JP4689624B2 - ペプチドまたは核酸マイクロパターン形成を使用してカーボンナノチューブを製造する方法 - Google Patents
ペプチドまたは核酸マイクロパターン形成を使用してカーボンナノチューブを製造する方法 Download PDFInfo
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Description
本発明は、一般に、カーボンナノチューブ技術に関し、より具体的には、パターン化されたアレイのカーボンナノチューブを製造する方法およびシステムに関する。
カーボンナノチューブは、円柱管に巻かれているシート状のグラファイトと考えることができる。グラファイトシートの基本的な反復単位は、長さ約1.42Åの炭素-炭素結合による炭素原子の六角形のリングからなる。それらの製造方法に応じて、チューブは多層型または単層型であってもよい。
より詳細に開示されているように、1つまたは複数のポリマー120、210分子に1つまたは複数の触媒ナノ粒子140、230を結合する段階、基板にポリマー120、210分子を結合する段階、典型的には、ポリマー120、210分子を除去する段階、および触媒ナノ粒子140、230上でカーボンナノチューブを製造する段階を含む、カーボンナノチューブを製造する方法が本明細書に提供される。ポリマー分子120、210は、例えばナノチューブを製造する前に整列されていてもよい核酸120またはペプチド210であってもよい。
ΔE = hνF/2L
によって与えられる。
Egap = 2 y0 acc/d
によってモデル化することができる。
1)流動は、分子内塩基対形成を破壊するのに十分な引っ張り力を提供しないことが多い(Hansma, et al., Nucleic Acids Res. 24: 713(1996))。
2)1本鎖核酸は非常に柔軟であり、乾燥によりほどけないようにするのが困難である。
3)整列される前に強く正に荷電した表面に結合する分子がある。および
4)1本鎖核酸の原子間力顕微鏡(AFM)観察は、高さ不足により困難である。
Claims (26)
- a) シリコンチップ基板上に規定された、触媒が結合する複数の位置を有するシリコンチップ基板を供する段階であって、該触媒が結合する位置のそれぞれが、ペプチド、タンパク質または核酸である生物ポリマー分子上の少なくとも2つの所定の位置の間の間隔により規定される段階と、
b) 少なくとも2つの触媒ナノ粒子を少なくとも2つの生物ポリマー分子に結合する段階と、
c) 該少なくとも2つの生物ポリマー分子を基板に結合する段階と、
d) 該生物ポリマー分子を除去する段階と、
e) 前記触媒ナノ粒子上でカーボンナノチューブを製造する段階と、
を含む方法。 - 生物ポリマー分子がペプチドまたはタンパク質である、請求項1記載の方法。
- 生物ポリマー分子が核酸である、請求項1記載の方法。
- 各触媒ナノ粒子を、生物ポリマー分子のあらかじめ選択した位置に結合する、請求項1記載の方法。
- 生物ポリマー分子を基板に結合する前に、触媒ナノ粒子を生物ポリマー分子に結合する、請求項1記載の方法。
- 生物ポリマー分子を基板に結合した後に、触媒ナノ粒子を生物ポリマー分子に結合する、請求項1記載の方法。
- ナノチューブを、規則的なアレイで基板に結合する、請求項1記載の方法。
- 隣接カーボンナノチューブ間の距離が均一である、請求項7記載の方法。
- カーボンナノチューブを、基板の選択した領域に結合する、請求項1記載の方法。
- 選択した各領域内のナノチューブの分布が非ランダムである、請求項9記載の方法。
- 基板に生物ポリマー分子を整列させる段階をさらに含む、請求項1記載の方法。
- 生物ポリマー分子が、光ピンセット、直流電場、交流電場、磁場、分子コーミングまたは微小流体流動によって整列される、請求項11記載の方法。
- 生物ポリマー分子が2本鎖DNA/強制流動整列によって整列される、請求項12記載の方法。
- 触媒ナノ粒子がフェリチンを含む、請求項1記載の方法。
- 炭化水素ガスによる化学蒸着を使用してカーボンナノチューブを製造する段階をさらに含む、請求項1記載の方法。
- ナノ粒子が、ビオチン-アビジン結合またはビオチン-ストレプトアビジン結合を使用して生物ポリマーに結合される、請求項1記載の方法。
- 基板が、ケイ素、酸化ケイ素、二酸化ケイ素、窒化ケイ素、ゲルマニウム、1つまたは複数の金属および/または石英を含む、請求項1記載の方法。
- 触媒ナノ粒子が、鉄、ニッケル、モリブデン、コバルト、亜鉛、ルテニウムおよび/またはコバルトを含む、請求項1記載の方法。
- 基板の1つまたは複数の選択した領域に結合されている規則的なアレイのカーボンナノチューブを含み、該ナノチューブが非ランダムパターンで各領域に配列されている、請求項1記載の方法に用いるための装置。
- 隣接ナノチューブ間の距離が均一である、請求項19記載の装置。
- 各ナノチューブが触媒ナノ粒子に結合されている、請求項19記載の装置。
- ナノチューブの径が均一である、請求項19記載の装置。
- 基板に結合される複数のカーボンナノチューブを含む装置であって、該ナノチューブが:
