JP4433676B2 - 炭素繊維強化炭素複合材料の製造方法 - Google Patents
炭素繊維強化炭素複合材料の製造方法 Download PDFInfo
- Publication number
- JP4433676B2 JP4433676B2 JP2003009312A JP2003009312A JP4433676B2 JP 4433676 B2 JP4433676 B2 JP 4433676B2 JP 2003009312 A JP2003009312 A JP 2003009312A JP 2003009312 A JP2003009312 A JP 2003009312A JP 4433676 B2 JP4433676 B2 JP 4433676B2
- Authority
- JP
- Japan
- Prior art keywords
- carbon fiber
- composite material
- less
- carbon
- gpa
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 229920000049 Carbon (fiber) Polymers 0.000 title claims description 97
- 239000004917 carbon fiber Substances 0.000 title claims description 97
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 title claims description 85
- 239000002131 composite material Substances 0.000 title claims description 60
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims description 33
- 229910052799 carbon Inorganic materials 0.000 title claims description 33
- 238000004519 manufacturing process Methods 0.000 title claims description 18
- 238000000034 method Methods 0.000 claims description 26
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 19
- 239000001301 oxygen Substances 0.000 claims description 19
- 229910052760 oxygen Inorganic materials 0.000 claims description 19
- 239000011230 binding agent Substances 0.000 claims description 12
- 239000007789 gas Substances 0.000 claims description 12
- 238000001179 sorption measurement Methods 0.000 claims description 12
- 230000003647 oxidation Effects 0.000 claims description 9
- 238000007254 oxidation reaction Methods 0.000 claims description 9
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 claims description 8
- 229910052743 krypton Inorganic materials 0.000 claims description 7
- DNNSSWSSYDEUBZ-UHFFFAOYSA-N krypton atom Chemical compound [Kr] DNNSSWSSYDEUBZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000008151 electrolyte solution Substances 0.000 claims description 5
- 239000000835 fiber Substances 0.000 description 29
- 238000012360 testing method Methods 0.000 description 13
- 239000011159 matrix material Substances 0.000 description 12
- 238000005259 measurement Methods 0.000 description 12
- 239000000523 sample Substances 0.000 description 10
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 8
- 238000003763 carbonization Methods 0.000 description 8
- 239000000463 material Substances 0.000 description 8
- 229920005989 resin Polymers 0.000 description 8
- 239000011347 resin Substances 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- 238000012937 correction Methods 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- 239000005011 phenolic resin Substances 0.000 description 5
- 239000011295 pitch Substances 0.000 description 5
- 230000008646 thermal stress Effects 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 238000005087 graphitization Methods 0.000 description 4
- 239000011229 interlayer Substances 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- 230000035945 sensitivity Effects 0.000 description 4
- 238000004513 sizing Methods 0.000 description 4
- 238000004381 surface treatment Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000012298 atmosphere Substances 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 125000000524 functional group Chemical group 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 229920002239 polyacrylonitrile Polymers 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 238000009864 tensile test Methods 0.000 description 3
- 229920005992 thermoplastic resin Polymers 0.000 description 3
- 229920001187 thermosetting polymer Polymers 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- 238000004438 BET method Methods 0.000 description 2
- YLQBMQCUIZJEEH-UHFFFAOYSA-N Furan Chemical compound C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- 229920000297 Rayon Polymers 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 229920000180 alkyd Polymers 0.000 description 2
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 2
- 238000010000 carbonizing Methods 0.000 description 2
- 239000011294 coal tar pitch Substances 0.000 description 2
- 239000004020 conductor Substances 0.000 description 2
- 238000001723 curing Methods 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003792 electrolyte Substances 0.000 description 2
- 239000003822 epoxy resin Substances 0.000 description 2
- 239000002783 friction material Substances 0.000 description 2
- 238000013007 heat curing Methods 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 239000011301 petroleum pitch Substances 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- 229920000647 polyepoxide Polymers 0.000 description 2
- -1 polyethylene Polymers 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- 229920000915 polyvinyl chloride Polymers 0.000 description 2
- 239000004800 polyvinyl chloride Substances 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 239000002964 rayon Substances 0.000 description 2
