JP4272067B2 - コロイド溶液の制御された蒸発のための連続法 - Google Patents
コロイド溶液の制御された蒸発のための連続法 Download PDFInfo
- Publication number
- JP4272067B2 JP4272067B2 JP2003555855A JP2003555855A JP4272067B2 JP 4272067 B2 JP4272067 B2 JP 4272067B2 JP 2003555855 A JP2003555855 A JP 2003555855A JP 2003555855 A JP2003555855 A JP 2003555855A JP 4272067 B2 JP4272067 B2 JP 4272067B2
- Authority
- JP
- Japan
- Prior art keywords
- colloidal solution
- evaporation
- evaporation zone
- pressure
- zone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000001704 evaporation Methods 0.000 title claims abstract description 163
- 230000008020 evaporation Effects 0.000 title claims abstract description 142
- 238000011437 continuous method Methods 0.000 title 1
- 238000000034 method Methods 0.000 claims abstract description 46
- 239000007788 liquid Substances 0.000 claims abstract description 16
- 239000002245 particle Substances 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims description 30
- 238000009835 boiling Methods 0.000 claims description 5
- 230000008569 process Effects 0.000 abstract description 26
- 238000003825 pressing Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 122
- 239000000463 material Substances 0.000 description 39
- 239000007787 solid Substances 0.000 description 14
- 230000008859 change Effects 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 11
- 238000004094 preconcentration Methods 0.000 description 8
- 239000000084 colloidal system Substances 0.000 description 7
- 239000002609 medium Substances 0.000 description 6
- 239000000919 ceramic Substances 0.000 description 5
- 235000013305 food Nutrition 0.000 description 5
- 239000011521 glass Substances 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 229920000642 polymer Polymers 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- 229920002261 Corn starch Polymers 0.000 description 4
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- 239000008120 corn starch Substances 0.000 description 4
- 239000000416 hydrocolloid Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000012736 aqueous medium Substances 0.000 description 3
- 230000015556 catabolic process Effects 0.000 description 3
- 238000006731 degradation reaction Methods 0.000 description 3
- 239000004816 latex Substances 0.000 description 3
- 229920000126 latex Polymers 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 239000003125 aqueous solvent Substances 0.000 description 2
- 235000021551 crystal sugar Nutrition 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000011552 falling film Substances 0.000 description 2
- 239000010408 film Substances 0.000 description 2
- 238000010304 firing Methods 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 235000021552 granulated sugar Nutrition 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 229910044991 metal oxide Inorganic materials 0.000 description 2
- 150000004706 metal oxides Chemical class 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229910000030 sodium bicarbonate Inorganic materials 0.000 description 2
- 235000017557 sodium bicarbonate Nutrition 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000000346 sugar Nutrition 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 229910052581 Si3N4 Inorganic materials 0.000 description 1
- 238000010793 Steam injection (oil industry) Methods 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 229910001593 boehmite Inorganic materials 0.000 description 1
- 235000008429 bread Nutrition 0.000 description 1
- 230000005587 bubbling Effects 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000001879 gelation Methods 0.000 description 1
- 239000008131 herbal destillate Substances 0.000 description 1
- FAHBNUUHRFUEAI-UHFFFAOYSA-M hydroxidooxidoaluminium Chemical compound O[Al]=O FAHBNUUHRFUEAI-UHFFFAOYSA-M 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 229910000021 magnesium carbonate Inorganic materials 0.000 description 1