a) シリコンチップ基板上に規定された、触媒が結合する複数の位置を有するシリコンチップ基板を供する段階であって、該触媒が結合する位置のそれぞれが、ペプチド、タンパク質または核酸である生物ポリマー分子上の少なくとも2つの所定の位置の間の間隔により規定される段階と、
b) 少なくとも2つの触媒ナノ粒子を少なくとも2つの生物ポリマー分子に結合する段階と、
c) 該少なくとも2つの生物ポリマー分子を基板に結合する段階と、
d) 該生物ポリマー分子を除去する段階と、
e) 前記触媒ナノ粒子上でカーボンナノチューブを製造する段階と、
を含む方法によって製造される装置。 - 基板が、ケイ素、酸化ケイ素、二酸化ケイ素、窒化ケイ素、ゲルマニウム、1つまたは複数の金属および/または石英を含む、請求項23記載の装置。
- 触媒ナノ粒子が、鉄、ニッケル、モリブデン、コバルト、亜鉛、ルテニウムおよび/またはコバルトを含む、請求項23記載の装置。
- 触媒ナノ粒子がフェリチンを含む、請求項23記載の装置。
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US10/750,141 US20050151126A1 (en) | 2003-12-31 | 2003-12-31 | Methods of producing carbon nanotubes using peptide or nucleic acid micropatterning |
US10/750,141 | 2003-12-31 | ||
PCT/US2004/043364 WO2005066367A2 (en) | 2003-12-31 | 2004-12-24 | Methods of producing carbon nanotubes using peptide or nucleic acid micropatterning |
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JP2007521222A JP2007521222A (ja) | 2007-08-02 |
JP4689624B2 true JP4689624B2 (ja) | 2011-05-25 |
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EP (1) | EP1699938A2 (ja) |
JP (1) | JP4689624B2 (ja) |
KR (1) | KR20070004596A (ja) |
CN (1) | CN101014532A (ja) |
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2004
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- 2004-12-24 EP EP04818073A patent/EP1699938A2/en not_active Withdrawn
- 2004-12-24 JP JP2006547383A patent/JP4689624B2/ja not_active Expired - Fee Related
- 2004-12-24 KR KR1020067015153A patent/KR20070004596A/ko not_active Application Discontinuation
- 2004-12-24 CN CNA2004800376029A patent/CN101014532A/zh active Pending
- 2004-12-28 TW TW093140923A patent/TWI310022B/zh not_active IP Right Cessation
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2006
- 2006-01-31 US US11/344,713 patent/US20090170725A1/en not_active Abandoned
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JP2007521222A (ja) | 2007-08-02 |
US20090169466A1 (en) | 2009-07-02 |
CN101014532A (zh) | 2007-08-08 |
WO2005066367A3 (en) | 2007-03-01 |
EP1699938A2 (en) | 2006-09-13 |
TW200525054A (en) | 2005-08-01 |
US20090170725A1 (en) | 2009-07-02 |
KR20070004596A (ko) | 2007-01-09 |
TWI310022B (en) | 2009-05-21 |
US20050151126A1 (en) | 2005-07-14 |
WO2005066367A2 (en) | 2005-07-21 |
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