JP2020533259A5 - - Google Patents
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- Publication number
- JP2020533259A5 JP2020533259A5 JP2020505855A JP2020505855A JP2020533259A5 JP 2020533259 A5 JP2020533259 A5 JP 2020533259A5 JP 2020505855 A JP2020505855 A JP 2020505855A JP 2020505855 A JP2020505855 A JP 2020505855A JP 2020533259 A5 JP2020533259 A5 JP 2020533259A5
- Authority
- JP
- Japan
- Prior art keywords
- methylpyrrolidinium
- bis
- molar ratio
- reaction mixture
- source
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000002808 molecular sieve Substances 0.000 claims description 10
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 8
- 239000011541 reaction mixture Substances 0.000 claims description 8
- AVFZOVWCLRSYKC-UHFFFAOYSA-N 1-methylpyrrolidine Chemical compound CN1CCCC1 AVFZOVWCLRSYKC-UHFFFAOYSA-N 0.000 claims description 6
- 229910018072 Al 2 O 3 Inorganic materials 0.000 claims description 5
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 5
- VZJFGSRCJCXDSG-UHFFFAOYSA-N Hexamethonium Chemical compound C[N+](C)(C)CCCCCC[N+](C)(C)C VZJFGSRCJCXDSG-UHFFFAOYSA-N 0.000 claims description 4
- 238000002425 crystallisation Methods 0.000 claims description 4
- 230000008025 crystallization Effects 0.000 claims description 4
- 229950002932 hexamethonium Drugs 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 2
- SBXORXZXXUXJIE-UHFFFAOYSA-N butane 1-methylpyrrolidine Chemical compound CCCC.CN1CCCC1 SBXORXZXXUXJIE-UHFFFAOYSA-N 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 239000013078 crystal Substances 0.000 claims description 2
- -1 hydroxide ions Chemical class 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 239000011148 porous material Substances 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- 229910052814 silicon oxide Inorganic materials 0.000 claims description 2
- 229910052708 sodium Inorganic materials 0.000 claims description 2
- 239000011734 sodium Substances 0.000 claims description 2
- 230000002194 synthesizing effect Effects 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 229910021536 Zeolite Inorganic materials 0.000 claims 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 1
- 239000010457 zeolite Substances 0.000 claims 1
- 238000000921 elemental analysis Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US15/697,777 US10053368B1 (en) | 2017-09-07 | 2017-09-07 | Synthesis of AFX framework type molecular sieves |
| US15/697,777 | 2017-09-07 | ||
| PCT/IB2018/054000 WO2019048940A1 (en) | 2017-09-07 | 2018-06-05 | SYNTHESIS OF AFX STRUCTURED TYPE MOLECULAR SIEVES |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2020533259A JP2020533259A (ja) | 2020-11-19 |
| JP2020533259A5 true JP2020533259A5 (OSRAM) | 2021-02-18 |
| JP7052007B2 JP7052007B2 (ja) | 2022-04-11 |
Family
ID=62778959
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2020505855A Active JP7052007B2 (ja) | 2017-09-07 | 2018-06-05 | Ａｆｘ骨格型分子ふるいの合成 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US10053368B1 (OSRAM) |
| EP (1) | EP3678993B1 (OSRAM) |
| JP (1) | JP7052007B2 (OSRAM) |
| KR (1) | KR102569712B1 (OSRAM) |
| CN (1) | CN110944942B (OSRAM) |
| ES (1) | ES2964959T3 (OSRAM) |
| WO (1) | WO2019048940A1 (OSRAM) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3081347B1 (fr) | 2018-05-24 | 2023-07-28 | Ifp Energies Now | Procede de preparation d'une zeolithe de type structural afx de haute purete avec un structurant organique azote |
| CN113039156A (zh) * | 2018-11-12 | 2021-06-25 | 太平洋工业发展公司 | 高热稳定性的afx沸石的制造方法 |
| EP3931152B1 (en) * | 2019-02-27 | 2023-09-06 | Chevron U.S.A. Inc. | Molecular sieve ssz-115, its synthesis and use |
| FR3095130B1 (fr) * | 2019-04-19 | 2022-03-11 | Ifp Energies Now | Synthese rapide d’un catalyseur comprenant une zeolithe de type structural afx et au moins un metal de transition pour la reduction selective de nox |
