JP2020089396A - 発酵麦芽飲料及びその製造方法 - Google Patents
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- 235000021577 malt beverage Nutrition 0.000 title claims abstract description 66
- 238000004519 manufacturing process Methods 0.000 title abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 65
- 238000000855 fermentation Methods 0.000 claims abstract description 64
- 230000004151 fermentation Effects 0.000 claims abstract description 64
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 claims abstract description 58
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 38
- 235000019658 bitter taste Nutrition 0.000 claims abstract description 26
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 19
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 19
- 229930007744 linalool Natural products 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims abstract description 19
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 16
- 239000000203 mixture Substances 0.000 claims abstract description 14
- 238000009835 boiling Methods 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims description 16
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 9
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 9
- 230000000694 effects Effects 0.000 claims description 9
- 239000001630 malic acid Substances 0.000 claims description 9
- 235000011090 malic acid Nutrition 0.000 claims description 9
- 108010051210 beta-Fructofuranosidase Proteins 0.000 claims description 5
- 239000001573 invertase Substances 0.000 claims description 5
- 235000011073 invertase Nutrition 0.000 claims description 5
- YOMSJEATGXXYPX-UHFFFAOYSA-N 2-methoxy-4-vinylphenol Chemical compound COC1=CC(C=C)=CC=C1O YOMSJEATGXXYPX-UHFFFAOYSA-N 0.000 description 20
- 235000008694 Humulus lupulus Nutrition 0.000 description 17
- 244000025221 Humulus lupulus Species 0.000 description 17
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 15
- 235000014680 Saccharomyces cerevisiae Nutrition 0.000 description 14
- 235000013339 cereals Nutrition 0.000 description 14
- 239000000047 product Substances 0.000 description 14
- 235000013405 beer Nutrition 0.000 description 10
- 235000000346 sugar Nutrition 0.000 description 10
- 238000012360 testing method Methods 0.000 description 10
- 240000005979 Hordeum vulgare Species 0.000 description 8
- 235000007340 Hordeum vulgare Nutrition 0.000 description 8
- 239000000243 solution Substances 0.000 description 8
- 235000019640 taste Nutrition 0.000 description 8
- 241000218228 Humulus Species 0.000 description 7
- ONIBWKKTOPOVIA-BYPYZUCNSA-N L-Proline Chemical compound OC(=O)[C@@H]1CCCN1 ONIBWKKTOPOVIA-BYPYZUCNSA-N 0.000 description 7
- ONIBWKKTOPOVIA-UHFFFAOYSA-N Proline Natural products OC(=O)C1CCCN1 ONIBWKKTOPOVIA-UHFFFAOYSA-N 0.000 description 7
- 238000011156 evaluation Methods 0.000 description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 235000013361 beverage Nutrition 0.000 description 6
- 238000001914 filtration Methods 0.000 description 6
- 102000004190 Enzymes Human genes 0.000 description 5
- 108090000790 Enzymes Proteins 0.000 description 5
- 238000004458 analytical method Methods 0.000 description 5
- 238000007796 conventional method Methods 0.000 description 5
- 229940088598 enzyme Drugs 0.000 description 5
- 239000000284 extract Substances 0.000 description 5
- 239000000706 filtrate Substances 0.000 description 5
- 239000000796 flavoring agent Substances 0.000 description 5
- 235000019634 flavors Nutrition 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 108091005804 Peptidases Proteins 0.000 description 4
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
- 239000004365 Protease Substances 0.000 description 4
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 4
- 241000209140 Triticum Species 0.000 description 4
- 235000021307 Triticum Nutrition 0.000 description 4
- 150000001413 amino acids Chemical class 0.000 description 4