- 239000006247 magnetic powder Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000001247 metal acetylides Chemical class 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 150000004767 nitrides Chemical class 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000002390 rotary evaporation Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- HQVNEWCFYHHQES-UHFFFAOYSA-N silicon nitride Chemical compound N12[Si]34N5[Si]62N3[Si]51N64 HQVNEWCFYHHQES-UHFFFAOYSA-N 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 150000004772 tellurides Chemical class 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/06—Flash distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/42—Regulation; Control
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S159/00—Concentrating evaporators
- Y10S159/08—Multieffect or multistage
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Colloid Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/028,216 US6869501B2 (en) | 2001-12-20 | 2001-12-20 | Continuous process for controlled concentration of colloidal solutions |
| PCT/US2002/036231 WO2003055268A2 (en) | 2001-12-20 | 2002-11-12 | Continuous process for controlled evaporation of colloidal solutions |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2005514189A JP2005514189A (ja) | 2005-05-19 |
| JP2005514189A5 JP2005514189A5 (enExample) | 2006-01-05 |
| JP4272067B2 true JP4272067B2 (ja) | 2009-06-03 |
Family
ID=21842189
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2003555855A Expired - Fee Related JP4272067B2 (ja) | 2001-12-20 | 2002-11-12 | コロイド溶液の制御された蒸発のための連続法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US6869501B2 (enExample) |
| EP (1) | EP1455917B1 (enExample) |
| JP (1) | JP4272067B2 (enExample) |
| KR (1) | KR100945364B1 (enExample) |
| AT (1) | ATE330682T1 (enExample) |
| AU (1) | AU2002352641A1 (enExample) |
| DE (1) | DE60212704T2 (enExample) |
| WO (1) | WO2003055268A2 (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070179216A1 (en) * | 2005-05-02 | 2007-08-02 | Degussa Ag | Method for producing aqueous polyurethane dispersions by means of flash evaporation |
| US8178045B2 (en) * | 2007-12-17 | 2012-05-15 | University Of Louisville Research Foundation, Inc. | Interchangeable preconcentrator connector assembly |
| WO2010014950A1 (en) * | 2008-07-31 | 2010-02-04 | University Of Louisville Rasearch Foundation, Inc. | Large volume analyte preconcentrator |
| US8448532B2 (en) * | 2009-03-18 | 2013-05-28 | The United States Of America As Represented By The Secretary Of The Navy | Actively cooled vapor preconcentrator |
| US8569691B2 (en) | 2009-11-24 | 2013-10-29 | University Of Louisville Research Foundation | Preconcentrator for analysis instruments |
| US8690866B2 (en) | 2010-08-23 | 2014-04-08 | Covidien Lp | Ablation devices utilizing exothermic chemical reactions, system including same, and methods of ablating tissue using same |
| ES2815073T3 (es) | 2013-06-27 | 2021-03-29 | Ivoclar Vivadent Inc | Circona nanocristalina y métodos de procesamiento de la misma |
| US9822039B1 (en) | 2016-08-18 | 2017-11-21 | Ivoclar Vivadent Ag | Metal oxide ceramic nanomaterials and methods of making and using same |
| CN115177965B (zh) * | 2022-07-11 | 2023-04-25 | 西安国康瑞金制药有限公司 | 一种从黄体酮生产母液中回收黄体酮的系统和方法 |
Family Cites Families (70)
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| BE619411A (enExample) | 1961-06-26 | |||
| GB1046185A (en) | 1963-09-27 | 1966-10-19 | Mobay Chemical Corp | Process for the recovery of polycarbonates from solutions thereof |
| US3493470A (en) | 1966-05-27 | 1970-02-03 | Phillips Petroleum Co | Volatile components by vaporization while maintaining the desired rate of vaporization by overhead flow control |
| US3470070A (en) | 1966-12-06 | 1969-09-30 | Phillips Petroleum Co | Flashing viscous polymer solutions |
| US3538193A (en) | 1967-04-06 | 1970-11-03 | Copolymer Rubber & Chem Corp | Recovery of polymeric materials from organic reaction mixtures |
| US3586089A (en) | 1967-05-02 | 1971-06-22 | Mitsui Petrochemical Ind | Method and apparatus for separating and drying organic high molecular weight substances |
| US3642492A (en) | 1967-06-01 | 1972-02-15 | Ralston Purina Co | Method of preparing a simulated skim milk |
| US3444052A (en) | 1967-12-11 | 1969-05-13 | Phillips Petroleum Co | Flash vaporization with vapor flow streams controlled by liquid level |