| FR3095199B1 (fr) | 2019-04-19 | 2021-10-29 | Ifp Energies Now | Procédé de synthèse rapide d'une zeolithe de type structural AFX avec une source de faujasite |
| US10822243B1 (en) * | 2019-07-29 | 2020-11-03 | Chevron U.S.A. Inc. | Molecular sieve SSZ-118, its synthesis and use |
| JP7249911B2 (ja) * | 2019-08-27 | 2023-03-31 | 東ソー株式会社 | ヘキサヒドロベンゾジピロリウム塩及びその用途 |
| WO2022056185A1 (en) * | 2020-09-11 | 2022-03-17 | Basf Corporation | Process for preparing zeolite material having an afx framework structure and zeolite material as prepared |
| CN116022805B (zh) * | 2021-10-26 | 2025-05-13 | 中国石油化工股份有限公司 | 小晶粒zsm-12分子筛及其制备方法 |
| CN116022804B (zh) * | 2021-10-26 | 2025-08-12 | 中国石油化工股份有限公司 | 大晶粒β分子筛及其制备方法 |
| CN117509667A (zh) * | 2023-11-30 | 2024-02-06 | 吉林大学 | 一种晶种辅助合成纳米高硅afx沸石分子筛的方法 |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4508837A (en) * | 1982-09-28 | 1985-04-02 | Chevron Research Company | Zeolite SSZ-16 |
| US5194235A (en) | 1992-08-27 | 1993-03-16 | Chevron Research And Technology Company | Synthesis of SSZ-16 zeolite catalyst |
| US5370851A (en) | 1993-05-27 | 1994-12-06 | Uop | Crystalline silicoalumino phosphates: SAPO-36 and SAPO-56 |
| DE19524148C1 (de) * | 1995-07-03 | 1996-08-29 | Bosch Gmbh Robert | Schwingungsaufnehmer |
| DK2848625T3 (da) * | 2008-08-14 | 2019-10-07 | Genentech Inc | Fremgangsmåder til fjernelse af en kontaminant under anvendelse af ion bytningsmembrankromatografi med forskydning af naturligt forekommende proteiner |
| US7820141B2 (en) * | 2008-10-10 | 2010-10-26 | Chevron U.S.A. Inc. | Molecular sieve SSZ-82 composition of matter and synthesis thereof |
| CA2693582A1 (en) * | 2009-02-27 | 2010-08-27 | Chevron U.S.A. Inc. | Synthesis of molecular sieve ssz-74 using a hydroxide-mediated gel |
| JP5908395B2 (ja) | 2009-04-09 | 2016-04-26 | カリフォルニア インスティチュート オブ テクノロジー | モレキュラーシーブ |
| US9757716B2 (en) * | 2012-12-21 | 2017-09-12 | Exxonmobil Chemical Patents Inc. | Synthesis of ZSM-5 |
| RU2650973C2 (ru) * | 2013-02-05 | 2018-04-18 | Басф Се | Способ получения титансодержащего цеолитного материала, имеющего каркасную структуру mww |
| JP6661615B2 (ja) * | 2014-09-03 | 2020-03-11 | エクソンモービル リサーチ アンド エンジニアリング カンパニーＥｘｘｏｎ Ｒｅｓｅａｒｃｈ Ａｎｄ Ｅｎｇｉｎｅｅｒｉｎｇ Ｃｏｍｐａｎｙ | 新規合成結晶材料のｅｍｍ−２６、その調製、およびその使用 |
| JP6494034B2 (ja) * | 2014-09-18 | 2019-04-03 | 国立大学法人広島大学 | リンを含有するｌｅｖ型結晶性アルミノシリケート、およびその製造方法、ならびにリンを含有するｌｅｖ型結晶性アルミノシリケートを含む触媒 |
| CN107107043A (zh) * | 2014-10-07 | 2017-08-29 | 庄信万丰股份有限公司 | 用于处理废气的分子筛催化剂 |
| CN107106978A (zh) | 2014-11-14 | 2017-08-29 | 庄信万丰股份有限公司 | Afx沸石 |
| JP6430303B2 (ja) * | 2015-03-16 | 2018-11-28 | 国立大学法人横浜国立大学 | Ａｆｘ型ゼオライトの製法 |
| JP6655959B2 (ja) * | 2015-04-17 | 2020-03-04 | 東ソー株式会社 | 微結晶ａｆｘ型アルミノシリケート及びその製造方法 |
| WO2017034823A1 (en) * | 2015-08-27 | 2017-03-02 | Chevron U.S.A. Inc. | Molecular sieve ssz-91, methods for preparing ssz-91, and uses for ssz-91 |
| US20170056870A1 (en) * | 2015-08-27 | 2017-03-02 | Chevron U.S.A. Inc. | Method for making molecular sieve ssz-91 |
| US9663377B1 (en) * | 2015-12-09 | 2017-05-30 | Chevron U.S.A. Inc. | Synthesis of molecular sieve SSZ-105 |
| WO2017200607A1 (en) * | 2016-05-20 | 2017-11-23 | Chevron U.S.A. Inc. | Synthesis of zeolite ssz-16 |
| US9908108B2 (en) * | 2016-06-07 | 2018-03-06 | Chevron U.S.A. Inc. | High-silica AFX framework type zeolites |
| JP6988111B2 (ja) * | 2017-03-17 | 2022-01-05 | 三菱ケミカル株式会社 | 酸素８員環ゼオライトの製造方法 |
-
2017
- 2017-09-07 US US15/697,777 patent/US10053368B1/en active Active
-
2018
- 2018-06-05 WO PCT/IB2018/054000 patent/WO2019048940A1/en not_active Ceased
- 2018-06-05 ES ES18734960T patent/ES2964959T3/es active Active
- 2018-06-05 CN CN201880048378.5A patent/CN110944942B/zh active Active
- 2018-06-05 JP JP2020505855A patent/JP7052007B2/ja active Active
- 2018-06-05 KR KR1020207009880A patent/KR102569712B1/ko active Active
- 2018-06-05 EP EP18734960.0A patent/EP3678993B1/en active Active
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