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 4
- 238000004128 high performance liquid chromatography Methods 0.000 description 4
- 230000001965 increasing effect Effects 0.000 description 4
- 235000015096 spirit Nutrition 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 229920002261 Corn starch Polymers 0.000 description 3
- NHTMVDHEPJAVLT-UHFFFAOYSA-N Isooctane Chemical compound CC(C)CC(C)(C)C NHTMVDHEPJAVLT-UHFFFAOYSA-N 0.000 description 3
- 240000008042 Zea mays Species 0.000 description 3
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 3
- 235000013334 alcoholic beverage Nutrition 0.000 description 3
- 229940041514 candida albicans extract Drugs 0.000 description 3
- 235000005822 corn Nutrition 0.000 description 3
- 239000008120 corn starch Substances 0.000 description 3
- JVSWJIKNEAIKJW-UHFFFAOYSA-N dimethyl-hexane Natural products CCCCCC(C)C JVSWJIKNEAIKJW-UHFFFAOYSA-N 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 150000007524 organic acids Chemical class 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000012138 yeast extract Substances 0.000 description 3
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 description 2
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 2
- 108090000637 alpha-Amylases Proteins 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 2
- 238000004167 beer analysis Methods 0.000 description 2
- 229940116229 borneol Drugs 0.000 description 2
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 description 2
- 235000021329 brown rice Nutrition 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000013065 commercial product Substances 0.000 description 2
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 description 2
- 235000019985 fermented beverage Nutrition 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 235000008216 herbs Nutrition 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 235000020094 liqueur Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000012046 mixed solvent Substances 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 238000011002 quantification Methods 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 239000006188 syrup Substances 0.000 description 2
- 235000020357 syrup Nutrition 0.000 description 2
- 238000004704 ultra performance liquid chromatography Methods 0.000 description 2
- KSEBMYQBYZTDHS-HWKANZROSA-M (E)-Ferulic acid Natural products COC1=CC(\C=C\C([O-])=O)=CC=C1O KSEBMYQBYZTDHS-HWKANZROSA-M 0.000 description 1
- JIZQRWKUYFNSDM-UHFFFAOYSA-N 3,4-dihydroxy-2-(3-methylbutanoyl)-5-(3-methylbutyl)-4-(4-methylpentanoyl)cyclopent-2-en-1-one Chemical compound CC(C)CCC1C(=O)C(C(=O)CC(C)C)=C(O)C1(O)C(=O)CCC(C)C JIZQRWKUYFNSDM-UHFFFAOYSA-N 0.000 description 1
- JENGQFYJSDYTDD-UHFFFAOYSA-N CC(C)CCC(O)C1(O)C(CC=C(C)C)C(O)C(C(=O)CC(C)C)=C1O Chemical compound CC(C)CCC(O)C1(O)C(CC=C(C)C)C(O)C(C(=O)CC(C)C)=C1O JENGQFYJSDYTDD-UHFFFAOYSA-N 0.000 description 1
- 108010073178 Glucan 1,4-alpha-Glucosidase Proteins 0.000 description 1
- 102100022624 Glucoamylase Human genes 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 229930193815 Isohumulone Natural products 0.000 description 1
- 239000005909 Kieselgur Substances 0.000 description 1
- 244000046052 Phaseolus vulgaris Species 0.000 description 1
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- UGXQOOQUZRUVSS-ZZXKWVIFSA-N [5-[3,5-dihydroxy-2-(1,3,4-trihydroxy-5-oxopentan-2-yl)oxyoxan-4-yl]oxy-3,4-dihydroxyoxolan-2-yl]methyl (e)-3-(4-hydroxyphenyl)prop-2-enoate Chemical compound OC1C(OC(CO)C(O)C(O)C=O)OCC(O)C1OC1C(O)C(O)C(COC(=O)\C=C\C=2C=CC(O)=CC=2)O1 UGXQOOQUZRUVSS-ZZXKWVIFSA-N 0.000 description 1
- 238000002835 absorbance Methods 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 102000004139 alpha-Amylases Human genes 0.000 description 1
- 229940024171 alpha-amylase Drugs 0.000 description 1
- 229920000617 arabinoxylan Polymers 0.000 description 1
- -1 barley and wheat Chemical compound 0.000 description 1