| US3495648A (en) | 1968-03-11 | 1970-02-17 | Pet Inc | Microwave apparatus for evaporating liquid mixtures |
| US3585104A (en) | 1968-07-29 | 1971-06-15 | Theodor N Kleinert | Organosolv pulping and recovery process |
| US3618588A (en) | 1969-01-14 | 1971-11-09 | Pepsico Inc | Caramel color manufacture |
| US3947376A (en) | 1969-04-28 | 1976-03-30 | Nalco Chemical Company | Silica sols containing large particle size silica |
| US3656534A (en) | 1969-05-06 | 1972-04-18 | Parkson Corp | Concentration by continuous flash evaporation |
| US3709706A (en) | 1969-05-16 | 1973-01-09 | Minnesota Mining & Mfg | Refractory fibers and other articles of zirconia and silica mixtures |
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| NL6913855A (enExample) | 1969-07-09 | 1971-03-15 | ||
| BE758596A (fr) | 1969-11-08 | 1971-05-06 | Basf Ag | Procede pour l'elimination de monomeres volatils a partir de solutions de polymeres d'acrylonitrile ainsi que leur concentration |
| US3582365A (en) | 1970-04-27 | 1971-06-01 | Food Enterprises Inc | Method and apparatus for treating milk and other liquid products |
| FR2096690B1 (enExample) | 1970-06-08 | 1974-08-09 | Inst Francais Du Petrole | |
| US3862014A (en) | 1971-01-26 | 1975-01-21 | Florida State | Distillation apparatus for recovering citrus essence |
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| US3857704A (en) * | 1971-03-05 | 1974-12-31 | Bp Chem Int Ltd | Mercury recovery process |
| JPS5414075B2 (enExample) | 1971-11-05 | 1979-06-04 | ||
| US3853839A (en) | 1972-01-19 | 1974-12-10 | Ralston Purina Co | Method of forming protein food product |
| US3852503A (en) | 1972-01-19 | 1974-12-03 | Ralston Purina Co | Method of making puddings containing soy protein |
| US3941664A (en) | 1972-08-29 | 1976-03-02 | Phillips Petroleum Company | Control for diluent removal from poly(arylene sulfide) reactor product |
| CA1032328A (en) | 1972-08-30 | 1978-06-06 | Crown Zellerbach International | Process for making discrete fibers by flashing a polymer solution having water dispersed therein |
| US3901673A (en) | 1972-12-15 | 1975-08-26 | Phillips Petroleum Co | Recovery of natural gas liquids by partial condensation |
| US3966538A (en) | 1973-01-09 | 1976-06-29 | Monsanto Company | Falling strand devolatilization apparatus |
| JPS5118781A (ja) | 1974-08-06 | 1976-02-14 | Mitsubishi Heavy Ind Ltd | Kobunshizairyoyoekikara kobunshizairyono bunrihoho |
| US4086414A (en) * | 1974-08-19 | 1978-04-25 | Ethyl Corporation | Steam stripping polyvinyl chloride resins |
| DE2511846A1 (de) | 1975-03-18 | 1976-09-23 | Franken Zuckerfab | Verfahren zur herstellung von fondantmasse und fondant-zubereitungen |
| US4038129A (en) | 1975-07-09 | 1977-07-26 | Wreszinski Rolf W | Method and apparatus for concentrating liquids |
| US4047965A (en) | 1976-05-04 | 1977-09-13 | Minnesota Mining And Manufacturing Company | Non-frangible alumina-silica fibers |
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-
2001
- 2001-12-20 US US10/028,216 patent/US6869501B2/en not_active Expired - Lifetime
-
2002
- 2002-11-12 WO PCT/US2002/036231 patent/WO2003055268A2/en not_active Ceased
- 2002-11-12 AU AU2002352641A patent/AU2002352641A1/en not_active Abandoned
- 2002-11-12 DE DE60212704T patent/DE60212704T2/de not_active Expired - Lifetime
- 2002-11-12 EP EP02789588A patent/EP1455917B1/en not_active Expired - Lifetime
- 2002-11-12 JP JP2003555855A patent/JP4272067B2/ja not_active Expired - Fee Related
- 2002-11-12 AT AT02789588T patent/ATE330682T1/de not_active IP Right Cessation
- 2002-11-12 KR KR1020047009538A patent/KR100945364B1/ko not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| KR20040075889A (ko) | 2004-08-30 |
| WO2003055268A2 (en) | 2003-07-03 |
| KR100945364B1 (ko) | 2010-03-08 |
| EP1455917B1 (en) | 2006-06-21 |
| JP2005514189A (ja) | 2005-05-19 |
| ATE330682T1 (de) | 2006-07-15 |
| US20030131948A1 (en) | 2003-07-17 |
| EP1455917A2 (en) | 2004-09-15 |
| US6869501B2 (en) | 2005-03-22 |
| WO2003055268A3 (en) | 2003-12-31 |
| AU2002352641A1 (en) | 2003-07-09 |
| DE60212704D1 (de) | 2006-08-03 |
| AU2002352641A8 (en) | 2003-07-09 |
| DE60212704T2 (de) | 2007-06-28 |
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