JP2021517522A - 非放射性安定同位元素を用いた優環境熱遮蔽フィルム及びその製造方法 - Google Patents
非放射性安定同位元素を用いた優環境熱遮蔽フィルム及びその製造方法 Download PDFInfo
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Abstract
Description
Claims (30)
- 基材層と、前記基材層の一面に形成された熱遮蔽層を含み、前記熱遮蔽層が、非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物を含むことを特徴とする、非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物が、酸素が欠乏したことを特徴とする、請求項1に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物は、(Y)Ax (182、183、184、186)W1O(3−n)形態の六方晶系型構造を形成することを特徴とする、請求項2に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記(Y)Aが、非放射性アルカリ金属元素または非放射性アルカリ土金属元素であることを特徴とする、請求項3に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記(Y)Aが、(23)Na、(39、41)K、(85)Rb、(133)Cs、(24、25、26)Mg、及び(42、43、44)Caのうち、いずれか1つであることを特徴とする、請求項4に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物が、非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)水和物を、300〜600℃の範囲でか焼させて、水酸基及び水分子を除去し、無定形を形成することを特徴とする、請求項3に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物が、前記か焼の以後、不活性ガスを投入した還元焼成により、酸素が欠乏した(Y)Ax (182、183、184、186)W1O(3−n)形態の六方晶系型構造を形成することを特徴とする、請求項6に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記不活性ガスが、N2、Ar、Ne、及びCO3のうち、いずれか1つ以上を含むことを特徴とする、請求項7に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記熱遮蔽層が、酸素が欠乏した前記非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物の耐熱性及び耐久性を向上させる不動態化皮膜をさらに含むことを特徴とする、請求項2に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記不動態化皮膜が、有機酸金属キレート化合物を含むことを特徴とする、請求項9に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記有機酸金属キレート(Chelate)化合物は、R1−M−R2構造を有し、前記Mは、Cu、Ag、Zn、Ni、W,及びCoのうちのいずれか1つの元素であり、前記R1及びR2は、低分子型グルタミン酸(Glutamic Acid)及び高分子型ナトリウムポリアスパーテート(Sodium Poly Aspartate)のうち、いずれか1つであることを特徴とする、請求項10に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 前記基材層は、ポリエチレンテレフタレート(Polyethylene Terephthalate)であることを特徴とする、請求項1に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルム。
- 基材層を提供する基材層提供ステップと、前記基材層提供ステップの後で、前記基材層の一面に非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物を含む熱遮蔽層を形成する熱遮蔽層形成ステップを含むことを特徴とする、非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物が、酸素が欠乏したことを特徴とする、請求項13に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物が、(Y)Ax (182、183、184、186)W1O(3−n)形態の六方晶系型構造を形成することを特徴とする、請求項14に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記(Y)Aが、非放射性アルカリ金属元素または非放射性アルカリ土金属元素であることを特徴とする、請求項15に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記(Y)Aが、(23)Na、(39、41)K、(85)Rb、(133)Cs、(24、25、26)Mg、及び(42、43、44)Caのうち、いずれか1つの元素であることを特徴とする、請求項16に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記熱遮蔽層形成ステップは、非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物を生成する非放射性化合物形成ステップと、前記非放射性化合物形成ステップの後で、前記非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物に不動態化皮膜を形成する不動態化皮膜ステップと、前記不動態化皮膜ステップの後で、前記基材層にコーティング膜を形成するコーティングステップとを含むことを特徴とする、請求項15に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記非放射性化合物形成ステップが、液状沈殿法により非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)水和物を合成する合成ステップと、前記合成ステップの後で、前記非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)水和物を300〜600℃の範囲でか焼させて水酸基及び水分子を除去し、無定形を形成する1次か焼ステップと、前記1次か焼ステップの後で、酸素が欠乏した(Y)Ax (182、183、184、186)W1O(3−n)形態の六方晶系型構造を形成するために不活性ガスの投入下に還元焼成をする2次還元焼成ステップを含むことを特徴とする、請求項18に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記不動態化皮膜ステップは、有機酸金属キレート化合物を製造する有機酸金属キレート化合物製造ステップと、前記有機酸金属キレート化合物製造ステップの後で、分散ゾルを形成する分散ゾル形成ステップを含むことを特徴とする、請求項18に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記有機酸金属キレート化合物製造ステップは、遷移金属を含む前駆体を有機酸溶媒に溶解させて、60〜80℃で4〜5時間の間撹拌してリフラックス(Reflux)させることを特徴とする、請求項20に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記分散ゾル形成ステップが、非放射性安定同位元素タングステンブロンズ(Tungsten Bronze)化合物20〜30重量%と、分散剤1〜10重量%と、有機酸金属キレート化合物5〜10重量%を含む分散ゾルを形成することを特徴とする、請求項20に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記コーティングステップが、コーティングゾルを形成するコーティングゾル形成ステップと、前記コーティングゾル形成ステップの後で、前記コーティングゾルを前記基材層に塗布するコーティングゾル塗布ステップと、前記コーティングゾル塗布ステップの後で、コーティングゾルが塗布された基材層を熱風乾燥及び紫外線硬化させる乾燥硬化ステップとを含むことを特徴とする、請求項18に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記コーティングゾル形成ステップが、分散ゾル40〜50重量%と、バインダー40〜50重量%と、有機溶剤10〜20重量%を含むコーティングゾルを形成することを特徴とする、請求項23に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記バインダーが、光重合体として紫外線照射により光重合を起こすオリゴマー(Oligomer)、モノマー(Monomer)、光開始剤を含むことを特徴とする、請求項24に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記有機溶剤が、メチルエチルケトン(Methyl Ethyl Ketone)、トルエン(Toluene)、エチルアセテート(Ethyl Acetate)、イソプロピルアルコール(Iso Propyl Alcohol)、エチルセロソルブ(Ethyl Cellosolve)、イソブチルアルコール(Isobutyl Alcohol)、ジメチルホルムアミド(Dimethylformamide)、エタノール(Ethanol)、ブチルセロソルブ(Butyl Cellosolve)、キシレン(Xylene)、1−オクタノール(1-Octanol)、ジエチレングリコール(Diethylene Glycol)、ニトロベンゼン(Nitrobenzene)のうち、いずれか1つ以上を含むことを特徴とする、請求項24に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記コーティングゾル塗布ステップは、マイクログラビア(Micro Gravure)コーティング、ナイフ(Knife)コーティング、及びロールツーロール(Roll to Roll)コーティングのうち、いずれか1つを使用することを特徴とする、請求項23に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記コーティングゾル塗布ステップは、コーティング塗膜の厚さを3〜4μmにすることを特徴とする、請求項23に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記熱遮蔽フィルム製造方法は、前記熱遮蔽層形成ステップの後で、前記熱遮蔽層の一面に粘着層を形成する粘着層形成ステップをさらに含むことを特徴とする、請求項13から28のうち、いずれか一項に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
- 前記熱遮蔽フィルム製造方法は、前記粘着層形成ステップの後で、前記粘着層の一面に離型紙を付着する離型紙付着ステップをさらに含むことを特徴とする、請求項29に記載の非放射性安定同位元素を用いた優環境熱遮蔽フィルムの製造方法。
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JP2022008462A (ja) | 2022-01-13 |
CN112969744A (zh) | 2021-06-15 |
WO2020218725A1 (ko) | 2020-10-29 |
EP3778733A1 (en) | 2021-02-17 |
US20210246278A1 (en) | 2021-08-12 |
KR102036253B1 (ko) | 2019-10-24 |
JP7117803B2 (ja) | 2022-08-15 |
JP6982914B2 (ja) | 2021-12-17 |
US20210355290A1 (en) | 2021-11-18 |
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US11453755B2 (en) | 2022-09-27 |
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