- 238000011088 calibration curve Methods 0.000 description 1
- 239000012159 carrier gas Substances 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000006114 decarboxylation reaction Methods 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- KSEBMYQBYZTDHS-UHFFFAOYSA-N ferulic acid Natural products COC1=CC(C=CC(O)=O)=CC=C1O KSEBMYQBYZTDHS-UHFFFAOYSA-N 0.000 description 1
- KSEBMYQBYZTDHS-HWKANZROSA-N ferulic acid Chemical compound COC1=CC(\C=C\C(O)=O)=CC=C1O KSEBMYQBYZTDHS-HWKANZROSA-N 0.000 description 1
- 229940114124 ferulic acid Drugs 0.000 description 1
- 235000001785 ferulic acid Nutrition 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 235000011868 grain product Nutrition 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000010813 internal standard method Methods 0.000 description 1
- 238000001032 ion-exclusion chromatography Methods 0.000 description 1
- QARXXMMQVDCYGZ-UHFFFAOYSA-N isohumulone Chemical compound CC(C)CC(=O)C1=C(O)C(O)(C(=O)CC=C(C)C)C(CC=C(C)C)C1=O QARXXMMQVDCYGZ-UHFFFAOYSA-N 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 235000019520 non-alcoholic beverage Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 235000012015 potatoes Nutrition 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000012086 standard solution Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000035922 thirst Effects 0.000 description 1
- QURCVMIEKCOAJU-UHFFFAOYSA-N trans-isoferulic acid Natural products COC1=CC=C(C=CC(O)=O)C=C1O QURCVMIEKCOAJU-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Landscapes
- Alcoholic Beverages (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
Description
[1] 麦芽比率が50〜66質量%の発酵原料と水とを含む混合物を糖化した後、煮沸して発酵原料液を調製する仕込工程と、
前記仕込工程により得られた発酵原料液に酵母を接種し、発酵を行う発酵工程と、
を少なくとも有し、
4VGの含有量が50〜150質量ppbであり、リナロールの含有量が10質量ppb以下であり、苦味価が10〜30BUである発酵麦芽飲料を製造することを特徴とする、発酵麦芽飲料の製造方法。
[2] 発酵原料の麦芽比率が50〜66質量%であり、4VGの含有量が50〜150質量ppbであり、リナロールの含有量が10質量ppb以下であり、かつ苦味価が10〜30BUであることを特徴とする、発酵麦芽飲料。
[3] リンゴ酸の含有量が50〜150質量ppmである、前記[2]の発酵麦芽飲料。
[4] インベルターゼ活性を有する、前記[2]又は[3]の発酵麦芽飲料。
なお、以降の実施例等において、特に記載のない限り、「%」は「質量%」を、「ppb」は「質量ppb」を、「ppm」は「質量ppm」を、それぞれ意味する。
発酵原料として麦芽粉砕物とコーンスターチを用い、かつ原料として使用するホップの品種及び量を調整することによって、麦芽使用比率と製造される発酵麦芽飲料の苦味価を調整したビールテイストの発酵麦芽飲料を製造し、コク及びキレを評価した。
キャピラリーカラム:商品名「DB−WAX」(長さ60m、内径0.25mm、膜厚0.25μm)、
オーブン温度:40℃(10分)→3℃/分→240℃(20分)、
キャリアガス:He、10psi低圧送気、
トランスファーライン温度:240℃、
MSイオンソース温度:230℃、
MSQポール温度:150℃、
フロント注入口温度:200℃、
定量に用いたイオン:m/z=110(borneol)、m/z=93(linalool)。
Claims (4)
- 麦芽比率が50〜66質量%の発酵原料と水とを含む混合物を糖化した後、煮沸して発酵原料液を調製する仕込工程と、
前記仕込工程により得られた発酵原料液に酵母を接種し、発酵を行う発酵工程と、
を少なくとも有し、
4VGの含有量が50〜150質量ppbであり、リナロールの含有量が10質量ppb以下であり、苦味価が10〜30BUである発酵麦芽飲料を製造することを特徴とする、発酵麦芽飲料の製造方法。 - 発酵原料の麦芽比率が50〜66質量%であり、4VGの含有量が50〜150質量ppbであり、リナロールの含有量が10質量ppb以下であり、かつ苦味価が10〜30BUであることを特徴とする、発酵麦芽飲料。
- リンゴ酸の含有量が50〜150質量ppmである、請求項2に記載の発酵麦芽飲料。
- インベルターゼ活性を有する、請求項2又は3に記載の発酵麦芽飲料。
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JPH11169161A (ja) * | 1997-12-16 | 1999-06-29 | Iyano Kyubee Shoten:Kk | ハト麦発泡酒の製造方法 |
JP2004321004A (ja) * | 2003-04-21 | 2004-11-18 | Asahi Breweries Ltd | 発酵麦芽飲料の製造方法 |
JP2009028007A (ja) * | 2007-07-30 | 2009-02-12 | Asahi Breweries Ltd | 麦芽アルコール飲料の製造方法 |
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JP2012125205A (ja) * | 2010-12-16 | 2012-07-05 | Kirin Brewery Co Ltd | プリン塩基化合物低減高香味ビール風味発酵アルコール飲料及びその製造方法 |
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JP2015123027A (ja) * | 2013-12-27 | 2015-07-06 | アサヒビール株式会社 | 発酵麦芽飲料 |
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2020
- 2020-03-13 JP JP2020044624A patent/JP7245187B2/ja active Active
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JPH11169161A (ja) * | 1997-12-16 | 1999-06-29 | Iyano Kyubee Shoten:Kk | ハト麦発泡酒の製造方法 |
JP2004321004A (ja) * | 2003-04-21 | 2004-11-18 | Asahi Breweries Ltd | 発酵麦芽飲料の製造方法 |
JP2009028007A (ja) * | 2007-07-30 | 2009-02-12 | Asahi Breweries Ltd | 麦芽アルコール飲料の製造方法 |
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