- 239000012783 reinforcing fiber Substances 0.000 description 2
- 239000011342 resin composition Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 239000002344 surface layer Substances 0.000 description 2
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 2
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- 229920001342 Bakelite® Polymers 0.000 description 1
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
- 239000010432 diamond Substances 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000007849 furan resin Substances 0.000 description 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 230000001678 irradiating effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000006902 nitrogenation reaction Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 238000011417 postcuring Methods 0.000 description 1
- 239000002296 pyrolytic carbon Substances 0.000 description 1
- 229920003987 resole Polymers 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 238000007740 vapor deposition Methods 0.000 description 1
Landscapes
- Ceramic Products (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2003009312A JP4433676B2 (ja) | 2003-01-17 | 2003-01-17 | 炭素繊維強化炭素複合材料の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2003009312A JP4433676B2 (ja) | 2003-01-17 | 2003-01-17 | 炭素繊維強化炭素複合材料の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2004217485A JP2004217485A (ja) | 2004-08-05 |
| JP2004217485A5 JP2004217485A5 (enExample) | 2005-12-08 |
| JP4433676B2 true JP4433676B2 (ja) | 2010-03-17 |
Family
ID=32898850
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2003009312A Expired - Fee Related JP4433676B2 (ja) | 2003-01-17 | 2003-01-17 | 炭素繊維強化炭素複合材料の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP4433676B2 (enExample) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5226238B2 (ja) * | 2007-03-30 | 2013-07-03 | 東邦テナックス株式会社 | 炭素繊維及びそれを用いた複合材料 |
| JP5251655B2 (ja) * | 2009-03-24 | 2013-07-31 | 東レ株式会社 | 炭素繊維およびその製造方法 |
-
2003
- 2003-01-17 JP JP2003009312A patent/JP4433676B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JP2004217485A (ja) | 2004-08-05 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Sun et al. | Controllable construction of gradient modulus intermediate layer on high strength and high modulus carbon fibers to enhance interfacial properties of epoxy composites by efficient electrochemical grafting | |
| EP3168334B1 (en) | Carbon fiber bundle and method for manufacturing same | |
| Kim et al. | A study on the microstructural changes and mechanical behaviors of carbon fibers induced by optimized electrochemical etching | |
| CN104805534B (zh) | 制备高强度高模量石墨纤维的方法 | |
| US20100266827A1 (en) | Carbon fiber and composite material using the same | |
| JP5907321B1 (ja) | 炭素繊維束およびその製造方法 | |
| JP2519042B2 (ja) | 炭素炭素複合材の製造方法 | |
| JP2664047B2 (ja) | 炭素繊維強化炭素複合材料の製造方法 | |
| JP4726102B2 (ja) | 炭素繊維及びその製造方法 | |
| JP4433676B2 (ja) | 炭素繊維強化炭素複合材料の製造方法 | |
| JP4953410B2 (ja) | 炭素繊維およびその製造方法 | |
| JP2004244258A (ja) | 炭素繊維強化炭素複合材料用炭素繊維およびその製造方法 | |
| JP2010047865A (ja) | 複合材料用炭素繊維とそれを用いた複合材料 | |
| JP2004277192A (ja) | 炭素繊維強化炭素複合材料用炭素繊維およびその製造方法 | |
| Yip et al. | Effect of surface oxygen on adhesion of carbon fiber reinforced composites | |
| JP5226238B2 (ja) | 炭素繊維及びそれを用いた複合材料 | |
| JPH07187833A (ja) | 炭素繊維強化炭素複合材料 | |
| JP7005822B1 (ja) | Ｃ／ｃコンポジット及びその製造方法、並びに熱処理用治具及びその製造方法 | |
| JP5251655B2 (ja) | 炭素繊維およびその製造方法 | |
| JPH0816032B2 (ja) | 高強度炭素炭素複合材の製造方法 | |
| JP5455408B2 (ja) | ポリアクリロニトリル系炭素繊維及びその製造方法 | |
| JP2004277907A (ja) | 炭素繊維およびその製造方法 | |
| JPH054463B2 (enExample) | ||
| JP7338176B2 (ja) | 炭素繊維強化ビニルエステル樹脂組成物およびその製造方法 | |
| JP5419768B2 (ja) | 炭素繊維の表面処理方法、及び同処理方法により製造する炭素繊維 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| A521 | Written amendment |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20051026 |
|
| A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20051026 |
|
| A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20090609 |
|
| A521 | Written amendment |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20090807 |
|
| TRDD | Decision of grant or rejection written | ||
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 Effective date: 20091208 |
|
| A01 | Written decision to grant a patent or to grant a registration (utility model) |
Free format text: JAPANESE INTERMEDIATE CODE: A01 |
|
| A61 | First payment of annual fees (during grant procedure) |
Free format text: JAPANESE INTERMEDIATE CODE: A61 Effective date: 20091221 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20130108 Year of fee payment: 3 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20130108 Year of fee payment: 3 |
|
| FPAY | Renewal fee payment (event date is renewal date of database) |
Free format text: PAYMENT UNTIL: 20140108 Year of fee payment: 4 |
|
| LAPS | Cancellation because of no payment of annual fees |