |
KR20080013896A (ko) | 2008-02-13 |
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